Evaluation of the reliability of twin variant analysis in Mg alloys by in situ EBSD technique

Electron backscatter diffraction (EBSD) is an orientation mapping technique, which has been widely used to study texture evolution and twinning behavior. This work aims to study the variant of {101¯2} twins during tensile deformation of AZ31 Mg alloys. An in-situ tensile stage was used, and coupled...

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Main Authors: Feiya Liu, Changfa Guo, Renlong Xin, Guilin Wu, Qing Liu
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2019-06-01
Series:Journal of Magnesium and Alloys
Online Access:http://www.sciencedirect.com/science/article/pii/S2213956719300209
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author Feiya Liu
Changfa Guo
Renlong Xin
Guilin Wu
Qing Liu
author_facet Feiya Liu
Changfa Guo
Renlong Xin
Guilin Wu
Qing Liu
author_sort Feiya Liu
collection DOAJ
description Electron backscatter diffraction (EBSD) is an orientation mapping technique, which has been widely used to study texture evolution and twinning behavior. This work aims to study the variant of {101¯2} twins during tensile deformation of AZ31 Mg alloys. An in-situ tensile stage was used, and coupled with EBSD technique, the variants of twins can be analyzed without releasing the tensile stress. Based on the EBSD maps, the first and second smallest misorientation angles (M1 and M2) between each active twin and respective potential variants were calculated, and the distribution of M1 values with tensile strain was obtained. The results indicated that {101¯2} twins were deviated from their ideal orientations with strain increased. The criteria of M1<4° and M2−M1>2° were suggested to be applied to select the data points for reliable variant identification. Moreover, it confirmed that the deviation of twin relationship was ascribed to the profuse basal glide in matrices and/or twins. Keywords: Twinning, Variant identification, Magnesium alloy, Lattice rotation, EBSD
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spelling doaj.art-028050228c2543e6a3ed06f50f7d24ab2024-04-16T22:04:04ZengKeAi Communications Co., Ltd.Journal of Magnesium and Alloys2213-95672019-06-0172258263Evaluation of the reliability of twin variant analysis in Mg alloys by in situ EBSD techniqueFeiya Liu0Changfa Guo1Renlong Xin2Guilin Wu3Qing Liu4Joint International Laboratory for Light Alloys (MOE), College of Materials Science and Engineering, Chongqing University, Sha Zheng Jie 174, Sha Ping Ba District, Chongqing, ChinaJoint International Laboratory for Light Alloys (MOE), College of Materials Science and Engineering, Chongqing University, Sha Zheng Jie 174, Sha Ping Ba District, Chongqing, China; College of Materials Science and Engineering, China Jiliang University, Hangzhou, ChinaJoint International Laboratory for Light Alloys (MOE), College of Materials Science and Engineering, Chongqing University, Sha Zheng Jie 174, Sha Ping Ba District, Chongqing, China; Corresponding author.Joint International Laboratory for Light Alloys (MOE), College of Materials Science and Engineering, Chongqing University, Sha Zheng Jie 174, Sha Ping Ba District, Chongqing, ChinaJoint International Laboratory for Light Alloys (MOE), College of Materials Science and Engineering, Chongqing University, Sha Zheng Jie 174, Sha Ping Ba District, Chongqing, ChinaElectron backscatter diffraction (EBSD) is an orientation mapping technique, which has been widely used to study texture evolution and twinning behavior. This work aims to study the variant of {101¯2} twins during tensile deformation of AZ31 Mg alloys. An in-situ tensile stage was used, and coupled with EBSD technique, the variants of twins can be analyzed without releasing the tensile stress. Based on the EBSD maps, the first and second smallest misorientation angles (M1 and M2) between each active twin and respective potential variants were calculated, and the distribution of M1 values with tensile strain was obtained. The results indicated that {101¯2} twins were deviated from their ideal orientations with strain increased. The criteria of M1<4° and M2−M1>2° were suggested to be applied to select the data points for reliable variant identification. Moreover, it confirmed that the deviation of twin relationship was ascribed to the profuse basal glide in matrices and/or twins. Keywords: Twinning, Variant identification, Magnesium alloy, Lattice rotation, EBSDhttp://www.sciencedirect.com/science/article/pii/S2213956719300209
spellingShingle Feiya Liu
Changfa Guo
Renlong Xin
Guilin Wu
Qing Liu
Evaluation of the reliability of twin variant analysis in Mg alloys by in situ EBSD technique
Journal of Magnesium and Alloys
title Evaluation of the reliability of twin variant analysis in Mg alloys by in situ EBSD technique
title_full Evaluation of the reliability of twin variant analysis in Mg alloys by in situ EBSD technique
title_fullStr Evaluation of the reliability of twin variant analysis in Mg alloys by in situ EBSD technique
title_full_unstemmed Evaluation of the reliability of twin variant analysis in Mg alloys by in situ EBSD technique
title_short Evaluation of the reliability of twin variant analysis in Mg alloys by in situ EBSD technique
title_sort evaluation of the reliability of twin variant analysis in mg alloys by in situ ebsd technique
url http://www.sciencedirect.com/science/article/pii/S2213956719300209
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AT renlongxin evaluationofthereliabilityoftwinvariantanalysisinmgalloysbyinsituebsdtechnique
AT guilinwu evaluationofthereliabilityoftwinvariantanalysisinmgalloysbyinsituebsdtechnique
AT qingliu evaluationofthereliabilityoftwinvariantanalysisinmgalloysbyinsituebsdtechnique