Characterizing the Soldering Alloy Type In–Ag–Ti and the Study of Direct Soldering of SiC Ceramics and Copper

The aim of the research was to characterize the soldering alloy In–Ag–Ti type, and to study the direct soldering of SiC ceramics and copper. The In10Ag4Ti solder has a broad melting interval, which mainly depends on its silver content. The liquid point of the solder is 256.5 °C. The solder microstru...

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Main Authors: Roman Koleňák, Igor Kostolný, Jaromír Drápala, Martin Sahul, Ján Urminský
Format: Article
Language:English
Published: MDPI AG 2018-04-01
Series:Metals
Subjects:
Online Access:http://www.mdpi.com/2075-4701/8/4/274
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author Roman Koleňák
Igor Kostolný
Jaromír Drápala
Martin Sahul
Ján Urminský
author_facet Roman Koleňák
Igor Kostolný
Jaromír Drápala
Martin Sahul
Ján Urminský
author_sort Roman Koleňák
collection DOAJ
description The aim of the research was to characterize the soldering alloy In–Ag–Ti type, and to study the direct soldering of SiC ceramics and copper. The In10Ag4Ti solder has a broad melting interval, which mainly depends on its silver content. The liquid point of the solder is 256.5 °C. The solder microstructure is composed of a matrix with solid solution (In), in which the phases of titanium (Ti3In4) and silver (AgIn2) are mainly segregated. The tensile strength of the solder is approximately 13 MPa. The strength of the solder increased with the addition of Ag and Ti. The solder bonds with SiC ceramics, owing to the interaction between active In metal and silicon infiltrated in the ceramics. XRD analysis has proven the interaction of titanium with ceramic material during the formation of the new minority phases of titanium silicide—SiTi and titanium carbide—C5Ti8. In and Ag also affect bond formation with the copper substrate. Two new phases were also observed in the bond interphase—(CuAg)6In5 and (AgCu)In2. The average shear strength of a combined joint of SiC–Cu, fabricated with In10Ag4Ti solder, was 14.5 MPa. The In–Ag–Ti solder type studied possesses excellent solderability with several metallic and ceramic materials.
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spelling doaj.art-060a5baa4eed453ca72e8ec056f56c742022-12-22T01:14:16ZengMDPI AGMetals2075-47012018-04-018427410.3390/met8040274met8040274Characterizing the Soldering Alloy Type In–Ag–Ti and the Study of Direct Soldering of SiC Ceramics and CopperRoman Koleňák0Igor Kostolný1Jaromír Drápala2Martin Sahul3Ján Urminský4Faculty of Materials Science and Technology in Trnava, Slovak University of Technology in Bratislava, Jána Bottu č. 2781/25, 917 24 Trnava, SlovakiaFaculty of Materials Science and Technology in Trnava, Slovak University of Technology in Bratislava, Jána Bottu č. 2781/25, 917 24 Trnava, SlovakiaFMMI—Faculty of Metallurgy and Material Engineering, 17. listopadu 15, Poruba, 708 33 Ostrava, Czech RepublicFaculty of Materials Science and Technology in Trnava, Slovak University of Technology in Bratislava, Jána Bottu č. 2781/25, 917 24 Trnava, SlovakiaFaculty of Materials Science and Technology in Trnava, Slovak University of Technology in Bratislava, Jána Bottu č. 2781/25, 917 24 Trnava, SlovakiaThe aim of the research was to characterize the soldering alloy In–Ag–Ti type, and to study the direct soldering of SiC ceramics and copper. The In10Ag4Ti solder has a broad melting interval, which mainly depends on its silver content. The liquid point of the solder is 256.5 °C. The solder microstructure is composed of a matrix with solid solution (In), in which the phases of titanium (Ti3In4) and silver (AgIn2) are mainly segregated. The tensile strength of the solder is approximately 13 MPa. The strength of the solder increased with the addition of Ag and Ti. The solder bonds with SiC ceramics, owing to the interaction between active In metal and silicon infiltrated in the ceramics. XRD analysis has proven the interaction of titanium with ceramic material during the formation of the new minority phases of titanium silicide—SiTi and titanium carbide—C5Ti8. In and Ag also affect bond formation with the copper substrate. Two new phases were also observed in the bond interphase—(CuAg)6In5 and (AgCu)In2. The average shear strength of a combined joint of SiC–Cu, fabricated with In10Ag4Ti solder, was 14.5 MPa. The In–Ag–Ti solder type studied possesses excellent solderability with several metallic and ceramic materials.http://www.mdpi.com/2075-4701/8/4/274solderceramicscopperflux-less soldering
spellingShingle Roman Koleňák
Igor Kostolný
Jaromír Drápala
Martin Sahul
Ján Urminský
Characterizing the Soldering Alloy Type In–Ag–Ti and the Study of Direct Soldering of SiC Ceramics and Copper
Metals
solder
ceramics
copper
flux-less soldering
title Characterizing the Soldering Alloy Type In–Ag–Ti and the Study of Direct Soldering of SiC Ceramics and Copper
title_full Characterizing the Soldering Alloy Type In–Ag–Ti and the Study of Direct Soldering of SiC Ceramics and Copper
title_fullStr Characterizing the Soldering Alloy Type In–Ag–Ti and the Study of Direct Soldering of SiC Ceramics and Copper
title_full_unstemmed Characterizing the Soldering Alloy Type In–Ag–Ti and the Study of Direct Soldering of SiC Ceramics and Copper
title_short Characterizing the Soldering Alloy Type In–Ag–Ti and the Study of Direct Soldering of SiC Ceramics and Copper
title_sort characterizing the soldering alloy type in ag ti and the study of direct soldering of sic ceramics and copper
topic solder
ceramics
copper
flux-less soldering
url http://www.mdpi.com/2075-4701/8/4/274
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