Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction

Central composite designs (CCDs) for UAE and WE were established by seven and five extraction factors, respectively, to determine their optimum conditions that maximized the saponins yields. These optimum conditions were employed successively to establish a sequential extraction (SE) of saponins fro...

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Main Authors: Elhag, Husam Eldin Elhag Abugabr, Nailaa, Aishath, Azilah, Ajit, Badhrulhisham, Abdul Aziz, Ahmad Ziad, Sulaiman
Format: Article
Language:English
Published: Elsevier Ltd 2018
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/21763/1/Sequential%20Extraction%20of%20Saponins%20from%20Eurycoma%20longifolia-1.pdf
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author Elhag, Husam Eldin Elhag Abugabr
Nailaa, Aishath
Azilah, Ajit
Badhrulhisham, Abdul Aziz
Ahmad Ziad, Sulaiman
author_facet Elhag, Husam Eldin Elhag Abugabr
Nailaa, Aishath
Azilah, Ajit
Badhrulhisham, Abdul Aziz
Ahmad Ziad, Sulaiman
author_sort Elhag, Husam Eldin Elhag Abugabr
collection UMP
description Central composite designs (CCDs) for UAE and WE were established by seven and five extraction factors, respectively, to determine their optimum conditions that maximized the saponins yields. These optimum conditions were employed successively to establish a sequential extraction (SE) of saponins from Eurycoma longifolia roots. Results identified the agitation speed as an influencing factor in altering the interactive effects of the extraction factors in UAE and WE. Optimized conditions illustrated that higher agitation speeds increased the yields of saponins in WE while UAE preferred lower agitation speed ranges. This implied that the high agitation speeds decreased the collision of microjets and particles and hence the the decrease of sonication efficiency. The SE extraction was proposed by initial sonication of the plant sample for a duration of 5 minutes and 29 seconds to 10 minutes followed by conventional WE for 20-25 minutes.
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spelling UMPir217632020-06-26T02:48:39Z http://umpir.ump.edu.my/id/eprint/21763/ Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction Elhag, Husam Eldin Elhag Abugabr Nailaa, Aishath Azilah, Ajit Badhrulhisham, Abdul Aziz Ahmad Ziad, Sulaiman TP Chemical technology Central composite designs (CCDs) for UAE and WE were established by seven and five extraction factors, respectively, to determine their optimum conditions that maximized the saponins yields. These optimum conditions were employed successively to establish a sequential extraction (SE) of saponins from Eurycoma longifolia roots. Results identified the agitation speed as an influencing factor in altering the interactive effects of the extraction factors in UAE and WE. Optimized conditions illustrated that higher agitation speeds increased the yields of saponins in WE while UAE preferred lower agitation speed ranges. This implied that the high agitation speeds decreased the collision of microjets and particles and hence the the decrease of sonication efficiency. The SE extraction was proposed by initial sonication of the plant sample for a duration of 5 minutes and 29 seconds to 10 minutes followed by conventional WE for 20-25 minutes. Elsevier Ltd 2018 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/21763/1/Sequential%20Extraction%20of%20Saponins%20from%20Eurycoma%20longifolia-1.pdf Elhag, Husam Eldin Elhag Abugabr and Nailaa, Aishath and Azilah, Ajit and Badhrulhisham, Abdul Aziz and Ahmad Ziad, Sulaiman (2018) Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction. Materials Today: Proceedings, 5 (10 Part 2). pp. 1-10. ISSN 2214-7853. (Published) https://doi.org/10.1016/j.matpr.2018.07.018 https://doi.org/10.1016/j.matpr.2018.07.018
spellingShingle TP Chemical technology
Elhag, Husam Eldin Elhag Abugabr
Nailaa, Aishath
Azilah, Ajit
Badhrulhisham, Abdul Aziz
Ahmad Ziad, Sulaiman
Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction
title Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction
title_full Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction
title_fullStr Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction
title_full_unstemmed Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction
title_short Sequential extraction of saponins from Eurycoma longifolia roots by water extraction and ultrasound-assisted extraction
title_sort sequential extraction of saponins from eurycoma longifolia roots by water extraction and ultrasound assisted extraction
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/21763/1/Sequential%20Extraction%20of%20Saponins%20from%20Eurycoma%20longifolia-1.pdf
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