Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers

Acetosolv technique is considered as one of the best alternative ways to extract technical lignin from biomass as it has high efficiency and environmentally friendly. In this study, microwave assisted acetosolv technique was used to extract lignin from oil palm empty fruit bunch (OPEFB) in the prese...

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Main Authors: Muhammad Nor Arifin, Yaakob, Rasidi, Roslan, Nurjannah, Salim, Siti Noor Hidayah, Mustapha, Sarani, Zakaria, Chin-Hua, Chia, Mohd Shaiful, Sajab, Nai Yuh, Peter Yek
Format: Article
Language:English
Published: Trans Tech Publications Ltd, Switzerland 2020
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/32579/1/Effect%20of%20Temperature%20on%20the%20Yield%20of%20Lignin%20Extracted%20Using%20Microwave-Assisted%20Acetosolv%20from%20Empty%20Fruit%20Bunch%20Fibers.pdf
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author Muhammad Nor Arifin, Yaakob
Rasidi, Roslan
Nurjannah, Salim
Siti Noor Hidayah, Mustapha
Sarani, Zakaria
Chin-Hua, Chia
Mohd Shaiful, Sajab
Nai Yuh, Peter Yek
author_facet Muhammad Nor Arifin, Yaakob
Rasidi, Roslan
Nurjannah, Salim
Siti Noor Hidayah, Mustapha
Sarani, Zakaria
Chin-Hua, Chia
Mohd Shaiful, Sajab
Nai Yuh, Peter Yek
author_sort Muhammad Nor Arifin, Yaakob
collection UMP
description Acetosolv technique is considered as one of the best alternative ways to extract technical lignin from biomass as it has high efficiency and environmentally friendly. In this study, microwave assisted acetosolv technique was used to extract lignin from oil palm empty fruit bunch (OPEFB) in the presence of 3% sulfuric acid catalyst reacted at various temperature. The yield of the extracted acetosolv lignin was calculated using the modified Technical Association of the Pulp and Paper Industry biomass composition analysis (TAPPI) method. The result showed that, as the temperature increased from 90 to 110 °C, the yield of lignin extracted also increase from 43.07 to 76.98%. The presence of guaiacyl and p-coumarate indicates the presence of active sites at C-3 and C-5 of the aromatic ring for polymerization reactions. Scanning Electron Microscopy images showed that removal of lignin is intensified as the microwave-assisted acetosolv temperature increased.
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spelling UMPir325792021-11-10T08:46:39Z http://umpir.ump.edu.my/id/eprint/32579/ Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers Muhammad Nor Arifin, Yaakob Rasidi, Roslan Nurjannah, Salim Siti Noor Hidayah, Mustapha Sarani, Zakaria Chin-Hua, Chia Mohd Shaiful, Sajab Nai Yuh, Peter Yek HD Industries. Land use. Labor SB Plant culture TP Chemical technology Acetosolv technique is considered as one of the best alternative ways to extract technical lignin from biomass as it has high efficiency and environmentally friendly. In this study, microwave assisted acetosolv technique was used to extract lignin from oil palm empty fruit bunch (OPEFB) in the presence of 3% sulfuric acid catalyst reacted at various temperature. The yield of the extracted acetosolv lignin was calculated using the modified Technical Association of the Pulp and Paper Industry biomass composition analysis (TAPPI) method. The result showed that, as the temperature increased from 90 to 110 °C, the yield of lignin extracted also increase from 43.07 to 76.98%. The presence of guaiacyl and p-coumarate indicates the presence of active sites at C-3 and C-5 of the aromatic ring for polymerization reactions. Scanning Electron Microscopy images showed that removal of lignin is intensified as the microwave-assisted acetosolv temperature increased. Trans Tech Publications Ltd, Switzerland 2020-03-12 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/32579/1/Effect%20of%20Temperature%20on%20the%20Yield%20of%20Lignin%20Extracted%20Using%20Microwave-Assisted%20Acetosolv%20from%20Empty%20Fruit%20Bunch%20Fibers.pdf Muhammad Nor Arifin, Yaakob and Rasidi, Roslan and Nurjannah, Salim and Siti Noor Hidayah, Mustapha and Sarani, Zakaria and Chin-Hua, Chia and Mohd Shaiful, Sajab and Nai Yuh, Peter Yek (2020) Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers. Materials Science Forum, 981. pp. 240-244. ISSN 1662-9752. (Published) https://www.scientific.net/MSF.981.240 https://doi.org/10.4028/www.scientific.net/MSF.981.240
spellingShingle HD Industries. Land use. Labor
SB Plant culture
TP Chemical technology
Muhammad Nor Arifin, Yaakob
Rasidi, Roslan
Nurjannah, Salim
Siti Noor Hidayah, Mustapha
Sarani, Zakaria
Chin-Hua, Chia
Mohd Shaiful, Sajab
Nai Yuh, Peter Yek
Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers
title Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers
title_full Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers
title_fullStr Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers
title_full_unstemmed Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers
title_short Effect of temperature on the yield of lignin extracted using microwave-sssisted acetosolv from empty fruit bunch fibers
title_sort effect of temperature on the yield of lignin extracted using microwave sssisted acetosolv from empty fruit bunch fibers
topic HD Industries. Land use. Labor
SB Plant culture
TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/32579/1/Effect%20of%20Temperature%20on%20the%20Yield%20of%20Lignin%20Extracted%20Using%20Microwave-Assisted%20Acetosolv%20from%20Empty%20Fruit%20Bunch%20Fibers.pdf
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