Synthesis of mesh-shaped calcia partially stabilized zirconia using eggshell membrane template as filler composite

Introduction: This experiment was conducted experimentally to synthesize Calcia Partially Stabilized Zirconia (Ca-PSZ) by sol-gel method using eggshell membrane template as a composite filler. The eggshell membrane was used to produce a mesh shaped structure, which hopefully can improve the mechanic...

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Main Authors: Gema Gempita, Zulia Hasratiningsih, Gantini Subrata, Bambang Sunendar Purwasasmita
Format: Article
Language:English
Published: Universitas Padjadjaran 2017-07-01
Series:Padjadjaran Journal of Dentistry
Subjects:
Online Access:http://jurnal.unpad.ac.id/pjd/article/view/13603
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author Gema Gempita
Zulia Hasratiningsih
Gantini Subrata
Bambang Sunendar Purwasasmita
author_facet Gema Gempita
Zulia Hasratiningsih
Gantini Subrata
Bambang Sunendar Purwasasmita
author_sort Gema Gempita
collection DOAJ
description Introduction: This experiment was conducted experimentally to synthesize Calcia Partially Stabilized Zirconia (Ca-PSZ) by sol-gel method using eggshell membrane template as a composite filler. The eggshell membrane was used to produce a mesh shaped structure, which hopefully can improve the mechanical properties of the composite. Method: Ca-PSZ filler was synthesized from ZrOCl2 precursor and Ca(NO3)2 stabilizer with a 24 hours immersion time. Ca-PSZ of synthesis then mixed with the resin matrix to test its composite hardness. Result: The EDS characterization results suggested that the sample contained elements of zirconia, calcium, and oxygen. Whereas, the XRD characterization identified that crystal structures that formed in the sample were nano scale tetragonal. Characterization of SEM showed Ca-PSZ with mesh structured. The average composite hardness value was 15.79 VHN. Conclusion: The composites with Ca-PSZ-synthesized filler could be prepared and its hardness value was higher than the composite with Ca-PSZ filler in spherical particles, but the hardness was still below the composite on the market.
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spelling doaj.art-03eb717bc92a4b9db35059a72b99faaf2022-12-21T17:43:03ZengUniversitas PadjadjaranPadjadjaran Journal of Dentistry1979-02012549-62122017-07-0129210.24198/pjd.vol29no2.136037550Synthesis of mesh-shaped calcia partially stabilized zirconia using eggshell membrane template as filler compositeGema Gempita0Zulia Hasratiningsih1Gantini Subrata2Bambang Sunendar Purwasasmita3Ministry of Health Republic of IndonesiaUniversitas PadjadjaranUniversitas PadjadjaranInstitut Teknologi BandungIntroduction: This experiment was conducted experimentally to synthesize Calcia Partially Stabilized Zirconia (Ca-PSZ) by sol-gel method using eggshell membrane template as a composite filler. The eggshell membrane was used to produce a mesh shaped structure, which hopefully can improve the mechanical properties of the composite. Method: Ca-PSZ filler was synthesized from ZrOCl2 precursor and Ca(NO3)2 stabilizer with a 24 hours immersion time. Ca-PSZ of synthesis then mixed with the resin matrix to test its composite hardness. Result: The EDS characterization results suggested that the sample contained elements of zirconia, calcium, and oxygen. Whereas, the XRD characterization identified that crystal structures that formed in the sample were nano scale tetragonal. Characterization of SEM showed Ca-PSZ with mesh structured. The average composite hardness value was 15.79 VHN. Conclusion: The composites with Ca-PSZ-synthesized filler could be prepared and its hardness value was higher than the composite with Ca-PSZ filler in spherical particles, but the hardness was still below the composite on the market.http://jurnal.unpad.ac.id/pjd/article/view/13603ca-psz filler, sol-gel method, eggshell membrane template, composite hardness
spellingShingle Gema Gempita
Zulia Hasratiningsih
Gantini Subrata
Bambang Sunendar Purwasasmita
Synthesis of mesh-shaped calcia partially stabilized zirconia using eggshell membrane template as filler composite
Padjadjaran Journal of Dentistry
ca-psz filler, sol-gel method, eggshell membrane template, composite hardness
title Synthesis of mesh-shaped calcia partially stabilized zirconia using eggshell membrane template as filler composite
title_full Synthesis of mesh-shaped calcia partially stabilized zirconia using eggshell membrane template as filler composite
title_fullStr Synthesis of mesh-shaped calcia partially stabilized zirconia using eggshell membrane template as filler composite
title_full_unstemmed Synthesis of mesh-shaped calcia partially stabilized zirconia using eggshell membrane template as filler composite
title_short Synthesis of mesh-shaped calcia partially stabilized zirconia using eggshell membrane template as filler composite
title_sort synthesis of mesh shaped calcia partially stabilized zirconia using eggshell membrane template as filler composite
topic ca-psz filler, sol-gel method, eggshell membrane template, composite hardness
url http://jurnal.unpad.ac.id/pjd/article/view/13603
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AT zuliahasratiningsih synthesisofmeshshapedcalciapartiallystabilizedzirconiausingeggshellmembranetemplateasfillercomposite
AT gantinisubrata synthesisofmeshshapedcalciapartiallystabilizedzirconiausingeggshellmembranetemplateasfillercomposite
AT bambangsunendarpurwasasmita synthesisofmeshshapedcalciapartiallystabilizedzirconiausingeggshellmembranetemplateasfillercomposite