Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood

Agarwood is well known as one of the expensive woods in the world. It has a unique scent which brings it to have wide usages especially in perfumery ingredient, as incense, in traditional medical preparation, and as symbol of wealth. Due to that, this paper presents the analysis on chemical profiles...

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Main Authors: Nurlaila, Ismail, Mohd Hezri, Fazalul Rahiman, Mohd Nasir, Taib, Mastura, Ibrahim, Seema, Zareen, Saiful Nizam, Tajuddin
Format: Conference or Workshop Item
Language:English
English
Published: Institute of Electrical and Electronics Engineers Inc. 2016
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/18252/1/Observation%20on%20SPME%20Different%20Headspace%20Fiber%20Coupled%20with%20GC-MS%20in%20Extracting%20High%20Quality%20Agarwood%20Chipwood.pdf
http://umpir.ump.edu.my/id/eprint/18252/7/Observation%20on%20SPME%20Different%20Headspace%20Fiber%20Coupled%20with%20GC-MS%20in%20Extracting%20High%20Quality%20Agarwood%20Chipwood%201.pdf
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author Nurlaila, Ismail
Mohd Hezri, Fazalul Rahiman
Mohd Nasir, Taib
Mastura, Ibrahim
Seema, Zareen
Saiful Nizam, Tajuddin
author_facet Nurlaila, Ismail
Mohd Hezri, Fazalul Rahiman
Mohd Nasir, Taib
Mastura, Ibrahim
Seema, Zareen
Saiful Nizam, Tajuddin
author_sort Nurlaila, Ismail
collection UMP
description Agarwood is well known as one of the expensive woods in the world. It has a unique scent which brings it to have wide usages especially in perfumery ingredient, as incense, in traditional medical preparation, and as symbol of wealth. Due to that, this paper presents the analysis on chemical profiles of agarwood chipwood, as a part of agarwood grading system. The work involved of Solid Phase Microextraction (SPME) coupled with Gas Chromatography - Mass Spectrometry (GC-MS) GC-MS in extracting high quality. Three headspace fibers; PDMS-DVB, CAR-PDMS and DVB-CAR-PDMS were used during the extraction to identify the compounds with the sampling time of 60 minutes. The result showed that high quality agarwood chipwood is made up of terpene group which are monoterpene hydrocarbon, sesquiterpene hydrocarbon and oxygenated sesquiterpene. The relative peak areas (%) for compounds are tabulated and plotted. The finding in this study confirmed that the difference in compounds extracted and their relative peak area (%) are due to different fiber's polarity and absorbent, Thus, it is significant and benefit especially in agarwood oil quality grading and its related area.
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spelling UMPir182522018-04-10T03:09:23Z http://umpir.ump.edu.my/id/eprint/18252/ Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood Nurlaila, Ismail Mohd Hezri, Fazalul Rahiman Mohd Nasir, Taib Mastura, Ibrahim Seema, Zareen Saiful Nizam, Tajuddin Q Science (General) Agarwood is well known as one of the expensive woods in the world. It has a unique scent which brings it to have wide usages especially in perfumery ingredient, as incense, in traditional medical preparation, and as symbol of wealth. Due to that, this paper presents the analysis on chemical profiles of agarwood chipwood, as a part of agarwood grading system. The work involved of Solid Phase Microextraction (SPME) coupled with Gas Chromatography - Mass Spectrometry (GC-MS) GC-MS in extracting high quality. Three headspace fibers; PDMS-DVB, CAR-PDMS and DVB-CAR-PDMS were used during the extraction to identify the compounds with the sampling time of 60 minutes. The result showed that high quality agarwood chipwood is made up of terpene group which are monoterpene hydrocarbon, sesquiterpene hydrocarbon and oxygenated sesquiterpene. The relative peak areas (%) for compounds are tabulated and plotted. The finding in this study confirmed that the difference in compounds extracted and their relative peak area (%) are due to different fiber's polarity and absorbent, Thus, it is significant and benefit especially in agarwood oil quality grading and its related area. Institute of Electrical and Electronics Engineers Inc. 2016 Conference or Workshop Item PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/18252/1/Observation%20on%20SPME%20Different%20Headspace%20Fiber%20Coupled%20with%20GC-MS%20in%20Extracting%20High%20Quality%20Agarwood%20Chipwood.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/18252/7/Observation%20on%20SPME%20Different%20Headspace%20Fiber%20Coupled%20with%20GC-MS%20in%20Extracting%20High%20Quality%20Agarwood%20Chipwood%201.pdf Nurlaila, Ismail and Mohd Hezri, Fazalul Rahiman and Mohd Nasir, Taib and Mastura, Ibrahim and Seema, Zareen and Saiful Nizam, Tajuddin (2016) Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood. In: International Conference on Automatic Control and Intelligent Systems (I2CACIS) , 22 October 2016 , Shah Alam, Selangor. pp. 214-218.. ISBN 978-1-5090-4186-2 http://ieeexplore.ieee.org/abstract/document/7885317/
spellingShingle Q Science (General)
Nurlaila, Ismail
Mohd Hezri, Fazalul Rahiman
Mohd Nasir, Taib
Mastura, Ibrahim
Seema, Zareen
Saiful Nizam, Tajuddin
Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood
title Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood
title_full Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood
title_fullStr Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood
title_full_unstemmed Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood
title_short Observation on SPME different headspace fiber coupled with GC-MS in extracting high quality agarwood chipwood
title_sort observation on spme different headspace fiber coupled with gc ms in extracting high quality agarwood chipwood
topic Q Science (General)
url http://umpir.ump.edu.my/id/eprint/18252/1/Observation%20on%20SPME%20Different%20Headspace%20Fiber%20Coupled%20with%20GC-MS%20in%20Extracting%20High%20Quality%20Agarwood%20Chipwood.pdf
http://umpir.ump.edu.my/id/eprint/18252/7/Observation%20on%20SPME%20Different%20Headspace%20Fiber%20Coupled%20with%20GC-MS%20in%20Extracting%20High%20Quality%20Agarwood%20Chipwood%201.pdf
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