One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole
In this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported.
Main Authors: | , |
---|---|
Format: | Article |
Language: | English |
Published: |
MDPI AG
2008-09-01
|
Series: | Molbank |
Subjects: | |
Online Access: | http://www.mdpi.com/1422-8599/2008/3// |
_version_ | 1811244424926068736 |
---|---|
author | Mehrak Faraji Avat Arman Taherpour |
author_facet | Mehrak Faraji Avat Arman Taherpour |
author_sort | Mehrak Faraji |
collection | DOAJ |
description | In this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported. |
first_indexed | 2024-04-12T14:24:47Z |
format | Article |
id | doaj.art-036fee41b8b040528d1ea8519e62ad73 |
institution | Directory Open Access Journal |
issn | 1422-8599 |
language | English |
last_indexed | 2024-04-12T14:24:47Z |
publishDate | 2008-09-01 |
publisher | MDPI AG |
record_format | Article |
series | Molbank |
spelling | doaj.art-036fee41b8b040528d1ea8519e62ad732022-12-22T03:29:27ZengMDPI AGMolbank1422-85992008-09-0120083M57710.3390/M577One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazoleMehrak FarajiAvat Arman TaherpourIn this study, a fast and good yield one-pot microwave-assisted synthesis (45 seconds) of 1H-phenanthro[9,10-d][1,2,3]triazole by a 1,3-dipolar cycloaddition reaction of sodium azide and 9-bromophenanthrene in the presence of potassium tert-butoxide in DMSO as solvent is reported.http://www.mdpi.com/1422-8599/2008/3//Microwave assisted synthesis13-Dipolar cycloadditionsBenzyne intermediate1H-Phenanthro[910-d][123]triazole123-Triazoles |
spellingShingle | Mehrak Faraji Avat Arman Taherpour One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole Molbank Microwave assisted synthesis 1 3-Dipolar cycloadditions Benzyne intermediate 1H-Phenanthro[9 10-d][1 2 3]triazole 1 2 3-Triazoles |
title | One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole |
title_full | One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole |
title_fullStr | One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole |
title_full_unstemmed | One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole |
title_short | One-pot Microwave-Assisted Synthesis of 1H-Phenanthro[9,10- d][1,2,3]triazole |
title_sort | one pot microwave assisted synthesis of 1h phenanthro 9 10 d 1 2 3 triazole |
topic | Microwave assisted synthesis 1 3-Dipolar cycloadditions Benzyne intermediate 1H-Phenanthro[9 10-d][1 2 3]triazole 1 2 3-Triazoles |
url | http://www.mdpi.com/1422-8599/2008/3// |
work_keys_str_mv | AT mehrakfaraji onepotmicrowaveassistedsynthesisof1hphenanthro910d123triazole AT avatarmantaherpour onepotmicrowaveassistedsynthesisof1hphenanthro910d123triazole |