POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique
Thermal degradation kinetics and mechanism of gallic acid was investigated at temperatures ranging from 60 to 120 °C with a heating time of 90 min. The ultra-performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometer was used to elucidate the degradation mechanism of...
| Main Authors: | , , , , |
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| Format: | Conference or Workshop Item |
| Language: | English |
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University of Nottingham
2019
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| Online Access: | http://umpir.ump.edu.my/id/eprint/26835/1/POCER1914_Elucidation%20of%20Gallic%20Acid%20Degradation.pdf |
| _version_ | 1825813052867477504 |
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| author | Afiqah, Yeop Pang, Sook Fun M. M., Yusoff Sureena, Abdullah Jolius, Gimbun |
| author_facet | Afiqah, Yeop Pang, Sook Fun M. M., Yusoff Sureena, Abdullah Jolius, Gimbun |
| author_sort | Afiqah, Yeop |
| collection | UMP |
| description | Thermal degradation kinetics and mechanism of gallic acid was investigated at temperatures ranging from 60 to 120 °C with a heating time of 90 min. The ultra-performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometer was used to elucidate the degradation mechanism of gallic acid in the heated sample. The degradation kinetics of gallic acid shows a good fit with the 1st order model with correlation coefficients of R2 ≥ 0.96. The kinetics rate constant (k) were 0.0011, 0.0038 and 0.0076 min-1 at the temperature of 60, 90 and 120 °C, respectively. This finding in this work may serve as a useful guide to minimize the gallic acid degradation and formation of unwanted by-products during processing of L. pumila. |
| first_indexed | 2024-03-06T12:38:18Z |
| format | Conference or Workshop Item |
| id | UMPir26835 |
| institution | Universiti Malaysia Pahang |
| language | English |
| last_indexed | 2024-03-06T12:38:18Z |
| publishDate | 2019 |
| publisher | University of Nottingham |
| record_format | dspace |
| spelling | UMPir268352019-12-16T08:04:13Z http://umpir.ump.edu.my/id/eprint/26835/ POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique Afiqah, Yeop Pang, Sook Fun M. M., Yusoff Sureena, Abdullah Jolius, Gimbun TP Chemical technology Thermal degradation kinetics and mechanism of gallic acid was investigated at temperatures ranging from 60 to 120 °C with a heating time of 90 min. The ultra-performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometer was used to elucidate the degradation mechanism of gallic acid in the heated sample. The degradation kinetics of gallic acid shows a good fit with the 1st order model with correlation coefficients of R2 ≥ 0.96. The kinetics rate constant (k) were 0.0011, 0.0038 and 0.0076 min-1 at the temperature of 60, 90 and 120 °C, respectively. This finding in this work may serve as a useful guide to minimize the gallic acid degradation and formation of unwanted by-products during processing of L. pumila. University of Nottingham 2019 Conference or Workshop Item PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/26835/1/POCER1914_Elucidation%20of%20Gallic%20Acid%20Degradation.pdf Afiqah, Yeop and Pang, Sook Fun and M. M., Yusoff and Sureena, Abdullah and Jolius, Gimbun (2019) POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique. In: Proceedings of the 5th Postgraduate Colloquium for Environmental Research (POCER 2019) , 8-9 August 2019 , Putrajaya, Malaysia. pp. 36-38., 8. ISBN 978-967-11279-6-4 (Published) https://www.nottingham.edu.my/Conferences/POCER/News-and-Proceedings.aspx |
| spellingShingle | TP Chemical technology Afiqah, Yeop Pang, Sook Fun M. M., Yusoff Sureena, Abdullah Jolius, Gimbun POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique |
| title | POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique |
| title_full | POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique |
| title_fullStr | POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique |
| title_full_unstemmed | POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique |
| title_short | POCER1914: Elucidation of Gallic Acid Degradation Pathway from Labisia Pumila via Mass Spectroscopy Technique |
| title_sort | pocer1914 elucidation of gallic acid degradation pathway from labisia pumila via mass spectroscopy technique |
| topic | TP Chemical technology |
| url | http://umpir.ump.edu.my/id/eprint/26835/1/POCER1914_Elucidation%20of%20Gallic%20Acid%20Degradation.pdf |
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