Electrochemical study of polyaniline powder and its characterization

Polyaniline powder has been successfully synthesized which has received great attention due to its stable environment and possessing excellent electrical, optical and an electrochemical properties. Synthesizing pol'yaniline powder was conducted to estimate the electrochemical and it's char...

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Autore principale: Nur Nabilah, Zulkifli
Natura: Undergraduates Project Papers
Lingua:English
Pubblicazione: 2012
Soggetti:
Accesso online:http://umpir.ump.edu.my/id/eprint/7829/1/NUR_NABILAH_BT_ZULKIFLI.PDF
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author Nur Nabilah, Zulkifli
author_facet Nur Nabilah, Zulkifli
author_sort Nur Nabilah, Zulkifli
collection UMP
description Polyaniline powder has been successfully synthesized which has received great attention due to its stable environment and possessing excellent electrical, optical and an electrochemical properties. Synthesizing pol'yaniline powder was conducted to estimate the electrochemical and it's characteristic. Here polyaniline powder was synthesized by oxidative polymerization with Ammonium Persulphate used as oxidant. The blue color polyaniline powder was further characterized using Fourier Transform Infrared Spectroscopy (FTIR), Thermal Gravimetric Analysis (TGA), X-Ray Diffraction (XRD), and Cyclic Volatmmetry (CV). The FTIR spectrum shows the presence of benzoid and quinoid ring observed at 1500 cm -1 and 1600 cm-1. A shark peak centered around 25.3° and 14.7°. Thermogram of polyaniline powder shows three step of weight loss ranging from 0°C to 600°C, 15 % for the first step and 13 % for the second step. The capacitance of polyaniline powder 8 F/g was obtained. The Nquist plots shows a semicircle indicating low resistivity.
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spelling UMPir78292021-06-09T03:31:21Z http://umpir.ump.edu.my/id/eprint/7829/ Electrochemical study of polyaniline powder and its characterization Nur Nabilah, Zulkifli QD Chemistry Polyaniline powder has been successfully synthesized which has received great attention due to its stable environment and possessing excellent electrical, optical and an electrochemical properties. Synthesizing pol'yaniline powder was conducted to estimate the electrochemical and it's characteristic. Here polyaniline powder was synthesized by oxidative polymerization with Ammonium Persulphate used as oxidant. The blue color polyaniline powder was further characterized using Fourier Transform Infrared Spectroscopy (FTIR), Thermal Gravimetric Analysis (TGA), X-Ray Diffraction (XRD), and Cyclic Volatmmetry (CV). The FTIR spectrum shows the presence of benzoid and quinoid ring observed at 1500 cm -1 and 1600 cm-1. A shark peak centered around 25.3° and 14.7°. Thermogram of polyaniline powder shows three step of weight loss ranging from 0°C to 600°C, 15 % for the first step and 13 % for the second step. The capacitance of polyaniline powder 8 F/g was obtained. The Nquist plots shows a semicircle indicating low resistivity. 2012 Undergraduates Project Papers NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/7829/1/NUR_NABILAH_BT_ZULKIFLI.PDF Nur Nabilah, Zulkifli (2012) Electrochemical study of polyaniline powder and its characterization. Faculty of Industrial Sciences & Technology, Universiti Malaysia Pahang.
spellingShingle QD Chemistry
Nur Nabilah, Zulkifli
Electrochemical study of polyaniline powder and its characterization
title Electrochemical study of polyaniline powder and its characterization
title_full Electrochemical study of polyaniline powder and its characterization
title_fullStr Electrochemical study of polyaniline powder and its characterization
title_full_unstemmed Electrochemical study of polyaniline powder and its characterization
title_short Electrochemical study of polyaniline powder and its characterization
title_sort electrochemical study of polyaniline powder and its characterization
topic QD Chemistry
url http://umpir.ump.edu.my/id/eprint/7829/1/NUR_NABILAH_BT_ZULKIFLI.PDF
work_keys_str_mv AT nurnabilahzulkifli electrochemicalstudyofpolyanilinepowderanditscharacterization