(E)-2-((4R,5R)-5-((Benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-ene-1,4-diol

(E)-2-((4R,5R)-5-((Benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-ene-1,4-diol

The synthesis of (E)-2-((4R,5R)-5-((benzyloxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)but-2-ene-1,4-diol by a one-step reduction of the appropriate 2-substituted butenolide is reported. Product characterization was carried out by IR, 1H NMR, 13C NMR, MS, elemental analysis and optical rotation.

Bibliographic Details
Main Authors: Carlos R. Carreras, Celina E. García, Víctor S. Martín, Carlos E. Tonn, David Díaz Díaz, Juan Pedro Ceñal
Format: Article
Language:English
Published: MDPI AG 2010-04-01
Series:Molbank
Subjects:
reduction
DIBAL-H
substituted butenolides
allylic diols
Online Access:http://www.mdpi.com/1422-8599/2010/2/M676/

Internet

http://www.mdpi.com/1422-8599/2010/2/M676/

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