One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole

One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole

In this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported.

Bibliographic Details
Main Authors: Mehrak Faraji, Avat Arman Taherpour
Format: Article
Language:English
Published: MDPI AG 2008-09-01
Series:Molbank
Subjects:
Microwave assisted synthesis
1
3-Dipolar cycloadditions
Benzyne intermediate
1H-Phenanthro[9
10-d][1
2
3]triazole
3-Triazoles
Online Access:http://www.mdpi.com/1422-8599/2008/3//
Description
Summary:In this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported.
ISSN:1422-8599

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