Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers

Interest in the nanotechnology invention has been increased among the researcher and industries which lead to many investigations and studies to develop a product with better performance. In this research, hydroxypropyl methylcellulose (HPMC) and poly (vinyl) alcoh...

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Main Authors: Etdal, Bakhiet, Siti Fazira, Samsudin, Farah Hanani, Zulkifli, Aizi Nor Mazila, Ramli
Format: Article
Published: Trans Tech Publications Ltd, Switzerland 2020
Subjects:
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author Etdal, Bakhiet
Siti Fazira, Samsudin
Farah Hanani, Zulkifli
Aizi Nor Mazila, Ramli
author_facet Etdal, Bakhiet
Siti Fazira, Samsudin
Farah Hanani, Zulkifli
Aizi Nor Mazila, Ramli
author_sort Etdal, Bakhiet
collection UMP
description Interest in the nanotechnology invention has been increased among the researcher and industries which lead to many investigations and studies to develop a product with better performance. In this research, hydroxypropyl methylcellulose (HPMC) and poly (vinyl) alcohol (PVA) nanofiber with the ratio 1:1 and the concentration of 5 wt% and 7 wt%, respectively, were successfully fabricated by using electrospinning technique. The HPMC/ PVA was then blended with the different concentration of cellulose nanocrystal (CNC) at 2 wt%, 4 wt%, 6 wt% and 8 wt%. The SEM results of HPMC/PVA/CNC nanofibers shown random orientation fibers with average diameters of 62.28 nm - 252.80 nm. The TGA results showed three major weight loss that prove the decomposotion of HPMC/PVA/CNC was occured with three maximum temperature peaks around 69 ̊C, 290 ̊C and 392 ̊C. As for DSC, the peak intensity of the Tg in the electrospun nanofiber are decreasing as the concentration of CNCs increased might be due to the interfering of the CNC with the crystallization of the polymer causing mobility of the amorphous regions to be higher. Therefore, the study on the thermal properties of HPMC/PVA incorporated with CNCs nanofibers could be a reference for various potential applications.
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spelling UMPir290962020-09-03T07:19:59Z http://umpir.ump.edu.my/id/eprint/29096/ Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers Etdal, Bakhiet Siti Fazira, Samsudin Farah Hanani, Zulkifli Aizi Nor Mazila, Ramli Q Science (General) Interest in the nanotechnology invention has been increased among the researcher and industries which lead to many investigations and studies to develop a product with better performance. In this research, hydroxypropyl methylcellulose (HPMC) and poly (vinyl) alcohol (PVA) nanofiber with the ratio 1:1 and the concentration of 5 wt% and 7 wt%, respectively, were successfully fabricated by using electrospinning technique. The HPMC/ PVA was then blended with the different concentration of cellulose nanocrystal (CNC) at 2 wt%, 4 wt%, 6 wt% and 8 wt%. The SEM results of HPMC/PVA/CNC nanofibers shown random orientation fibers with average diameters of 62.28 nm - 252.80 nm. The TGA results showed three major weight loss that prove the decomposotion of HPMC/PVA/CNC was occured with three maximum temperature peaks around 69 ̊C, 290 ̊C and 392 ̊C. As for DSC, the peak intensity of the Tg in the electrospun nanofiber are decreasing as the concentration of CNCs increased might be due to the interfering of the CNC with the crystallization of the polymer causing mobility of the amorphous regions to be higher. Therefore, the study on the thermal properties of HPMC/PVA incorporated with CNCs nanofibers could be a reference for various potential applications. Trans Tech Publications Ltd, Switzerland 2020-03-12 Article PeerReviewed Etdal, Bakhiet and Siti Fazira, Samsudin and Farah Hanani, Zulkifli and Aizi Nor Mazila, Ramli (2020) Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers. Materials Science Forum, 981. pp. 115-120. ISSN 1662-9752. (Published) https://doi.org/10.4028/www.scientific.net/MSF.981.115 https://doi.org/10.4028/www.scientific.net/MSF.981.115
spellingShingle Q Science (General)
Etdal, Bakhiet
Siti Fazira, Samsudin
Farah Hanani, Zulkifli
Aizi Nor Mazila, Ramli
Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers
title Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers
title_full Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers
title_fullStr Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers
title_full_unstemmed Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers
title_short Thermal Characterizations of HPMC/PVA Impregnated with CNC Electrospun Nanofibers
title_sort thermal characterizations of hpmc pva impregnated with cnc electrospun nanofibers
topic Q Science (General)
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AT sitifazirasamsudin thermalcharacterizationsofhpmcpvaimpregnatedwithcncelectrospunnanofibers
AT farahhananizulkifli thermalcharacterizationsofhpmcpvaimpregnatedwithcncelectrospunnanofibers
AT aizinormazilaramli thermalcharacterizationsofhpmcpvaimpregnatedwithcncelectrospunnanofibers