The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic
Lead zirconate titanate Pb(Zr0.52Ti0.48)O3, (PZT) from mixture of commercial PbO, TiO2 and ZrO2 powders were successfully prepared using planetary ball mill. The microstructure and electrical properties of PZT ceramic were found to be more sensitive to the sintering condition. The infl...
| Main Authors: | , , , , , , |
|---|---|
| Format: | Article |
| Language: | English English |
| Published: |
Faculty Mechanical Engineering, UMP
2014
|
| Subjects: | |
| Online Access: | http://umpir.ump.edu.my/id/eprint/3995/1/P267.pdf http://umpir.ump.edu.my/id/eprint/3995/4/fkp-2014-wanazhar-effect%20of%20sintering.pdf |
| _version_ | 1825821461773811712 |
|---|---|
| author | Wan Azhar, Wan Yusoff Nur Shafiza Afzan, Sharif Julie J., Mohamed Hutagalung, Sabar Derita Zainal Arifin, Ahmad Mohd Zulkifly, Abdullah Hasmaliza, Mohamad |
| author_facet | Wan Azhar, Wan Yusoff Nur Shafiza Afzan, Sharif Julie J., Mohamed Hutagalung, Sabar Derita Zainal Arifin, Ahmad Mohd Zulkifly, Abdullah Hasmaliza, Mohamad |
| author_sort | Wan Azhar, Wan Yusoff |
| collection | UMP |
| description | Lead zirconate titanate Pb(Zr0.52Ti0.48)O3, (PZT) from mixture of commercial PbO, TiO2 and ZrO2 powders were successfully prepared using planetary ball mill. The microstructure and electrical properties of PZT ceramic were found to be more sensitive to the sintering condition. The influence of microstructure and electrical properties towards sintering condition of the samples were studied. SEM analysis indicated that shorter sintering time with higher sintering temperature promotes fine structure and densification. This have been proves where relative density of the obtained sintered PZT ceramics was measured to be approximately 99 % of the theoretical density. The electrical properties of the ceramic sintered at higher temperature with different sintering time were measured at high frequencies. The result revealed that different sintering conditions give big impact to the electrical behavior in a broad frequency region. |
| first_indexed | 2024-03-06T11:41:53Z |
| format | Article |
| id | UMPir3995 |
| institution | Universiti Malaysia Pahang |
| language | English English |
| last_indexed | 2024-03-06T11:41:53Z |
| publishDate | 2014 |
| publisher | Faculty Mechanical Engineering, UMP |
| record_format | dspace |
| spelling | UMPir39952018-07-25T04:23:11Z http://umpir.ump.edu.my/id/eprint/3995/ The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic Wan Azhar, Wan Yusoff Nur Shafiza Afzan, Sharif Julie J., Mohamed Hutagalung, Sabar Derita Zainal Arifin, Ahmad Mohd Zulkifly, Abdullah Hasmaliza, Mohamad TJ Mechanical engineering and machinery Lead zirconate titanate Pb(Zr0.52Ti0.48)O3, (PZT) from mixture of commercial PbO, TiO2 and ZrO2 powders were successfully prepared using planetary ball mill. The microstructure and electrical properties of PZT ceramic were found to be more sensitive to the sintering condition. The influence of microstructure and electrical properties towards sintering condition of the samples were studied. SEM analysis indicated that shorter sintering time with higher sintering temperature promotes fine structure and densification. This have been proves where relative density of the obtained sintered PZT ceramics was measured to be approximately 99 % of the theoretical density. The electrical properties of the ceramic sintered at higher temperature with different sintering time were measured at high frequencies. The result revealed that different sintering conditions give big impact to the electrical behavior in a broad frequency region. Faculty Mechanical Engineering, UMP 2014-07-01 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/3995/1/P267.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/3995/4/fkp-2014-wanazhar-effect%20of%20sintering.pdf Wan Azhar, Wan Yusoff and Nur Shafiza Afzan, Sharif and Julie J., Mohamed and Hutagalung, Sabar Derita and Zainal Arifin, Ahmad and Mohd Zulkifly, Abdullah and Hasmaliza, Mohamad (2014) The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic. Journal of Mechanical Engineering and Sciences (JMES) , 6. pp. 901-906. ISSN 2289-4659 (print); 2231-8380 (online). (Published) http://dx.doi.org/10.15282/jmes.6.2014.16.0086 DOI: 10.15282/jmes.6.2014.16.0086 |
| spellingShingle | TJ Mechanical engineering and machinery Wan Azhar, Wan Yusoff Nur Shafiza Afzan, Sharif Julie J., Mohamed Hutagalung, Sabar Derita Zainal Arifin, Ahmad Mohd Zulkifly, Abdullah Hasmaliza, Mohamad The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic |
| title | The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic |
| title_full | The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic |
| title_fullStr | The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic |
| title_full_unstemmed | The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic |
| title_short | The Effect of Sintering Conditions on the Microstructure and Electrical Properties of Pb(Zr0.52Ti0.48)O3 Ceramic |
| title_sort | effect of sintering conditions on the microstructure and electrical properties of pb zr0 52ti0 48 o3 ceramic |
| topic | TJ Mechanical engineering and machinery |
| url | http://umpir.ump.edu.my/id/eprint/3995/1/P267.pdf http://umpir.ump.edu.my/id/eprint/3995/4/fkp-2014-wanazhar-effect%20of%20sintering.pdf |
| work_keys_str_mv | AT wanazharwanyusoff theeffectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT nurshafizaafzansharif theeffectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT juliejmohamed theeffectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT hutagalungsabarderita theeffectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT zainalarifinahmad theeffectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT mohdzulkiflyabdullah theeffectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT hasmalizamohamad theeffectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT wanazharwanyusoff effectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT nurshafizaafzansharif effectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT juliejmohamed effectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT hutagalungsabarderita effectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT zainalarifinahmad effectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT mohdzulkiflyabdullah effectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic AT hasmalizamohamad effectofsinteringconditionsonthemicrostructureandelectricalpropertiesofpbzr052ti048o3ceramic |