1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole
1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole (<b>1</b>) was synthesized, starting from 9<i>H</i>-carbazole and 4-fluorobenzonitrile, by Friedel–Crafts acylation, using boron trichloride to direct the substitution in 1-position. Single-crystal X-ray diffraction analysis...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
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MDPI AG
2022-08-01
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| Series: | Molbank |
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| Online Access: | https://www.mdpi.com/1422-8599/2022/3/M1430 |
| _version_ | 1827658428349153280 |
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| author | Markus Laube Jonas König Martin Köckerling Torsten Kniess |
| author_facet | Markus Laube Jonas König Martin Köckerling Torsten Kniess |
| author_sort | Markus Laube |
| collection | DOAJ |
| description | 1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole (<b>1</b>) was synthesized, starting from 9<i>H</i>-carbazole and 4-fluorobenzonitrile, by Friedel–Crafts acylation, using boron trichloride to direct the substitution in 1-position. Single-crystal X-ray diffraction analysis unambiguously revealed the molecular structure of <b>1</b>. |
| first_indexed | 2024-03-09T23:03:34Z |
| format | Article |
| id | doaj.art-01e39845b61b40eba37a2e46e4d47d85 |
| institution | Directory Open Access Journal |
| issn | 1422-8599 |
| language | English |
| last_indexed | 2024-03-09T23:03:34Z |
| publishDate | 2022-08-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molbank |
| spelling | doaj.art-01e39845b61b40eba37a2e46e4d47d852023-11-23T17:57:45ZengMDPI AGMolbank1422-85992022-08-0120223M143010.3390/M14301-(4-Fluorobenzoyl)-9<i>H</i>-carbazoleMarkus Laube0Jonas König1Martin Köckerling2Torsten Kniess3Department Radiopharmaceutical and Chemical Biology, Institute of Radiopharmaceutical Cancer Research, Helmholtz-Zentrum Dresden-Rossendorf, Bautzner Landstraße 400, 01328 Dresden, GermanyDepartment of Inorganic Solid-State Chemistry, Institute of Chemistry, University of Rostock, Albert-Einstein-Str. 3a, 18059 Rostock, GermanyDepartment of Inorganic Solid-State Chemistry, Institute of Chemistry, University of Rostock, Albert-Einstein-Str. 3a, 18059 Rostock, GermanyDepartment Radiopharmaceutical and Chemical Biology, Institute of Radiopharmaceutical Cancer Research, Helmholtz-Zentrum Dresden-Rossendorf, Bautzner Landstraße 400, 01328 Dresden, Germany1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole (<b>1</b>) was synthesized, starting from 9<i>H</i>-carbazole and 4-fluorobenzonitrile, by Friedel–Crafts acylation, using boron trichloride to direct the substitution in 1-position. Single-crystal X-ray diffraction analysis unambiguously revealed the molecular structure of <b>1</b>.https://www.mdpi.com/1422-8599/2022/3/M1430carbazoleFriedel–Crafts acylationboron trichloridestructure determination |
| spellingShingle | Markus Laube Jonas König Martin Köckerling Torsten Kniess 1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole Molbank carbazole Friedel–Crafts acylation boron trichloride structure determination |
| title | 1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole |
| title_full | 1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole |
| title_fullStr | 1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole |
| title_full_unstemmed | 1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole |
| title_short | 1-(4-Fluorobenzoyl)-9<i>H</i>-carbazole |
| title_sort | 1 4 fluorobenzoyl 9 i h i carbazole |
| topic | carbazole Friedel–Crafts acylation boron trichloride structure determination |
| url | https://www.mdpi.com/1422-8599/2022/3/M1430 |
| work_keys_str_mv | AT markuslaube 14fluorobenzoyl9ihicarbazole AT jonaskonig 14fluorobenzoyl9ihicarbazole AT martinkockerling 14fluorobenzoyl9ihicarbazole AT torstenkniess 14fluorobenzoyl9ihicarbazole |