Analysis the Volatiles and Its Aroma Contribution in Rosa Sterilis by HS-SPME and LLE-SAFE

To comprehensively analyze the composition and contribution of volatile components in Rosa sterilis, the headspace solid phase microextraction (HS-SPME) and liquid liquid extraction with solvent assisted flavor evaporation (LLE-SAFE) was used, along with gas chromatography-mass spectrometry (GC-MS)...

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Main Authors: Haoran MO, Mingzheng HUANG, Qun ZHANG, Weiyuan TANG, Tingting LI, Cunbin XU, Xiaozhu LIU, Zhihai YU, Xin LI
Format: Article
Language:zho
Published: The editorial department of Science and Technology of Food Industry 2023-10-01
Series:Shipin gongye ke-ji
Subjects:
Online Access:http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2022090300
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author Haoran MO
Mingzheng HUANG
Qun ZHANG
Weiyuan TANG
Tingting LI
Cunbin XU
Xiaozhu LIU
Zhihai YU
Xin LI
author_facet Haoran MO
Mingzheng HUANG
Qun ZHANG
Weiyuan TANG
Tingting LI
Cunbin XU
Xiaozhu LIU
Zhihai YU
Xin LI
author_sort Haoran MO
collection DOAJ
description To comprehensively analyze the composition and contribution of volatile components in Rosa sterilis, the headspace solid phase microextraction (HS-SPME) and liquid liquid extraction with solvent assisted flavor evaporation (LLE-SAFE) was used, along with gas chromatography-mass spectrometry (GC-MS) to analyze the volatile components. The odor active value (OAV) was used to evaluate the contribution of volatile components to the overall aroma of R. sterilis juice. The results showed that a total of 115 volatile components were identified using both methods, with 59 identified using HS-SPME and 75 identified using LLE-SAFE. These components included 25 esters, 27 alcohols, 11 aldehydes, 14 ketones, 18 acids, 14 terpenes, and 6 other compounds. Analysis of the odor active value (OAV) showed that 30 volatile components, including isoamyl alcohol, 2-hexenal, ethyl hexanoate, ethyl acetate, butyl acetate, hexanal, and hexanoic acid, contributed strongly to the aroma of R. sterilis. This study provides theoretical support for revealing the aroma profile and chemical essence of R. sterilis.
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spelling doaj.art-05744ffc6f074d068eb1eb04b6fbfd7a2023-10-11T09:18:38ZzhoThe editorial department of Science and Technology of Food IndustryShipin gongye ke-ji1002-03062023-10-01442028929710.13386/j.issn1002-0306.20220903002022090300-20Analysis the Volatiles and Its Aroma Contribution in Rosa Sterilis by HS-SPME and LLE-SAFEHaoran MO0Mingzheng HUANG1Qun ZHANG2Weiyuan TANG3Tingting LI4Cunbin XU5Xiaozhu LIU6Zhihai YU7Xin LI8College of Food & Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang 550003, ChinaCollege of Food & Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang 550003, ChinaCollege of Food & Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang 550003, ChinaCollege of Food & Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang 550003, ChinaCollege of Food & Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang 550003, ChinaCollege of Food & Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang 550003, ChinaCollege of Food & Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang 550003, ChinaCollege of Food & Pharmaceutical Engineering, Guizhou Institute of Technology, Guiyang 550003, ChinaKey Laboratory of Environmental Pollution Monitoring and Disease Control, Ministry of Education, School of Public Health, Guizhou Medical University, Guiyang 550025, ChinaTo comprehensively analyze the composition and contribution of volatile components in Rosa sterilis, the headspace solid phase microextraction (HS-SPME) and liquid liquid extraction with solvent assisted flavor evaporation (LLE-SAFE) was used, along with gas chromatography-mass spectrometry (GC-MS) to analyze the volatile components. The odor active value (OAV) was used to evaluate the contribution of volatile components to the overall aroma of R. sterilis juice. The results showed that a total of 115 volatile components were identified using both methods, with 59 identified using HS-SPME and 75 identified using LLE-SAFE. These components included 25 esters, 27 alcohols, 11 aldehydes, 14 ketones, 18 acids, 14 terpenes, and 6 other compounds. Analysis of the odor active value (OAV) showed that 30 volatile components, including isoamyl alcohol, 2-hexenal, ethyl hexanoate, ethyl acetate, butyl acetate, hexanal, and hexanoic acid, contributed strongly to the aroma of R. sterilis. This study provides theoretical support for revealing the aroma profile and chemical essence of R. sterilis.http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2022090300rosa sterilishs-spmesafeodor active valuearoma contribution
spellingShingle Haoran MO
Mingzheng HUANG
Qun ZHANG
Weiyuan TANG
Tingting LI
Cunbin XU
Xiaozhu LIU
Zhihai YU
Xin LI
Analysis the Volatiles and Its Aroma Contribution in Rosa Sterilis by HS-SPME and LLE-SAFE
Shipin gongye ke-ji
rosa sterilis
hs-spme
safe
odor active value
aroma contribution
title Analysis the Volatiles and Its Aroma Contribution in Rosa Sterilis by HS-SPME and LLE-SAFE
title_full Analysis the Volatiles and Its Aroma Contribution in Rosa Sterilis by HS-SPME and LLE-SAFE
title_fullStr Analysis the Volatiles and Its Aroma Contribution in Rosa Sterilis by HS-SPME and LLE-SAFE
title_full_unstemmed Analysis the Volatiles and Its Aroma Contribution in Rosa Sterilis by HS-SPME and LLE-SAFE
title_short Analysis the Volatiles and Its Aroma Contribution in Rosa Sterilis by HS-SPME and LLE-SAFE
title_sort analysis the volatiles and its aroma contribution in rosa sterilis by hs spme and lle safe
topic rosa sterilis
hs-spme
safe
odor active value
aroma contribution
url http://www.spgykj.com/cn/article/doi/10.13386/j.issn1002-0306.2022090300
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