Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties

Separation of xylose from xylose-glucose solution using polyester thin-film composite (TFC) membrane was investigated using fractional factorial design with manipulation of interfacial polymerization (IP) factors between triethanoamine (TEOA) and trimesoyl chloride (TMC). In previous study, the rela...

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Main Authors: K. H., Mah, Wan Mohd Hafizuddin, Wan Yussof, Mazrul Nizam, Abu Seman, A. W., Mohammad
Format: Conference or Workshop Item
Language:English
Published: 2015
Subjects:
Online Access:http://umpir.ump.edu.my/id/eprint/9548/1/fkksa-2015-K.%20H.%20Mah-Separation%20Of%20Xylose.pdf
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author K. H., Mah
Wan Mohd Hafizuddin, Wan Yussof
Mazrul Nizam, Abu Seman
A. W., Mohammad
author_facet K. H., Mah
Wan Mohd Hafizuddin, Wan Yussof
Mazrul Nizam, Abu Seman
A. W., Mohammad
author_sort K. H., Mah
collection UMP
description Separation of xylose from xylose-glucose solution using polyester thin-film composite (TFC) membrane was investigated using fractional factorial design with manipulation of interfacial polymerization (IP) factors between triethanoamine (TEOA) and trimesoyl chloride (TMC). In previous study, the relation between xylose separation factor and all affecting factors were developed in a model. In this present study, a new TFC membrane were produced from this model by the reaction between 4 % (w/v) TEOA concentration, 0.25 % (w/v) TMC concentration, reaction time of 44.85 minutes, pH 8, and curing at 60 ℃ for 30 minutes. Evaluation on the performance of TFC membrane shows that the xylose separation factor obtained in the study was 1.686, which has an error of 4.27 % compared to the predicted value. Membrane fouling has been studied for a course of 6 hours where the normalized relative flux (NRF) was at 16.61 (±3.53) %. From this value, irreversible fouling resulted in 11.02 (±5.60) % which might due to internal pore blockage of glucose and xylose. In contrast, reversible fouling of 5.59 % can be obtained back after cleaning with ultrapure water.
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spelling UMPir95482018-02-07T06:42:51Z http://umpir.ump.edu.my/id/eprint/9548/ Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties K. H., Mah Wan Mohd Hafizuddin, Wan Yussof Mazrul Nizam, Abu Seman A. W., Mohammad TP Chemical technology Separation of xylose from xylose-glucose solution using polyester thin-film composite (TFC) membrane was investigated using fractional factorial design with manipulation of interfacial polymerization (IP) factors between triethanoamine (TEOA) and trimesoyl chloride (TMC). In previous study, the relation between xylose separation factor and all affecting factors were developed in a model. In this present study, a new TFC membrane were produced from this model by the reaction between 4 % (w/v) TEOA concentration, 0.25 % (w/v) TMC concentration, reaction time of 44.85 minutes, pH 8, and curing at 60 ℃ for 30 minutes. Evaluation on the performance of TFC membrane shows that the xylose separation factor obtained in the study was 1.686, which has an error of 4.27 % compared to the predicted value. Membrane fouling has been studied for a course of 6 hours where the normalized relative flux (NRF) was at 16.61 (±3.53) %. From this value, irreversible fouling resulted in 11.02 (±5.60) % which might due to internal pore blockage of glucose and xylose. In contrast, reversible fouling of 5.59 % can be obtained back after cleaning with ultrapure water. 2015 Conference or Workshop Item NonPeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/9548/1/fkksa-2015-K.%20H.%20Mah-Separation%20Of%20Xylose.pdf K. H., Mah and Wan Mohd Hafizuddin, Wan Yussof and Mazrul Nizam, Abu Seman and A. W., Mohammad (2015) Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties. In: International Conference on Environment 2015 (ICENV 2015) , 18-19 August 2015 , Eastin Hotel, Pulau Pinang. pp. 1-8.. (Published)
spellingShingle TP Chemical technology
K. H., Mah
Wan Mohd Hafizuddin, Wan Yussof
Mazrul Nizam, Abu Seman
A. W., Mohammad
Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties
title Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties
title_full Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties
title_fullStr Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties
title_full_unstemmed Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties
title_short Separation Of Xylose From Glucose Using Thinfilm Composite Membrane: A Study On Separation Performance And Fouling Properties
title_sort separation of xylose from glucose using thinfilm composite membrane a study on separation performance and fouling properties
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/9548/1/fkksa-2015-K.%20H.%20Mah-Separation%20Of%20Xylose.pdf
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