Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption

The increase of carbon dioxide (CO2) concentrations in the atmosphere is one of alarming issues nowadays. Thus, development and optimization of new solid adsorbents is highly demanded for the establishment of energy-efficient and high-throughput CO2 capture pro...

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Main Authors: Nur Fatihah, Tajul Arifin, Nur Azira Natasha, Zulkipli, Norhaniza, Yusof, Ahmad Fauzi, Ismail, Farhana, Aziz, Wan Norharyati, Wan Salleh, Juhana, Jaafar, Nik Abdul Hadi, Md Nordin, Norazlianie, Sazali
Format: Article
Language:English
Published: Akademi Baru 2019
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/26176/7/Preparation%20and%20Characterization%20of%20APTES.pdf
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author Nur Fatihah, Tajul Arifin
Nur Azira Natasha, Zulkipli
Norhaniza, Yusof
Ahmad Fauzi, Ismail
Farhana, Aziz
Wan Norharyati, Wan Salleh
Juhana, Jaafar
Nik Abdul Hadi, Md Nordin
Norazlianie, Sazali
author_facet Nur Fatihah, Tajul Arifin
Nur Azira Natasha, Zulkipli
Norhaniza, Yusof
Ahmad Fauzi, Ismail
Farhana, Aziz
Wan Norharyati, Wan Salleh
Juhana, Jaafar
Nik Abdul Hadi, Md Nordin
Norazlianie, Sazali
author_sort Nur Fatihah, Tajul Arifin
collection UMP
description The increase of carbon dioxide (CO2) concentrations in the atmosphere is one of alarming issues nowadays. Thus, development and optimization of new solid adsorbents is highly demanded for the establishment of energy-efficient and high-throughput CO2 capture processes in industry. Herein, graphene oxide (GO) adsorbent was prepared and further functionalized by amine functionalization, 3-aminopropyl-triethoxysilane (APTES). GO was prepared using Modified Hummer’s Method followed by functionalization with APTES. GO and APTES-GO were characterized using Fourier Transmission Infrared Spectroscopy (FTIR), Raman spectroscopy, scanning electron microscope (SEM), and N2 adsorption isotherm. The N2 adsorption capacity for APTES. GO at 15 bar is the highest (179 mmol/g) compared to other lower pressures and pristine GO at any pressure. FTIR analysis showed significant peaks at 1474 cm−1 and 1440cm−1 indicating the presence of N-H and NH2 groups, respectively
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spelling UMPir261762019-11-29T04:30:44Z http://umpir.ump.edu.my/id/eprint/26176/ Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption Nur Fatihah, Tajul Arifin Nur Azira Natasha, Zulkipli Norhaniza, Yusof Ahmad Fauzi, Ismail Farhana, Aziz Wan Norharyati, Wan Salleh Juhana, Jaafar Nik Abdul Hadi, Md Nordin Norazlianie, Sazali Q Science (General) The increase of carbon dioxide (CO2) concentrations in the atmosphere is one of alarming issues nowadays. Thus, development and optimization of new solid adsorbents is highly demanded for the establishment of energy-efficient and high-throughput CO2 capture processes in industry. Herein, graphene oxide (GO) adsorbent was prepared and further functionalized by amine functionalization, 3-aminopropyl-triethoxysilane (APTES). GO was prepared using Modified Hummer’s Method followed by functionalization with APTES. GO and APTES-GO were characterized using Fourier Transmission Infrared Spectroscopy (FTIR), Raman spectroscopy, scanning electron microscope (SEM), and N2 adsorption isotherm. The N2 adsorption capacity for APTES. GO at 15 bar is the highest (179 mmol/g) compared to other lower pressures and pristine GO at any pressure. FTIR analysis showed significant peaks at 1474 cm−1 and 1440cm−1 indicating the presence of N-H and NH2 groups, respectively Akademi Baru 2019 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/26176/7/Preparation%20and%20Characterization%20of%20APTES.pdf Nur Fatihah, Tajul Arifin and Nur Azira Natasha, Zulkipli and Norhaniza, Yusof and Ahmad Fauzi, Ismail and Farhana, Aziz and Wan Norharyati, Wan Salleh and Juhana, Jaafar and Nik Abdul Hadi, Md Nordin and Norazlianie, Sazali (2019) Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption. Journal of Advanced Research in Fluid Mechanics and Thermal Sciences, 61 (2). pp. 297-305. ISSN 2289-7879. (Published) http://www.akademiabaru.com/doc/ARFMTSV61_N2_P297_305.pdf
spellingShingle Q Science (General)
Nur Fatihah, Tajul Arifin
Nur Azira Natasha, Zulkipli
Norhaniza, Yusof
Ahmad Fauzi, Ismail
Farhana, Aziz
Wan Norharyati, Wan Salleh
Juhana, Jaafar
Nik Abdul Hadi, Md Nordin
Norazlianie, Sazali
Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption
title Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption
title_full Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption
title_fullStr Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption
title_full_unstemmed Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption
title_short Preparation and characterization of APTES-functionalized graphene oxide for CO2 adsorption
title_sort preparation and characterization of aptes functionalized graphene oxide for co2 adsorption
topic Q Science (General)
url http://umpir.ump.edu.my/id/eprint/26176/7/Preparation%20and%20Characterization%20of%20APTES.pdf
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