Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy

Wear on Co-Cr-Mo biomedical implants is still a major issue especially for applications in articulation joints like in total ankle, knee and hip arthroplasty. Generation of excessive wear particles can coagulate in body tissues which later cause inflammation, bone loss and necrosis. Modification of...

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Main Authors: S., Izman, M. A., Hassan, Mas Ayu, Hassan, Mohammed Rafiq, Abdul Kadir, Mohammed Ruslan, Abdullah, Mahmood, Anwar, A., Shah, R., Daud
Format: Article
Language:English
Published: Trans Tech Publications, Switzerland 2012
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/28110/1/Effect%20of%20pretreatment%20process%20on%20thermal%20oxidation%20of%20biomedical%20.pdf
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author S., Izman
M. A., Hassan
Mas Ayu, Hassan
Mohammed Rafiq, Abdul Kadir
Mohammed Ruslan, Abdullah
Mahmood, Anwar
A., Shah
R., Daud
author_facet S., Izman
M. A., Hassan
Mas Ayu, Hassan
Mohammed Rafiq, Abdul Kadir
Mohammed Ruslan, Abdullah
Mahmood, Anwar
A., Shah
R., Daud
author_sort S., Izman
collection UMP
description Wear on Co-Cr-Mo biomedical implants is still a major issue especially for applications in articulation joints like in total ankle, knee and hip arthroplasty. Generation of excessive wear particles can coagulate in body tissues which later cause inflammation, bone loss and necrosis. Modification of implant surfaces is a common technique for increasing the hardness and thus minimizing these effects. In this study, thermal oxidation method was carried out on the Co-Cr-Mo to investigate the effects of different pretreatment processes and surface roughness on the hardness of oxide layer formed. Prior to oxidation process, all samples were annealed and pickled to remove residual stress and oxide scales respectively. The oxidation process was done inside furnace under atmospheric condition for 3 hours at 1160 °C. The metallic compositions, surface morphology and hardness of the oxide layer formed on the substrate were verified using X-ray diffraction (XRD), scanning electron microscope and micro-Vickers hardness analysis respectively. It is found that mechanical pretreatment provides oxide/carbide layer with higher hardness than chemical pretreatment method. It is believed that remnants of polishing diamond pastes trapped in roughness valleys react with metal matrix and later transform into carbides during oxidation process. In contrast, initial surface roughness of the substrate has no significant effect on the hardness of oxide/carbide layer.
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spelling UMPir281102020-05-05T07:53:22Z http://umpir.ump.edu.my/id/eprint/28110/ Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy S., Izman M. A., Hassan Mas Ayu, Hassan Mohammed Rafiq, Abdul Kadir Mohammed Ruslan, Abdullah Mahmood, Anwar A., Shah R., Daud T Technology (General) TJ Mechanical engineering and machinery Wear on Co-Cr-Mo biomedical implants is still a major issue especially for applications in articulation joints like in total ankle, knee and hip arthroplasty. Generation of excessive wear particles can coagulate in body tissues which later cause inflammation, bone loss and necrosis. Modification of implant surfaces is a common technique for increasing the hardness and thus minimizing these effects. In this study, thermal oxidation method was carried out on the Co-Cr-Mo to investigate the effects of different pretreatment processes and surface roughness on the hardness of oxide layer formed. Prior to oxidation process, all samples were annealed and pickled to remove residual stress and oxide scales respectively. The oxidation process was done inside furnace under atmospheric condition for 3 hours at 1160 °C. The metallic compositions, surface morphology and hardness of the oxide layer formed on the substrate were verified using X-ray diffraction (XRD), scanning electron microscope and micro-Vickers hardness analysis respectively. It is found that mechanical pretreatment provides oxide/carbide layer with higher hardness than chemical pretreatment method. It is believed that remnants of polishing diamond pastes trapped in roughness valleys react with metal matrix and later transform into carbides during oxidation process. In contrast, initial surface roughness of the substrate has no significant effect on the hardness of oxide/carbide layer. Trans Tech Publications, Switzerland 2012 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/28110/1/Effect%20of%20pretreatment%20process%20on%20thermal%20oxidation%20of%20biomedical%20.pdf S., Izman and M. A., Hassan and Mas Ayu, Hassan and Mohammed Rafiq, Abdul Kadir and Mohammed Ruslan, Abdullah and Mahmood, Anwar and A., Shah and R., Daud (2012) Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy. Advanced Materials Research, 399-401. pp. 1564-1567. ISSN 1022-6680 (print), 1662-8985 (online). (Published) https://doi.org/10.4028/www.scientific.net/AMR.399-401.1564
spellingShingle T Technology (General)
TJ Mechanical engineering and machinery
S., Izman
M. A., Hassan
Mas Ayu, Hassan
Mohammed Rafiq, Abdul Kadir
Mohammed Ruslan, Abdullah
Mahmood, Anwar
A., Shah
R., Daud
Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy
title Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy
title_full Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy
title_fullStr Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy
title_full_unstemmed Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy
title_short Effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy
title_sort effect of pretreatment process on thermal oxidation of biomedical grade cobalt based alloy
topic T Technology (General)
TJ Mechanical engineering and machinery
url http://umpir.ump.edu.my/id/eprint/28110/1/Effect%20of%20pretreatment%20process%20on%20thermal%20oxidation%20of%20biomedical%20.pdf
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