Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production

Present work proposes on the synthesis of nano calcium oxide derived from waste cockle shell (Anadara granosa) and applied as heterogenous catalyst in biodiesel production via transesterification reaction under reaction parameter 15:1 methanol to oil ratio, 5 wt.% catalyst and 3 hour reation time an...

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Main Authors: Muhammad Nor Fazli, Abd Malek, Livitra, Pushparaja, Noraini, Mat Hussin, Nurul Hajar, Embong, Bhuyar, Prakash, Mohd Hasbi, Ab. Rahim, Maniam, Gaanty Pragas
Format: Article
Language:English
Published: Slovak University of Agriculture 2021
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/32773/1/Exploration%20of%20efficiency%20of%20nano%20calcium%20oxide%20%28cao%29%20as%20catalyst%20for%20enhancement%20of%20biodiesel%20production.pdf
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author Muhammad Nor Fazli, Abd Malek
Livitra, Pushparaja
Noraini, Mat Hussin
Nurul Hajar, Embong
Bhuyar, Prakash
Mohd Hasbi, Ab. Rahim
Maniam, Gaanty Pragas
author_facet Muhammad Nor Fazli, Abd Malek
Livitra, Pushparaja
Noraini, Mat Hussin
Nurul Hajar, Embong
Bhuyar, Prakash
Mohd Hasbi, Ab. Rahim
Maniam, Gaanty Pragas
author_sort Muhammad Nor Fazli, Abd Malek
collection UMP
description Present work proposes on the synthesis of nano calcium oxide derived from waste cockle shell (Anadara granosa) and applied as heterogenous catalyst in biodiesel production via transesterification reaction under reaction parameter 15:1 methanol to oil ratio, 5 wt.% catalyst and 3 hour reation time and constant temperature at 65 ± 2 °C. The waste cockle shell was prepared in nano size via ball mill technique which was run for 36 hours at 350 rpm speed and then calcined at 900 °C for 2 hours to decompose calcium carbonate, CaCOî into nano calcium oxide, n-CaO. The catalyst was characterized by particle size analyzer, Transmission Electron Microscopy, Field Emission Scanning Electron Microscope, Surface Area Analyser, X-Ray Diffractometer, Fourier transform infrared, Hammet indicator and benzoic acid titration. Particle size of n-CaO catalyst was found within the range of 29 nm to 67.5 nm. Specific surface area of synthesised n-CaO is 8.41 m2/g with basicity strength of 0.055 mmol/g. Methyl ester conversion of palm oil with n-CaO as a catalyst was 88.87 wt.%.
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spelling UMPir327732022-03-08T07:06:20Z http://umpir.ump.edu.my/id/eprint/32773/ Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production Muhammad Nor Fazli, Abd Malek Livitra, Pushparaja Noraini, Mat Hussin Nurul Hajar, Embong Bhuyar, Prakash Mohd Hasbi, Ab. Rahim Maniam, Gaanty Pragas T Technology (General) TP Chemical technology Present work proposes on the synthesis of nano calcium oxide derived from waste cockle shell (Anadara granosa) and applied as heterogenous catalyst in biodiesel production via transesterification reaction under reaction parameter 15:1 methanol to oil ratio, 5 wt.% catalyst and 3 hour reation time and constant temperature at 65 ± 2 °C. The waste cockle shell was prepared in nano size via ball mill technique which was run for 36 hours at 350 rpm speed and then calcined at 900 °C for 2 hours to decompose calcium carbonate, CaCOî into nano calcium oxide, n-CaO. The catalyst was characterized by particle size analyzer, Transmission Electron Microscopy, Field Emission Scanning Electron Microscope, Surface Area Analyser, X-Ray Diffractometer, Fourier transform infrared, Hammet indicator and benzoic acid titration. Particle size of n-CaO catalyst was found within the range of 29 nm to 67.5 nm. Specific surface area of synthesised n-CaO is 8.41 m2/g with basicity strength of 0.055 mmol/g. Methyl ester conversion of palm oil with n-CaO as a catalyst was 88.87 wt.%. Slovak University of Agriculture 2021-08-01 Article PeerReviewed pdf en cc_by_nd_4 http://umpir.ump.edu.my/id/eprint/32773/1/Exploration%20of%20efficiency%20of%20nano%20calcium%20oxide%20%28cao%29%20as%20catalyst%20for%20enhancement%20of%20biodiesel%20production.pdf Muhammad Nor Fazli, Abd Malek and Livitra, Pushparaja and Noraini, Mat Hussin and Nurul Hajar, Embong and Bhuyar, Prakash and Mohd Hasbi, Ab. Rahim and Maniam, Gaanty Pragas (2021) Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production. Journal of Microbiology, Biotechnology and Food Sciences, 11 (1). pp. 1-4. ISSN 1338-5178. (Published) https://doi.org/10.15414/jmbfs.3935 https://doi.org/10.15414/jmbfs.3935
spellingShingle T Technology (General)
TP Chemical technology
Muhammad Nor Fazli, Abd Malek
Livitra, Pushparaja
Noraini, Mat Hussin
Nurul Hajar, Embong
Bhuyar, Prakash
Mohd Hasbi, Ab. Rahim
Maniam, Gaanty Pragas
Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production
title Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production
title_full Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production
title_fullStr Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production
title_full_unstemmed Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production
title_short Exploration of efficiency of nano calcium oxide (CaO) as catalyst for enhancement of biodiesel production
title_sort exploration of efficiency of nano calcium oxide cao as catalyst for enhancement of biodiesel production
topic T Technology (General)
TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/32773/1/Exploration%20of%20efficiency%20of%20nano%20calcium%20oxide%20%28cao%29%20as%20catalyst%20for%20enhancement%20of%20biodiesel%20production.pdf
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