Characterisation of Cellulose Nanofibres Derived from Chemical and Mechanical Treatments

Optimised routes have been established to obtain high aspect ratio cellulose microfibrils derived from plant feedstocks, involving a combination of a chemical and mechanical treatment using a high pressure microfluidizer. By this means, nano-cellulose was produced using different pretreatment protoc...

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Main Authors: Muhamad Martini, Hornsby Peter, Carmichael Eugene, Zakaria Muhammad, Seok Yew Been, Mohamed Saiful, Sharma Shekhar
Format: Article
Language:English
Published: EDP Sciences 2019-01-01
Series:MATEC Web of Conferences
Online Access:https://doi.org/10.1051/matecconf/201925301002
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author Muhamad Martini
Hornsby Peter
Carmichael Eugene
Zakaria Muhammad
Seok Yew Been
Mohamed Saiful
Sharma Shekhar
author_facet Muhamad Martini
Hornsby Peter
Carmichael Eugene
Zakaria Muhammad
Seok Yew Been
Mohamed Saiful
Sharma Shekhar
author_sort Muhamad Martini
collection DOAJ
description Optimised routes have been established to obtain high aspect ratio cellulose microfibrils derived from plant feedstocks, involving a combination of a chemical and mechanical treatment using a high pressure microfluidizer. By this means, nano-cellulose was produced using different pretreatment protocols. The nanofibres produced were characterised for its particle size distribution measurement (laser diffraction and zeta potential analysis) and fourier transform infrared for its structural analysis. Results obtained and subsequent trends observed in chemical, mechanical and chemo-mechanical treated nanofibres were compared and contrasted. The chemomechanical treatment (TEMPO-oxidation and high pressure microfluidisation) yielded higher aspect ratio nanofibrils than nanofibrils made by solely chemical or mechanical treatment.
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spelling doaj.art-04eb2230a9204600a792747467d95f432022-12-21T20:19:00ZengEDP SciencesMATEC Web of Conferences2261-236X2019-01-012530100210.1051/matecconf/201925301002matecconf_msme2018_01002Characterisation of Cellulose Nanofibres Derived from Chemical and Mechanical TreatmentsMuhamad Martini0Hornsby Peter1Carmichael Eugene2Zakaria Muhammad3Seok Yew Been4Mohamed Saiful5Sharma Shekhar6Faculty of Innovative Design and Technology, Universiti Sultan Zainal AbidinPolymer Cluster, Queen’s University Belfast, School of Mechanical and Aerospace Engineering, Ashby BuildingApplied Plant Science Division, Agri-Food and Bioscience InstituteFaculty of Manufacturing Engineering Technology, TATI University CollegeFaculty of Innovative Design and Technology, Universiti Sultan Zainal AbidinFaculty of Innovative Design and Technology, Universiti Sultan Zainal AbidinApplied Plant Science Division, Agri-Food and Bioscience InstituteOptimised routes have been established to obtain high aspect ratio cellulose microfibrils derived from plant feedstocks, involving a combination of a chemical and mechanical treatment using a high pressure microfluidizer. By this means, nano-cellulose was produced using different pretreatment protocols. The nanofibres produced were characterised for its particle size distribution measurement (laser diffraction and zeta potential analysis) and fourier transform infrared for its structural analysis. Results obtained and subsequent trends observed in chemical, mechanical and chemo-mechanical treated nanofibres were compared and contrasted. The chemomechanical treatment (TEMPO-oxidation and high pressure microfluidisation) yielded higher aspect ratio nanofibrils than nanofibrils made by solely chemical or mechanical treatment.https://doi.org/10.1051/matecconf/201925301002
spellingShingle Muhamad Martini
Hornsby Peter
Carmichael Eugene
Zakaria Muhammad
Seok Yew Been
Mohamed Saiful
Sharma Shekhar
Characterisation of Cellulose Nanofibres Derived from Chemical and Mechanical Treatments
MATEC Web of Conferences
title Characterisation of Cellulose Nanofibres Derived from Chemical and Mechanical Treatments
title_full Characterisation of Cellulose Nanofibres Derived from Chemical and Mechanical Treatments
title_fullStr Characterisation of Cellulose Nanofibres Derived from Chemical and Mechanical Treatments
title_full_unstemmed Characterisation of Cellulose Nanofibres Derived from Chemical and Mechanical Treatments
title_short Characterisation of Cellulose Nanofibres Derived from Chemical and Mechanical Treatments
title_sort characterisation of cellulose nanofibres derived from chemical and mechanical treatments
url https://doi.org/10.1051/matecconf/201925301002
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