Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves

A combined effect of microwave irradiation and solvent types on the phenolic compounds extraction from Orthosiphon stamineus leaves was studied. The effect of as extraction time, the microwave irradiation power and solid to solvent ratio on the extraction yield was studied. Aqueous solvent provides...

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Main Authors: Sook, Fun Pang, Mei, Zhu Lau, M. M., Yusoff, Jolius, Gimbun
Format: Article
Language:English
Published: Trans Tech Publications 2017
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/16376/1/fist-2017-pang-Microwave-Irradiation%20Induced%20Fast%20Simultaneous1.pdf
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author Sook, Fun Pang
Mei, Zhu Lau
M. M., Yusoff
Jolius, Gimbun
author_facet Sook, Fun Pang
Mei, Zhu Lau
M. M., Yusoff
Jolius, Gimbun
author_sort Sook, Fun Pang
collection UMP
description A combined effect of microwave irradiation and solvent types on the phenolic compounds extraction from Orthosiphon stamineus leaves was studied. The effect of as extraction time, the microwave irradiation power and solid to solvent ratio on the extraction yield was studied. Aqueous solvent provides a broader range of polarity than the pure solvent, and hence enabled a simultaneous extraction of both methoxylated and hydroxylated phenolic compounds. It was found that the extraction time of 2 minutes, microwave irradiation power at 300W and 20:1 solvent to solid ratio yielded highest simultaneous extraction of polyphenols (i.e. rosmarinic acid 32.45 mg RA/g DW, sinensetin 261.15 ?g Sin/g DW and eupatorin 2.27 mg Eup/g DW). Result from this work may serve as a useful guide to obtain higher yield of polyphenols from O. stamineus.
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spelling UMPir163762018-02-12T05:57:45Z http://umpir.ump.edu.my/id/eprint/16376/ Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves Sook, Fun Pang Mei, Zhu Lau M. M., Yusoff Jolius, Gimbun TP Chemical technology A combined effect of microwave irradiation and solvent types on the phenolic compounds extraction from Orthosiphon stamineus leaves was studied. The effect of as extraction time, the microwave irradiation power and solid to solvent ratio on the extraction yield was studied. Aqueous solvent provides a broader range of polarity than the pure solvent, and hence enabled a simultaneous extraction of both methoxylated and hydroxylated phenolic compounds. It was found that the extraction time of 2 minutes, microwave irradiation power at 300W and 20:1 solvent to solid ratio yielded highest simultaneous extraction of polyphenols (i.e. rosmarinic acid 32.45 mg RA/g DW, sinensetin 261.15 ?g Sin/g DW and eupatorin 2.27 mg Eup/g DW). Result from this work may serve as a useful guide to obtain higher yield of polyphenols from O. stamineus. Trans Tech Publications 2017-03 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/16376/1/fist-2017-pang-Microwave-Irradiation%20Induced%20Fast%20Simultaneous1.pdf Sook, Fun Pang and Mei, Zhu Lau and M. M., Yusoff and Jolius, Gimbun (2017) Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves. Materials Science Forum, 890. pp. 155-158. ISSN 0255-5476. (Published) http://dx.doi.org/10.4028/www.scientific.net/MSF.890.155 doi: 10.4028/www.scientific.net/MSF.890.155
spellingShingle TP Chemical technology
Sook, Fun Pang
Mei, Zhu Lau
M. M., Yusoff
Jolius, Gimbun
Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves
title Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves
title_full Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves
title_fullStr Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves
title_full_unstemmed Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves
title_short Microwave-Irradiation Induced Fast Simultaneous Extraction of Methoxylated and Hydroxylated Phenolic Compounds from Orthosiphon stamineus Leaves
title_sort microwave irradiation induced fast simultaneous extraction of methoxylated and hydroxylated phenolic compounds from orthosiphon stamineus leaves
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/16376/1/fist-2017-pang-Microwave-Irradiation%20Induced%20Fast%20Simultaneous1.pdf
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