The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane

Supported liquid membrane (SLM) is an effective method to separate a high-demand levulinic acid (LA) from an aqueous or biomass hydrolysate solution. Several factors can influence the separation of LA using SLM. In this study, three hollow fiber (HF) SLM (HFSLM) operation parameters, such as carrier...

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Main Authors: Vikneswary, Rajendaren, Syed Mohd Saufi, Tuan Chik, Mior Ahmad Khushairi, Mohd Zahari
Format: Article
Language:English
English
Published: Elsevier B.V. 2024
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/41648/1/The%20use%20of%20factorial%20design%20for%20levulinic%20acid%20extraction%20via%20hollow%20fiber_ABST.pdf
http://umpir.ump.edu.my/id/eprint/41648/2/The%20use%20of%20factorial%20design%20for%20levulinic%20acid%20extraction%20via%20hollow%20fiber.pdf
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author Vikneswary, Rajendaren
Syed Mohd Saufi, Tuan Chik
Mior Ahmad Khushairi, Mohd Zahari
author_facet Vikneswary, Rajendaren
Syed Mohd Saufi, Tuan Chik
Mior Ahmad Khushairi, Mohd Zahari
author_sort Vikneswary, Rajendaren
collection UMP
description Supported liquid membrane (SLM) is an effective method to separate a high-demand levulinic acid (LA) from an aqueous or biomass hydrolysate solution. Several factors can influence the separation of LA using SLM. In this study, three hollow fiber (HF) SLM (HFSLM) operation parameters, such as carrier concentration (0.1–0.5 M tri-n-octylamine, (TOA), stripping concentration (0.25–0.75 M sodium hydroxide (NaOH), and feed concentration (10–30 g/L LA) was analyzed by using a 23 full factorial design (FFD). The results showed that all three factors significantly impact the extraction of LA. The order of contribution effects towards LA extraction was LA feed concentration > NaOH stripping concentration > TOA carrier concentration. The design proposed a valid condition of factors such as 0.5 M TOA, 0.75 M NaOH, and 10 g/L of LA with LA extraction of 69.6 ± 2.16 %. The result proved that FFD effectively improved the LA extraction in the HFSLM process by considering all the factors involved.
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spelling UMPir416482024-06-24T01:31:15Z http://umpir.ump.edu.my/id/eprint/41648/ The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane Vikneswary, Rajendaren Syed Mohd Saufi, Tuan Chik Mior Ahmad Khushairi, Mohd Zahari TP Chemical technology Supported liquid membrane (SLM) is an effective method to separate a high-demand levulinic acid (LA) from an aqueous or biomass hydrolysate solution. Several factors can influence the separation of LA using SLM. In this study, three hollow fiber (HF) SLM (HFSLM) operation parameters, such as carrier concentration (0.1–0.5 M tri-n-octylamine, (TOA), stripping concentration (0.25–0.75 M sodium hydroxide (NaOH), and feed concentration (10–30 g/L LA) was analyzed by using a 23 full factorial design (FFD). The results showed that all three factors significantly impact the extraction of LA. The order of contribution effects towards LA extraction was LA feed concentration > NaOH stripping concentration > TOA carrier concentration. The design proposed a valid condition of factors such as 0.5 M TOA, 0.75 M NaOH, and 10 g/L of LA with LA extraction of 69.6 ± 2.16 %. The result proved that FFD effectively improved the LA extraction in the HFSLM process by considering all the factors involved. Elsevier B.V. 2024-02 Article PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/41648/1/The%20use%20of%20factorial%20design%20for%20levulinic%20acid%20extraction%20via%20hollow%20fiber_ABST.pdf pdf en http://umpir.ump.edu.my/id/eprint/41648/2/The%20use%20of%20factorial%20design%20for%20levulinic%20acid%20extraction%20via%20hollow%20fiber.pdf Vikneswary, Rajendaren and Syed Mohd Saufi, Tuan Chik and Mior Ahmad Khushairi, Mohd Zahari (2024) The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane. Journal of the Indian Chemical Society, 101 (2). pp. 1-6. ISSN 0019-4522. (Published) https://doi.org/10.1016/j.jics.2024.101122 https://doi.org/10.1016/j.jics.2024.101122
spellingShingle TP Chemical technology
Vikneswary, Rajendaren
Syed Mohd Saufi, Tuan Chik
Mior Ahmad Khushairi, Mohd Zahari
The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane
title The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane
title_full The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane
title_fullStr The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane
title_full_unstemmed The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane
title_short The use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane
title_sort use of factorial design for levulinic acid extraction via hollow fiber supported liquid membrane
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/41648/1/The%20use%20of%20factorial%20design%20for%20levulinic%20acid%20extraction%20via%20hollow%20fiber_ABST.pdf
http://umpir.ump.edu.my/id/eprint/41648/2/The%20use%20of%20factorial%20design%20for%20levulinic%20acid%20extraction%20via%20hollow%20fiber.pdf
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