Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler

This paper studies on the effect of the addition of carbon filler towards the performance of superabsorbent polymer composite (SAPc). In this work, the SAPc was synthesized using inverse suspension polymerization method. The process involved two different solutions; dispersed phase which contains pa...

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Main Authors: Munirah Ezzah, Tuan Zakaria, Saidatul Shima, Jamari, Yeong, Yi Ling, Suriati, Ghazali
Format: Article
Language:English
English
Published: IOP Publishing 2017
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/18097/1/Synthesis%20of%20Superabsorbent%20Polymer%20via%20Inverse%20Suspension%20Method-%20Effect%20of%20Carbon%20Filler.pdf
http://umpir.ump.edu.my/id/eprint/18097/2/Synthesis%20of%20Superabsorbent%20Polymer%20via%20Inverse%20Suspension%20Method-%20Effect%20of%20Carbon%20Filler%201.pdf
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author Munirah Ezzah, Tuan Zakaria
Saidatul Shima, Jamari
Yeong, Yi Ling
Suriati, Ghazali
author_facet Munirah Ezzah, Tuan Zakaria
Saidatul Shima, Jamari
Yeong, Yi Ling
Suriati, Ghazali
author_sort Munirah Ezzah, Tuan Zakaria
collection UMP
description This paper studies on the effect of the addition of carbon filler towards the performance of superabsorbent polymer composite (SAPc). In this work, the SAPc was synthesized using inverse suspension polymerization method. The process involved two different solutions; dispersed phase which contains partially neutralized acrylic acid, acrylamide, APS and NN-Methylenebisacrylamide, and continuous phase which contains cyclohexane, span-80 and carbon filler (at different weight percent). The optimum SAPs and filler ratio was measured in terms of water retention in soil and characterized by Mastersizer, FTIR and SEM. Biodegradability of the polymer was determined by soil burial test and SAPc with 0.02% carbon has highest biodegradability rate. SAPc with 0.04wt% carbon showed the optimal water retention percentage among all the samples. The synthesized SAPc producing spherical shapes with parallel alignment due to the addition of carbon fiber. It can be concluded that the addition of carbon fiber able to enhance the performance of the SAP composite (SAPc).
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spelling UMPir180972017-08-10T06:58:29Z http://umpir.ump.edu.my/id/eprint/18097/ Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler Munirah Ezzah, Tuan Zakaria Saidatul Shima, Jamari Yeong, Yi Ling Suriati, Ghazali TP Chemical technology This paper studies on the effect of the addition of carbon filler towards the performance of superabsorbent polymer composite (SAPc). In this work, the SAPc was synthesized using inverse suspension polymerization method. The process involved two different solutions; dispersed phase which contains partially neutralized acrylic acid, acrylamide, APS and NN-Methylenebisacrylamide, and continuous phase which contains cyclohexane, span-80 and carbon filler (at different weight percent). The optimum SAPs and filler ratio was measured in terms of water retention in soil and characterized by Mastersizer, FTIR and SEM. Biodegradability of the polymer was determined by soil burial test and SAPc with 0.02% carbon has highest biodegradability rate. SAPc with 0.04wt% carbon showed the optimal water retention percentage among all the samples. The synthesized SAPc producing spherical shapes with parallel alignment due to the addition of carbon fiber. It can be concluded that the addition of carbon fiber able to enhance the performance of the SAP composite (SAPc). IOP Publishing 2017 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/18097/1/Synthesis%20of%20Superabsorbent%20Polymer%20via%20Inverse%20Suspension%20Method-%20Effect%20of%20Carbon%20Filler.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/18097/2/Synthesis%20of%20Superabsorbent%20Polymer%20via%20Inverse%20Suspension%20Method-%20Effect%20of%20Carbon%20Filler%201.pdf Munirah Ezzah, Tuan Zakaria and Saidatul Shima, Jamari and Yeong, Yi Ling and Suriati, Ghazali (2017) Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler. IOP Conference Series: Materials Science and Engineering, 204 (1). pp. 1-6. ISSN 1757-8981 (Print), 1757-899X (Online). (Published) http://iopscience.iop.org/article/10.1088/1757-899X/204/1/012013/meta doi:10.1088/1757-899X/204/1/012013
spellingShingle TP Chemical technology
Munirah Ezzah, Tuan Zakaria
Saidatul Shima, Jamari
Yeong, Yi Ling
Suriati, Ghazali
Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler
title Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler
title_full Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler
title_fullStr Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler
title_full_unstemmed Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler
title_short Synthesis of Superabsorbent Polymer via Inverse Suspension Method: Effect of Carbon Filler
title_sort synthesis of superabsorbent polymer via inverse suspension method effect of carbon filler
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/18097/1/Synthesis%20of%20Superabsorbent%20Polymer%20via%20Inverse%20Suspension%20Method-%20Effect%20of%20Carbon%20Filler.pdf
http://umpir.ump.edu.my/id/eprint/18097/2/Synthesis%20of%20Superabsorbent%20Polymer%20via%20Inverse%20Suspension%20Method-%20Effect%20of%20Carbon%20Filler%201.pdf
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