Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method
Calcium hydroxyphosphate (hydroxyapatite) is a calcium phosphate that is widely used in biomedical application. Hydroxyapatite is an excellent component for bone substitutes for their chemical and structural similarity to natural bone component. In this research, hydroxyapatite was synthesized from...
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| Format: | Conference or Workshop Item |
| Language: | English |
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Trans Tech Publications
2020
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| Online Access: | http://umpir.ump.edu.my/id/eprint/32354/1/Preparation%20and%20characterization%20of%20calcium%20hydroxyphosphate%20.pdf |
| _version_ | 1796994782494457856 |
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| author | Nor Hakimin, Abdullah An'amt, Mohamed Noor Mohd Sukhairi, Mat Rasat Sarizam, Mamat Mazlan, Mohamed Norshahidatul Akmar, Mohd Shohaimi Zamani, A. H. Nurasmat, Mohd Shukri Mohammad Khairul Azhar, Abdul Razab Mohamad Faiz, Mohd Amin |
| author_facet | Nor Hakimin, Abdullah An'amt, Mohamed Noor Mohd Sukhairi, Mat Rasat Sarizam, Mamat Mazlan, Mohamed Norshahidatul Akmar, Mohd Shohaimi Zamani, A. H. Nurasmat, Mohd Shukri Mohammad Khairul Azhar, Abdul Razab Mohamad Faiz, Mohd Amin |
| author_sort | Nor Hakimin, Abdullah |
| collection | UMP |
| description | Calcium hydroxyphosphate (hydroxyapatite) is a calcium phosphate that is widely used in biomedical application. Hydroxyapatite is an excellent component for bone substitutes for their chemical and structural similarity to natural bone component. In this research, hydroxyapatite was synthesized from tilapia fish bones and scales using calcination method with 3 different temperatures namely 1000 °C, 900 °C and 800 °C. The obtained hydroxyapatite powder was characterized using several techniques such as Fourier-Transform infrared spectroscopy Attenuated total reflection (FTIR-ATR), scanning electron microscope (SEM), proximate analysis and X-ray diffraction (XRD). The results indicated that temperature 1000 °C has the highest weight loss with 21.825 g compared to the temperature 800 °C and 900 °C. From FTIR-ATR analysis, the presence of characteristic peaks for hydroxyl group, phosphate groups and water molecule indicated that the powder were hydroxyapatite. SEM results showed that increasing temperature had led to more dense structure. The hydroxyapatite powder were further analysed for their proximate analysis. The results proved that the highest contents of ash, fat, moisture and crude protein were observed at 1000 °C as compared to 900 °C and 800 °C. Based on this study, it revealed that produced pure hydroxyapatite from natural resources could be a potential candidate for food industry as protein enhancer. |
| first_indexed | 2024-03-06T12:52:43Z |
| format | Conference or Workshop Item |
| id | UMPir32354 |
| institution | Universiti Malaysia Pahang |
| language | English |
| last_indexed | 2024-03-06T12:52:43Z |
| publishDate | 2020 |
| publisher | Trans Tech Publications |
| record_format | dspace |
| spelling | UMPir323542021-11-10T03:23:25Z http://umpir.ump.edu.my/id/eprint/32354/ Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method Nor Hakimin, Abdullah An'amt, Mohamed Noor Mohd Sukhairi, Mat Rasat Sarizam, Mamat Mazlan, Mohamed Norshahidatul Akmar, Mohd Shohaimi Zamani, A. H. Nurasmat, Mohd Shukri Mohammad Khairul Azhar, Abdul Razab Mohamad Faiz, Mohd Amin TP Chemical technology Calcium hydroxyphosphate (hydroxyapatite) is a calcium phosphate that is widely used in biomedical application. Hydroxyapatite is an excellent component for bone substitutes for their chemical and structural similarity to natural bone component. In this research, hydroxyapatite was synthesized from tilapia fish bones and scales using calcination method with 3 different temperatures namely 1000 °C, 900 °C and 800 °C. The obtained hydroxyapatite powder was characterized using several techniques such as Fourier-Transform infrared spectroscopy Attenuated total reflection (FTIR-ATR), scanning electron microscope (SEM), proximate analysis and X-ray diffraction (XRD). The results indicated that temperature 1000 °C has the highest weight loss with 21.825 g compared to the temperature 800 °C and 900 °C. From FTIR-ATR analysis, the presence of characteristic peaks for hydroxyl group, phosphate groups and water molecule indicated that the powder were hydroxyapatite. SEM results showed that increasing temperature had led to more dense structure. The hydroxyapatite powder were further analysed for their proximate analysis. The results proved that the highest contents of ash, fat, moisture and crude protein were observed at 1000 °C as compared to 900 °C and 800 °C. Based on this study, it revealed that produced pure hydroxyapatite from natural resources could be a potential candidate for food industry as protein enhancer. Trans Tech Publications 2020 Conference or Workshop Item PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/32354/1/Preparation%20and%20characterization%20of%20calcium%20hydroxyphosphate%20.pdf Nor Hakimin, Abdullah and An'amt, Mohamed Noor and Mohd Sukhairi, Mat Rasat and Sarizam, Mamat and Mazlan, Mohamed and Norshahidatul Akmar, Mohd Shohaimi and Zamani, A. H. and Nurasmat, Mohd Shukri and Mohammad Khairul Azhar, Abdul Razab and Mohamad Faiz, Mohd Amin (2020) Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method. In: Materials Science Forum: 3rd International Conference on Advanced Materials Characterization Techniques (AMCT 2019) , 23-24 July 2019 , Kangar. 596 -601., 1010. ISSN 0255-5476 ISBN 9783035715828 https://doi.org/10.4028/www.scientific.net/MSF.1010.596 |
| spellingShingle | TP Chemical technology Nor Hakimin, Abdullah An'amt, Mohamed Noor Mohd Sukhairi, Mat Rasat Sarizam, Mamat Mazlan, Mohamed Norshahidatul Akmar, Mohd Shohaimi Zamani, A. H. Nurasmat, Mohd Shukri Mohammad Khairul Azhar, Abdul Razab Mohamad Faiz, Mohd Amin Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method |
| title | Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method |
| title_full | Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method |
| title_fullStr | Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method |
| title_full_unstemmed | Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method |
| title_short | Preparation and characterization of calcium hydroxyphosphate (hydroxyapatite) from tilapia fish bones and scales via calcination method |
| title_sort | preparation and characterization of calcium hydroxyphosphate hydroxyapatite from tilapia fish bones and scales via calcination method |
| topic | TP Chemical technology |
| url | http://umpir.ump.edu.my/id/eprint/32354/1/Preparation%20and%20characterization%20of%20calcium%20hydroxyphosphate%20.pdf |
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