Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein

This paper presents the Orthosiphon stamineus polyphenol extraction and microencapsulation study using whey protein isolate, gum arabic and maltodextrin. Polyphenol content was analysed using ultra-performance liquid chromatography. The highest yield of rosmarinic acid (38.70 mg RA/g DW) was obtaine...

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Main Authors: Sook, Fun Pang, Jolius, Gimbun, M. M., Yusoff, Luqman Chuah, Abdullah
Format: Conference or Workshop Item
Language:English
Published: 2015
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/9410/1/Microencapsulation%20of%20Polyphenols%20from%20Orthosiphon%20stamineus%20Leaves%20Extracts%20using%20Polysaccharide%20and%20Protein.pdf
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author Sook, Fun Pang
Jolius, Gimbun
M. M., Yusoff
Luqman Chuah, Abdullah
author_facet Sook, Fun Pang
Jolius, Gimbun
M. M., Yusoff
Luqman Chuah, Abdullah
author_sort Sook, Fun Pang
collection UMP
description This paper presents the Orthosiphon stamineus polyphenol extraction and microencapsulation study using whey protein isolate, gum arabic and maltodextrin. Polyphenol content was analysed using ultra-performance liquid chromatography. The highest yield of rosmarinic acid (38.70 mg RA/g DW) was obtained using 70% aqueous methanol, whereas the highest yield of sinensetin (261.21 µg Sin/g DW) and eupatorin (2.71 mg Eup/g DW) was obtained using isopropanol. Aqueous solvent such as 70% ethanol provide a broader range of polarity than the pure solvent, and hence enhances a simultaneous extraction of both methoxylated and hydroxylated compounds. It was found that microwave assisted extraction is capable to perform an efficient and very fast extraction of polyphenols within 2 minutes, compared to the ultrasonic assisted extraction which require 90 minutes. Microencapsulation of polyphenols from O. stamineus using WPI, maltodextrin and gum arabic has successfully reduced polyphenol degradation during spray drying. The highest polyphenol retention of rosmarinic acid (84.25%), sinensetin (83.96%) and eupatorin (85.61%) was achieved by microencapsulation using gum arabic. The gum arabic derived microcapsule has a smooth spherical surface which enhance particle flowability.
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spelling UMPir94102018-07-27T08:26:09Z http://umpir.ump.edu.my/id/eprint/9410/ Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein Sook, Fun Pang Jolius, Gimbun M. M., Yusoff Luqman Chuah, Abdullah Q Science (General) TP Chemical technology This paper presents the Orthosiphon stamineus polyphenol extraction and microencapsulation study using whey protein isolate, gum arabic and maltodextrin. Polyphenol content was analysed using ultra-performance liquid chromatography. The highest yield of rosmarinic acid (38.70 mg RA/g DW) was obtained using 70% aqueous methanol, whereas the highest yield of sinensetin (261.21 µg Sin/g DW) and eupatorin (2.71 mg Eup/g DW) was obtained using isopropanol. Aqueous solvent such as 70% ethanol provide a broader range of polarity than the pure solvent, and hence enhances a simultaneous extraction of both methoxylated and hydroxylated compounds. It was found that microwave assisted extraction is capable to perform an efficient and very fast extraction of polyphenols within 2 minutes, compared to the ultrasonic assisted extraction which require 90 minutes. Microencapsulation of polyphenols from O. stamineus using WPI, maltodextrin and gum arabic has successfully reduced polyphenol degradation during spray drying. The highest polyphenol retention of rosmarinic acid (84.25%), sinensetin (83.96%) and eupatorin (85.61%) was achieved by microencapsulation using gum arabic. The gum arabic derived microcapsule has a smooth spherical surface which enhance particle flowability. 2015 Conference or Workshop Item NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/9410/1/Microencapsulation%20of%20Polyphenols%20from%20Orthosiphon%20stamineus%20Leaves%20Extracts%20using%20Polysaccharide%20and%20Protein.pdf Sook, Fun Pang and Jolius, Gimbun and M. M., Yusoff and Luqman Chuah, Abdullah (2015) Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein. In: Proceeding Book MUCET 2014, Volume: 1 Engineering & Technology , 10-11 November 2014 , Mahkota Hotel Bandar Hilir Melaka. pp. 352-358.. (Published) http://ocs.utem.edu.my/index.php/mucet2014/MUCET2014/paper/view/133
spellingShingle Q Science (General)
TP Chemical technology
Sook, Fun Pang
Jolius, Gimbun
M. M., Yusoff
Luqman Chuah, Abdullah
Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein
title Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein
title_full Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein
title_fullStr Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein
title_full_unstemmed Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein
title_short Microencapsulation of Polyphenols from Orthosiphon stamineus Leaves Extracts using Polysaccharide and Protein
title_sort microencapsulation of polyphenols from orthosiphon stamineus leaves extracts using polysaccharide and protein
topic Q Science (General)
TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/9410/1/Microencapsulation%20of%20Polyphenols%20from%20Orthosiphon%20stamineus%20Leaves%20Extracts%20using%20Polysaccharide%20and%20Protein.pdf
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