Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation

Mixed matrix membranes (MMMs) comprising of where polyvinyl chloride (PVC) and graphene oxide (GO) were employed in the membrane fabrication in order to improve the membrane characteristics. In this study of gas separation using mixed matrix membrane, gases such as CO2 and CH4 were used. The objecti...

Full description

Bibliographic Details
Main Authors: K. R., Raj, Sunarti, Abd Rahman
Format: Conference or Workshop Item
Language:English
Published: IOP Publishing Ltd 2019
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/27597/1/11.%20Preliminary%20screening%20study%20using%20ffd%20on%20incorporation.pdf
_version_ 1796993924748804096
author K. R., Raj
Sunarti, Abd Rahman
author_facet K. R., Raj
Sunarti, Abd Rahman
author_sort K. R., Raj
collection UMP
description Mixed matrix membranes (MMMs) comprising of where polyvinyl chloride (PVC) and graphene oxide (GO) were employed in the membrane fabrication in order to improve the membrane characteristics. In this study of gas separation using mixed matrix membrane, gases such as CO2 and CH4 were used. The objectives of this research were to synthesize and develop MMMs PVC/GO, and also to carry out screening to determine best factors condition for membrane to function at high selectivity. The development of MMMs PVC/GO was based on 5 factors. Based on the screening tests, the run which was made up of factors PVC 20%, GO 4%, 1 bar of pressure during gas permeation, NMP solvent, and immersion time of 300s, shows to have the highest selectivity at 26.09 which was above the upper bound lines in the Robeson’s Upper bound plot. Fractional Factorial Design (FFD) was applied to study the minimalization of influenced factors during MMMs preparation. Based on the FFD run, the R-squared (R2 ) was 1.00. Factors that had less impact on the maximum selectivity were the time membrane immersed in water bath (s), and also gas pressure during gas permeation test.
first_indexed 2024-03-06T12:40:28Z
format Conference or Workshop Item
id UMPir27597
institution Universiti Malaysia Pahang
language English
last_indexed 2024-03-06T12:40:28Z
publishDate 2019
publisher IOP Publishing Ltd
record_format dspace
spelling UMPir275972020-04-06T02:58:42Z http://umpir.ump.edu.my/id/eprint/27597/ Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation K. R., Raj Sunarti, Abd Rahman TP Chemical technology Mixed matrix membranes (MMMs) comprising of where polyvinyl chloride (PVC) and graphene oxide (GO) were employed in the membrane fabrication in order to improve the membrane characteristics. In this study of gas separation using mixed matrix membrane, gases such as CO2 and CH4 were used. The objectives of this research were to synthesize and develop MMMs PVC/GO, and also to carry out screening to determine best factors condition for membrane to function at high selectivity. The development of MMMs PVC/GO was based on 5 factors. Based on the screening tests, the run which was made up of factors PVC 20%, GO 4%, 1 bar of pressure during gas permeation, NMP solvent, and immersion time of 300s, shows to have the highest selectivity at 26.09 which was above the upper bound lines in the Robeson’s Upper bound plot. Fractional Factorial Design (FFD) was applied to study the minimalization of influenced factors during MMMs preparation. Based on the FFD run, the R-squared (R2 ) was 1.00. Factors that had less impact on the maximum selectivity were the time membrane immersed in water bath (s), and also gas pressure during gas permeation test. IOP Publishing Ltd 2019 Conference or Workshop Item PeerReviewed pdf en cc_by http://umpir.ump.edu.my/id/eprint/27597/1/11.%20Preliminary%20screening%20study%20using%20ffd%20on%20incorporation.pdf K. R., Raj and Sunarti, Abd Rahman (2019) Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation. In: IOP Conference Series: Materials Science and Engineering, 1st ProSES Symposium 2019 , 4 September 2019 , Kuantan, Pahang, Malaysia. pp. 1-15., 702 (012041). ISSN 1757-899X https://doi.org/10.1088/1757-899X/702/1/012041
spellingShingle TP Chemical technology
K. R., Raj
Sunarti, Abd Rahman
Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation
title Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation
title_full Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation
title_fullStr Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation
title_full_unstemmed Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation
title_short Preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance CO2/CH4 separation
title_sort preliminary screening study using ffd on incorporation of graphene oxide in pvc in mixed matrix membrane to enhance co2 ch4 separation
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/27597/1/11.%20Preliminary%20screening%20study%20using%20ffd%20on%20incorporation.pdf
work_keys_str_mv AT krraj preliminaryscreeningstudyusingffdonincorporationofgrapheneoxideinpvcinmixedmatrixmembranetoenhanceco2ch4separation
AT sunartiabdrahman preliminaryscreeningstudyusingffdonincorporationofgrapheneoxideinpvcinmixedmatrixmembranetoenhanceco2ch4separation