Chemical Analysis of Sexual Lubricant Residue: A Comparison of Medical Examination Swabs Analyzed Using Spectroscopic Techniques

Sexual assault kits are the standard method for collecting and preserving sexual assault evidence. During the sexual assault examination, swabs are commonly used to collect bodily fluids as sexual assault evidence from the vagina, anus, mouth, and skin. The type of fiber swab used during collection...

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Main Authors: Safiya J. Best, Santana Thomas, Nancy Flynn, Candice Bridge
Format: Article
Language:English
Published: MDPI AG 2023-12-01
Series:Forensic Sciences
Subjects:
Online Access:https://www.mdpi.com/2673-6756/3/4/45
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author Safiya J. Best
Santana Thomas
Nancy Flynn
Candice Bridge
author_facet Safiya J. Best
Santana Thomas
Nancy Flynn
Candice Bridge
author_sort Safiya J. Best
collection DOAJ
description Sexual assault kits are the standard method for collecting and preserving sexual assault evidence. During the sexual assault examination, swabs are commonly used to collect bodily fluids as sexual assault evidence from the vagina, anus, mouth, and skin. The type of fiber swab used during collection can greatly influence the recovery of the substrate. In cases where lubricant residue may be present, it would be useful to identify the swab type that would be the most efficient in the collection of lubricant residues. In this study, four types of swabs with different fibers (i.e., cotton, polyester, rayon, and foam) with sexual lubricants present, were extracted in various solvents. The extracts were analyzed using attenuated total reflectance Fourier-transform infrared (ATR-FTIR) and Raman spectroscopy. The Pearson correlation coefficient (PCCs) test was applied to determine a pairwise comparison between swab lube extracts and the standard lubricant reference. Visual comparisons of the lubricant reference, blank fiber swab, and the fiber lubricant extract were used to determine peak overlap, significance, and matrix interference.
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spelling doaj.art-0276d0ff1a1142be8fec945f1b1b0a8f2023-12-22T14:09:11ZengMDPI AGForensic Sciences2673-67562023-12-013462063710.3390/forensicsci3040045Chemical Analysis of Sexual Lubricant Residue: A Comparison of Medical Examination Swabs Analyzed Using Spectroscopic TechniquesSafiya J. Best0Santana Thomas1Nancy Flynn2Candice Bridge3Department of Chemistry, University of Central Florida, Orlando, FL 32816, USANational Center for Forensic Science, University of Central Florida, Orlando, FL 32816, USADepartment of Chemistry, University of Central Florida, Orlando, FL 32816, USADepartment of Chemistry, University of Central Florida, Orlando, FL 32816, USASexual assault kits are the standard method for collecting and preserving sexual assault evidence. During the sexual assault examination, swabs are commonly used to collect bodily fluids as sexual assault evidence from the vagina, anus, mouth, and skin. The type of fiber swab used during collection can greatly influence the recovery of the substrate. In cases where lubricant residue may be present, it would be useful to identify the swab type that would be the most efficient in the collection of lubricant residues. In this study, four types of swabs with different fibers (i.e., cotton, polyester, rayon, and foam) with sexual lubricants present, were extracted in various solvents. The extracts were analyzed using attenuated total reflectance Fourier-transform infrared (ATR-FTIR) and Raman spectroscopy. The Pearson correlation coefficient (PCCs) test was applied to determine a pairwise comparison between swab lube extracts and the standard lubricant reference. Visual comparisons of the lubricant reference, blank fiber swab, and the fiber lubricant extract were used to determine peak overlap, significance, and matrix interference.https://www.mdpi.com/2673-6756/3/4/45forensic lubricantsoptimal swabsample collectionATR-FTIRRaman spectroscopy
spellingShingle Safiya J. Best
Santana Thomas
Nancy Flynn
Candice Bridge
Chemical Analysis of Sexual Lubricant Residue: A Comparison of Medical Examination Swabs Analyzed Using Spectroscopic Techniques
Forensic Sciences
forensic lubricants
optimal swab
sample collection
ATR-FTIR
Raman spectroscopy
title Chemical Analysis of Sexual Lubricant Residue: A Comparison of Medical Examination Swabs Analyzed Using Spectroscopic Techniques
title_full Chemical Analysis of Sexual Lubricant Residue: A Comparison of Medical Examination Swabs Analyzed Using Spectroscopic Techniques
title_fullStr Chemical Analysis of Sexual Lubricant Residue: A Comparison of Medical Examination Swabs Analyzed Using Spectroscopic Techniques
title_full_unstemmed Chemical Analysis of Sexual Lubricant Residue: A Comparison of Medical Examination Swabs Analyzed Using Spectroscopic Techniques
title_short Chemical Analysis of Sexual Lubricant Residue: A Comparison of Medical Examination Swabs Analyzed Using Spectroscopic Techniques
title_sort chemical analysis of sexual lubricant residue a comparison of medical examination swabs analyzed using spectroscopic techniques
topic forensic lubricants
optimal swab
sample collection
ATR-FTIR
Raman spectroscopy
url https://www.mdpi.com/2673-6756/3/4/45
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AT nancyflynn chemicalanalysisofsexuallubricantresidueacomparisonofmedicalexaminationswabsanalyzedusingspectroscopictechniques
AT candicebridge chemicalanalysisofsexuallubricantresidueacomparisonofmedicalexaminationswabsanalyzedusingspectroscopictechniques