C<sub>f</sub>/SiC Ceramic Matrix Composites with Extraordinary Thermomechanical Properties up to 2000 °C

The thermomechanical properties of carbon fiber reinforced silicon carbide ceramic matrix composites (C<sub>f</sub>/SiC CMCs) were studied up to 2000 °C using high-temperature in situ flexural testing in argon. The CMC specimens were fabricated using an ultrahigh concentration (66 vol%)...

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Bibliographic Details
Main Authors: Min-sung Park, Jian Gu, Heesoo Lee, Sea-Hoon Lee, Lun Feng, William G. Fahrenholtz
Format: Article
Language:English
Published: MDPI AG 2023-12-01
Series:Nanomaterials
Subjects:
Online Access:https://www.mdpi.com/2079-4991/14/1/72
Description
Summary:The thermomechanical properties of carbon fiber reinforced silicon carbide ceramic matrix composites (C<sub>f</sub>/SiC CMCs) were studied up to 2000 °C using high-temperature in situ flexural testing in argon. The CMC specimens were fabricated using an ultrahigh concentration (66 vol%) aqueous slurry containing nano-sized silicon carbide powder. The SiC powder compacts were obtained by drying the slurry and were densified using the precursor impregnation and pyrolysis (PIP) method with field assisted sintering technology/spark plasma sintering (FAST/SPS). The high relative density of the SiC green body (77.6%) enabled densification within 2.5 days using four PIP cycles. In contrast, conventional PIP processes take over 7 days. The in situ flexural strength of the C<sub>f</sub>/SiC CMC was 434 MPa at 1750 °C, which was 84% higher than the room temperature value. The value further increased to 542 MPa at 2000 °C. Possible mechanisms to explain the excellent strength of the CMC at elevated temperatures are discussed.
ISSN:2079-4991