The influence of growth temperature on the properties of zinc oxide by thermal oxidation

Zinc thin films were successfully deposited on Si substrate by thermal evaporation method under constant base pressure of 1.604x10-4 Pa. Thermal oxidation of the deposited film was carried out at two different growth temperatures of 300oC and 500oC. The effects of growth temperature on the propertie...

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Main Authors: Nuraini, Abdullah, Noor Mazni, Ismail, Dewan Muhammad, Nuruzzaman
Format: Article
Language:English
English
Published: The Malaysian Analytical Sciences Society 2018
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/21111/1/The%20influence%20of%20growth%20temperature-fkp-2018.pdf
http://umpir.ump.edu.my/id/eprint/21111/7/The%20influence%20of%20growth%20temperature-fkp-2018-1.pdf
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author Nuraini, Abdullah
Noor Mazni, Ismail
Dewan Muhammad, Nuruzzaman
author_facet Nuraini, Abdullah
Noor Mazni, Ismail
Dewan Muhammad, Nuruzzaman
author_sort Nuraini, Abdullah
collection UMP
description Zinc thin films were successfully deposited on Si substrate by thermal evaporation method under constant base pressure of 1.604x10-4 Pa. Thermal oxidation of the deposited film was carried out at two different growth temperatures of 300oC and 500oC. The effects of growth temperature on the properties of zinc oxide were investigated. Thermal oxidation for constant time 1 hour in horizontal tube furnace in air condition was carried out. The white-silver zinc thin films were changed to black-brown zinc oxide after thermal oxidation at temperature 500oC. FESEM results show that the zinc particles were almost round shape with nanostructures in size. ZnO nanowires were successfully obtained at low growth temperature of 300oC and the size become decrease as the growth temperature was increased to 500oC. The XRD results confirmed that ZnO was started to oxidize at growth temperature of 300oC with the sharpest peak obtained was indexed to ZnO(101). However, the oxidation of Zn was not fully completed while there are Zn peaks appear at this temperature. At growth temperature 500oC, all the peaks were indexed to ZnO with the sharpest peak was ZnO(101) meaning that the oxidation was completed. The calculated particle sizes were varied from 27.841nm to 36.788nm for ZnO at 300°C and 0.697nm to 161.18nm for ZnO of 500°C.
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spelling UMPir211112022-03-14T02:40:39Z http://umpir.ump.edu.my/id/eprint/21111/ The influence of growth temperature on the properties of zinc oxide by thermal oxidation Nuraini, Abdullah Noor Mazni, Ismail Dewan Muhammad, Nuruzzaman T Technology (General) TS Manufactures Zinc thin films were successfully deposited on Si substrate by thermal evaporation method under constant base pressure of 1.604x10-4 Pa. Thermal oxidation of the deposited film was carried out at two different growth temperatures of 300oC and 500oC. The effects of growth temperature on the properties of zinc oxide were investigated. Thermal oxidation for constant time 1 hour in horizontal tube furnace in air condition was carried out. The white-silver zinc thin films were changed to black-brown zinc oxide after thermal oxidation at temperature 500oC. FESEM results show that the zinc particles were almost round shape with nanostructures in size. ZnO nanowires were successfully obtained at low growth temperature of 300oC and the size become decrease as the growth temperature was increased to 500oC. The XRD results confirmed that ZnO was started to oxidize at growth temperature of 300oC with the sharpest peak obtained was indexed to ZnO(101). However, the oxidation of Zn was not fully completed while there are Zn peaks appear at this temperature. At growth temperature 500oC, all the peaks were indexed to ZnO with the sharpest peak was ZnO(101) meaning that the oxidation was completed. The calculated particle sizes were varied from 27.841nm to 36.788nm for ZnO at 300°C and 0.697nm to 161.18nm for ZnO of 500°C. The Malaysian Analytical Sciences Society 2018 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/21111/1/The%20influence%20of%20growth%20temperature-fkp-2018.pdf pdf en http://umpir.ump.edu.my/id/eprint/21111/7/The%20influence%20of%20growth%20temperature-fkp-2018-1.pdf Nuraini, Abdullah and Noor Mazni, Ismail and Dewan Muhammad, Nuruzzaman (2018) The influence of growth temperature on the properties of zinc oxide by thermal oxidation. Malaysian Journal of Analytical Sciences, 22 (6). pp. 1084-1089. ISSN 1394 - 2506. (Published) https://doi.org/10.17576/mjas-2018-2206-19 https://doi.org/10.17576/mjas-2018-2206-19
spellingShingle T Technology (General)
TS Manufactures
Nuraini, Abdullah
Noor Mazni, Ismail
Dewan Muhammad, Nuruzzaman
The influence of growth temperature on the properties of zinc oxide by thermal oxidation
title The influence of growth temperature on the properties of zinc oxide by thermal oxidation
title_full The influence of growth temperature on the properties of zinc oxide by thermal oxidation
title_fullStr The influence of growth temperature on the properties of zinc oxide by thermal oxidation
title_full_unstemmed The influence of growth temperature on the properties of zinc oxide by thermal oxidation
title_short The influence of growth temperature on the properties of zinc oxide by thermal oxidation
title_sort influence of growth temperature on the properties of zinc oxide by thermal oxidation
topic T Technology (General)
TS Manufactures
url http://umpir.ump.edu.my/id/eprint/21111/1/The%20influence%20of%20growth%20temperature-fkp-2018.pdf
http://umpir.ump.edu.my/id/eprint/21111/7/The%20influence%20of%20growth%20temperature-fkp-2018-1.pdf
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