Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy

Gold nanoparticle films are of interest in several branches of science and technology, and accurate sample characterization is needed but technically demanding. We prepared such films by DC magnetron sputtering and recorded their mass thickness by Rutherford backscattering spectroscopy. The geometri...

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Main Authors: Pia C. Lansåker, Anders Hallén, Gunnar A. Niklasson, Claes G. Granqvist
Format: Article
Language:English
Published: AIP Publishing LLC 2014-10-01
Series:AIP Advances
Online Access:http://dx.doi.org/10.1063/1.4897340
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author Pia C. Lansåker
Anders Hallén
Gunnar A. Niklasson
Claes G. Granqvist
author_facet Pia C. Lansåker
Anders Hallén
Gunnar A. Niklasson
Claes G. Granqvist
author_sort Pia C. Lansåker
collection DOAJ
description Gold nanoparticle films are of interest in several branches of science and technology, and accurate sample characterization is needed but technically demanding. We prepared such films by DC magnetron sputtering and recorded their mass thickness by Rutherford backscattering spectroscopy. The geometric thickness dg—from the substrate to the tops of the nanoparticles—was obtained by scanning electron microscopy (SEM) combined with image analysis as well as by atomic force microscopy (AFM). The various techniques yielded an internally consistent characterization of the films. In particular, very similar results for dg were obtained by SEM with image analysis and by AFM.
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spelling doaj.art-01301596795c45c892018816930fbbd92022-12-22T03:17:07ZengAIP Publishing LLCAIP Advances2158-32262014-10-01410107101107101-610.1063/1.4897340005410ADVCharacterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopyPia C. Lansåker0Anders Hallén1Gunnar A. Niklasson2Claes G. Granqvist3Department of Engineering Sciences, The Ångström Laboratory, Uppsala University, P. O. Box 534, SE-751 21 Uppsala, SwedenRoyal Institute of Technology, KTH-ICT, Elektrum 229, Kista, SE-164 40 Stockholm, SwedenDepartment of Engineering Sciences, The Ångström Laboratory, Uppsala University, P. O. Box 534, SE-751 21 Uppsala, SwedenDepartment of Engineering Sciences, The Ångström Laboratory, Uppsala University, P. O. Box 534, SE-751 21 Uppsala, SwedenGold nanoparticle films are of interest in several branches of science and technology, and accurate sample characterization is needed but technically demanding. We prepared such films by DC magnetron sputtering and recorded their mass thickness by Rutherford backscattering spectroscopy. The geometric thickness dg—from the substrate to the tops of the nanoparticles—was obtained by scanning electron microscopy (SEM) combined with image analysis as well as by atomic force microscopy (AFM). The various techniques yielded an internally consistent characterization of the films. In particular, very similar results for dg were obtained by SEM with image analysis and by AFM.http://dx.doi.org/10.1063/1.4897340
spellingShingle Pia C. Lansåker
Anders Hallén
Gunnar A. Niklasson
Claes G. Granqvist
Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy
AIP Advances
title Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy
title_full Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy
title_fullStr Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy
title_full_unstemmed Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy
title_short Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy
title_sort characterization of gold nanoparticle films rutherford backscattering spectroscopy scanning electron microscopy with image analysis and atomic force microscopy
url http://dx.doi.org/10.1063/1.4897340
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