Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil
Agarwood (Aquilaria malaccensis) is very well known as the most expensive wood in the world due to its wide applications in perfumery, cosmetic traditional medicine, and religious ceremonies. The study aimed to give an in-depth characterisation focusing on marker compounds in A. malaccensis from dif...
Main Authors: | , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Elsevier B.V.
2023
|
Subjects: | |
Online Access: | http://umpir.ump.edu.my/id/eprint/41652/1/Gas%20chromatography%20mass%20spectrometry%20couple%20with%20quadrupole%20time-of-flight.pdf |
_version_ | 1825815730169315328 |
---|---|
author | Erny Haslina, Abd Latib Huq, A. K. M. Moyeenul Zareen, Seema Saiful Nizam, Tajuddin |
author_facet | Erny Haslina, Abd Latib Huq, A. K. M. Moyeenul Zareen, Seema Saiful Nizam, Tajuddin |
author_sort | Erny Haslina, Abd Latib |
collection | UMP |
description | Agarwood (Aquilaria malaccensis) is very well known as the most expensive wood in the world due to its wide applications in perfumery, cosmetic traditional medicine, and religious ceremonies. The study aimed to give an in-depth characterisation focusing on marker compounds in A. malaccensis from different places in Malaysia. The establishment of an oxygenated sesquiterpenes chemical profile of the fungus-infected agarwood oil was achieved by gas chromatography mass spectrometry (GC–MS) coupled with quadrupole time (QTOF) technique. Aroma compounds were identified as sesquiterpenes and oxygenated sesquiterpenes where agarospirol was found in samples of all locations (3.12%, 3.54%, 3.36% and 2.26% from Melaka, Pahang, Kelantan A and Kelantan B respectively) and also N-hexadecanoic acid as one of the major compounds. Both compounds were further isolated by Prep-GC and confirmed by NMR. This study provides a reference for agarwood oil analysis from different origins in Malaysia. |
first_indexed | 2024-09-25T03:50:38Z |
format | Article |
id | UMPir41652 |
institution | Universiti Malaysia Pahang |
language | English |
last_indexed | 2024-09-25T03:50:38Z |
publishDate | 2023 |
publisher | Elsevier B.V. |
record_format | dspace |
spelling | UMPir416522024-06-24T02:07:41Z http://umpir.ump.edu.my/id/eprint/41652/ Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil Erny Haslina, Abd Latib Huq, A. K. M. Moyeenul Zareen, Seema Saiful Nizam, Tajuddin Q Science (General) QH Natural history TP Chemical technology Agarwood (Aquilaria malaccensis) is very well known as the most expensive wood in the world due to its wide applications in perfumery, cosmetic traditional medicine, and religious ceremonies. The study aimed to give an in-depth characterisation focusing on marker compounds in A. malaccensis from different places in Malaysia. The establishment of an oxygenated sesquiterpenes chemical profile of the fungus-infected agarwood oil was achieved by gas chromatography mass spectrometry (GC–MS) coupled with quadrupole time (QTOF) technique. Aroma compounds were identified as sesquiterpenes and oxygenated sesquiterpenes where agarospirol was found in samples of all locations (3.12%, 3.54%, 3.36% and 2.26% from Melaka, Pahang, Kelantan A and Kelantan B respectively) and also N-hexadecanoic acid as one of the major compounds. Both compounds were further isolated by Prep-GC and confirmed by NMR. This study provides a reference for agarwood oil analysis from different origins in Malaysia. Elsevier B.V. 2023-09 Article PeerReviewed pdf en cc_by_nc_nd_4 http://umpir.ump.edu.my/id/eprint/41652/1/Gas%20chromatography%20mass%20spectrometry%20couple%20with%20quadrupole%20time-of-flight.pdf Erny Haslina, Abd Latib and Huq, A. K. M. Moyeenul and Zareen, Seema and Saiful Nizam, Tajuddin (2023) Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil. Arabian Journal of Chemistry, 16 (9). pp. 1-9. ISSN 1878-5352. (Published) https://doi.org/10.1016/j.arabjc.2023.105025 https://doi.org/10.1016/j.arabjc.2023.105025 |
spellingShingle | Q Science (General) QH Natural history TP Chemical technology Erny Haslina, Abd Latib Huq, A. K. M. Moyeenul Zareen, Seema Saiful Nizam, Tajuddin Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil |
title | Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil |
title_full | Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil |
title_fullStr | Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil |
title_full_unstemmed | Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil |
title_short | Gas chromatography mass spectrometry couple with quadrupole time-of-flight (GC-QTOF MS) as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil |
title_sort | gas chromatography mass spectrometry couple with quadrupole time of flight gc qtof ms as a powerful tool for profiling of oxygenated sesquiterpenes in agarwood oil |
topic | Q Science (General) QH Natural history TP Chemical technology |
url | http://umpir.ump.edu.my/id/eprint/41652/1/Gas%20chromatography%20mass%20spectrometry%20couple%20with%20quadrupole%20time-of-flight.pdf |
work_keys_str_mv | AT ernyhaslinaabdlatib gaschromatographymassspectrometrycouplewithquadrupoletimeofflightgcqtofmsasapowerfultoolforprofilingofoxygenatedsesquiterpenesinagarwoodoil AT huqakmmoyeenul gaschromatographymassspectrometrycouplewithquadrupoletimeofflightgcqtofmsasapowerfultoolforprofilingofoxygenatedsesquiterpenesinagarwoodoil AT zareenseema gaschromatographymassspectrometrycouplewithquadrupoletimeofflightgcqtofmsasapowerfultoolforprofilingofoxygenatedsesquiterpenesinagarwoodoil AT saifulnizamtajuddin gaschromatographymassspectrometrycouplewithquadrupoletimeofflightgcqtofmsasapowerfultoolforprofilingofoxygenatedsesquiterpenesinagarwoodoil |