Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata
Oil palm frond (OPF) juice has been known as a good source of sugars to replace commercial sugars to produce methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate. The aim of this study was to investigate the effect of temperature (°C), initial pH medium, agitation speed (rpm) and concentration of...
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| Format: | Conference or Workshop Item |
| Language: | English English |
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Penerbit UTM Press
2017
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| Subjects: | |
| Online Access: | http://umpir.ump.edu.my/id/eprint/20263/2/fkksa-2017-nang-Full%20Factorial%20Design%20for%20Production%20of%20Methyl%2031.pdf http://umpir.ump.edu.my/id/eprint/20263/4/fkksa-2017-nang-Full%20Factorial%20Design%20for%20Production%20of%20Methyl%203.pdf |
| _version_ | 1796992539725660160 |
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| author | Nang Nor Azimah, Long Nadzri Mior Ahmad Khushairi, Mohd Zahari Saiful Nizam, Tajuddin Che Mohd Aizal, Che Mohd |
| author_facet | Nang Nor Azimah, Long Nadzri Mior Ahmad Khushairi, Mohd Zahari Saiful Nizam, Tajuddin Che Mohd Aizal, Che Mohd |
| author_sort | Nang Nor Azimah, Long Nadzri |
| collection | UMP |
| description | Oil palm frond (OPF) juice has been known as a good source of sugars to replace commercial sugars to produce methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate. The aim of this study was to investigate the effect of temperature (°C), initial pH medium, agitation speed (rpm) and concentration of glucose (g/L) on the production of methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate from OPF juice by using Ceratocystis fimbriata (C. fimbriata). The design of experiment (DOE) method was used to screen the best parameters affecting the production of methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate. The Gas Chromatography-Mass Spectroscopy (GC-MS) with Solid Phase Micro Extraction (SPME) was used to analyze and separate the peak of methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate. Based on the GC-MS analysis, it showed that the most favorable condition for methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate production was achieved at an initial pH medium (8), agitation speed (100 rpm), temperature (25°C) and 30 g/L of glucose in OPF juice. Methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate were produced when the retention time was 32.80 min, the relative peak area was 0.24 % of chromatogram area. This result showed the great potential usage of OPF juice as a substrate to produce methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate by C. fimbriata. |
| first_indexed | 2024-03-06T12:21:29Z |
| format | Conference or Workshop Item |
| id | UMPir20263 |
| institution | Universiti Malaysia Pahang |
| language | English English |
| last_indexed | 2024-03-06T12:21:29Z |
| publishDate | 2017 |
| publisher | Penerbit UTM Press |
| record_format | dspace |
| spelling | UMPir202632018-01-22T01:34:27Z http://umpir.ump.edu.my/id/eprint/20263/ Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata Nang Nor Azimah, Long Nadzri Mior Ahmad Khushairi, Mohd Zahari Saiful Nizam, Tajuddin Che Mohd Aizal, Che Mohd TP Chemical technology Oil palm frond (OPF) juice has been known as a good source of sugars to replace commercial sugars to produce methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate. The aim of this study was to investigate the effect of temperature (°C), initial pH medium, agitation speed (rpm) and concentration of glucose (g/L) on the production of methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate from OPF juice by using Ceratocystis fimbriata (C. fimbriata). The design of experiment (DOE) method was used to screen the best parameters affecting the production of methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate. The Gas Chromatography-Mass Spectroscopy (GC-MS) with Solid Phase Micro Extraction (SPME) was used to analyze and separate the peak of methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate. Based on the GC-MS analysis, it showed that the most favorable condition for methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate production was achieved at an initial pH medium (8), agitation speed (100 rpm), temperature (25°C) and 30 g/L of glucose in OPF juice. Methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate were produced when the retention time was 32.80 min, the relative peak area was 0.24 % of chromatogram area. This result showed the great potential usage of OPF juice as a substrate to produce methyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate by C. fimbriata. Penerbit UTM Press 2017 Conference or Workshop Item PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/20263/2/fkksa-2017-nang-Full%20Factorial%20Design%20for%20Production%20of%20Methyl%2031.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/20263/4/fkksa-2017-nang-Full%20Factorial%20Design%20for%20Production%20of%20Methyl%203.pdf Nang Nor Azimah, Long Nadzri and Mior Ahmad Khushairi, Mohd Zahari and Saiful Nizam, Tajuddin and Che Mohd Aizal, Che Mohd (2017) Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata. In: 2nd International Conference on Separation Technology (ICoST’17) , 15-16 April 2017 , Johor Bahru, Malaysia. pp. 1-10.. ISBN 978-967-0194-85-1 |
| spellingShingle | TP Chemical technology Nang Nor Azimah, Long Nadzri Mior Ahmad Khushairi, Mohd Zahari Saiful Nizam, Tajuddin Che Mohd Aizal, Che Mohd Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata |
| title | Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata |
| title_full | Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata |
| title_fullStr | Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata |
| title_full_unstemmed | Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata |
| title_short | Full Factorial Design for Production of Methyl 3-(3,5-Di-Tert-Butyl-4-Hydroxyphenyl) Propionate Using Oil Palm Frond Juice as a Sole Substrate by Ceratocystis fimbriata |
| title_sort | full factorial design for production of methyl 3 3 5 di tert butyl 4 hydroxyphenyl propionate using oil palm frond juice as a sole substrate by ceratocystis fimbriata |
| topic | TP Chemical technology |
| url | http://umpir.ump.edu.my/id/eprint/20263/2/fkksa-2017-nang-Full%20Factorial%20Design%20for%20Production%20of%20Methyl%2031.pdf http://umpir.ump.edu.my/id/eprint/20263/4/fkksa-2017-nang-Full%20Factorial%20Design%20for%20Production%20of%20Methyl%203.pdf |
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