Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods

Microwave-assisted hydrodistillation (MAHD) is a promising and advanced technology that uses microwave heating to extract essential oils from dry leaves. Currently available conventional methods are time consuming, thermally unsafe and require costly solvents. In the current study, MAHD and traditio...

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Main Authors: Azhari, Hamid Nour, Sundarajan, Siva
Format: Conference or Workshop Item
Language:English
Published: IOP Publishing Ltd 2019
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/35882/1/Characterization%20of%20bioactive%20compounds%20extracted%20from%20patchouli_Comparing%20microwave-assisted%20hydrodistillation.pdf
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author Azhari, Hamid Nour
Sundarajan, Siva
author_facet Azhari, Hamid Nour
Sundarajan, Siva
author_sort Azhari, Hamid Nour
collection UMP
description Microwave-assisted hydrodistillation (MAHD) is a promising and advanced technology that uses microwave heating to extract essential oils from dry leaves. Currently available conventional methods are time consuming, thermally unsafe and require costly solvents. In the current study, MAHD and traditional hydrodistillation (HD) techniques were compared and their effectiveness in the separation of the essential oil from dry patchouli leaves have been studied. The patchouli oil that obtained from MAHD and HD extraction methods were characterized using gas chromatography-mass spectrometry (GC-MS) analysis and the impact of the two extraction methods on the plant morphology were observed using scanning electron microscopy (SEM) analysis. The results indicated that MAHD method extracted 5 % of essential oil at solid to solvent ratio of 1:12 g/ml from patchouli leaves as compared to 4 % obtained using HD method at 45 minutes of extraction time. In addition, MAHD method can retain 16 compounds while only 11 chemical compounds were extracted using HD. Thus, MAHD showed a greater potential for better production of the essential oil from patchouli leaves as compared to HD method.
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spelling UMPir358822023-05-24T04:19:48Z http://umpir.ump.edu.my/id/eprint/35882/ Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods Azhari, Hamid Nour Sundarajan, Siva HD Industries. Land use. Labor Q Science (General) TP Chemical technology Microwave-assisted hydrodistillation (MAHD) is a promising and advanced technology that uses microwave heating to extract essential oils from dry leaves. Currently available conventional methods are time consuming, thermally unsafe and require costly solvents. In the current study, MAHD and traditional hydrodistillation (HD) techniques were compared and their effectiveness in the separation of the essential oil from dry patchouli leaves have been studied. The patchouli oil that obtained from MAHD and HD extraction methods were characterized using gas chromatography-mass spectrometry (GC-MS) analysis and the impact of the two extraction methods on the plant morphology were observed using scanning electron microscopy (SEM) analysis. The results indicated that MAHD method extracted 5 % of essential oil at solid to solvent ratio of 1:12 g/ml from patchouli leaves as compared to 4 % obtained using HD method at 45 minutes of extraction time. In addition, MAHD method can retain 16 compounds while only 11 chemical compounds were extracted using HD. Thus, MAHD showed a greater potential for better production of the essential oil from patchouli leaves as compared to HD method. IOP Publishing Ltd 2019-12-09 Conference or Workshop Item PeerReviewed pdf en cc_by http://umpir.ump.edu.my/id/eprint/35882/1/Characterization%20of%20bioactive%20compounds%20extracted%20from%20patchouli_Comparing%20microwave-assisted%20hydrodistillation.pdf Azhari, Hamid Nour and Sundarajan, Siva (2019) Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods. In: IOP Conference Series: Materials Science and Engineering; 1st Process Systems Engineering and Safety Symposium 2019, ProSES 2019 , 4 September 2019 , Kuantan, Pahang, Malaysia. pp. 1-11., 702 (012042). ISSN 1757-8981 (Published) https://doi.org/10.1088/1757-899X/702/1/012042
spellingShingle HD Industries. Land use. Labor
Q Science (General)
TP Chemical technology
Azhari, Hamid Nour
Sundarajan, Siva
Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods
title Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods
title_full Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods
title_fullStr Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods
title_full_unstemmed Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods
title_short Characterization of bioactive compounds extracted from patchouli : Comparing microwave-assisted hydrodistillation and hydrodistillation methods
title_sort characterization of bioactive compounds extracted from patchouli comparing microwave assisted hydrodistillation and hydrodistillation methods
topic HD Industries. Land use. Labor
Q Science (General)
TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/35882/1/Characterization%20of%20bioactive%20compounds%20extracted%20from%20patchouli_Comparing%20microwave-assisted%20hydrodistillation.pdf
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AT sundarajansiva characterizationofbioactivecompoundsextractedfrompatchoulicomparingmicrowaveassistedhydrodistillationandhydrodistillationmethods