Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry
A new chelating resin, 2-mercaptobenzothiazole loaded Amberlite XAD-1180 was prepared and used for separation and preconcentration of Cd(II) and Pb(II) ions prior to their determinations by flame atomic absorption spectrometry. The optimum pH for simultaneous retention of the elements and the best e...
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| Format: | Article |
| Language: | English |
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Elsevier
2017-01-01
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| Series: | Arabian Journal of Chemistry |
| Subjects: | |
| Online Access: | http://www.sciencedirect.com/science/article/pii/S1878535213001068 |
| _version_ | 1818423005600022528 |
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| author | Şerife Tokalıoğlu Aysel Papak Şenol Kartal |
| author_facet | Şerife Tokalıoğlu Aysel Papak Şenol Kartal |
| author_sort | Şerife Tokalıoğlu |
| collection | DOAJ |
| description | A new chelating resin, 2-mercaptobenzothiazole loaded Amberlite XAD-1180 was prepared and used for separation and preconcentration of Cd(II) and Pb(II) ions prior to their determinations by flame atomic absorption spectrometry. The optimum pH for simultaneous retention of the elements and the best elution means for their simultaneous elution were 9.5 and 2 mol L−1 HNO3, respectively. The detection limits for Cd(II) and Pb(II) were 0.35 and 5.0 μg L−1, respectively. The accuracy of the method was confırmed both by analyzing the certified reference material (RM 8704 Buffalo river sediment) and performing recovery studies. |
| first_indexed | 2024-12-14T13:35:16Z |
| format | Article |
| id | doaj.art-06fbfd5841da4852852a5853ce0c9782 |
| institution | Directory Open Access Journal |
| issn | 1878-5352 |
| language | English |
| last_indexed | 2024-12-14T13:35:16Z |
| publishDate | 2017-01-01 |
| publisher | Elsevier |
| record_format | Article |
| series | Arabian Journal of Chemistry |
| spelling | doaj.art-06fbfd5841da4852852a5853ce0c97822022-12-21T22:59:35ZengElsevierArabian Journal of Chemistry1878-53522017-01-01101192310.1016/j.arabjc.2013.04.017Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometryŞerife TokalıoğluAysel PapakŞenol KartalA new chelating resin, 2-mercaptobenzothiazole loaded Amberlite XAD-1180 was prepared and used for separation and preconcentration of Cd(II) and Pb(II) ions prior to their determinations by flame atomic absorption spectrometry. The optimum pH for simultaneous retention of the elements and the best elution means for their simultaneous elution were 9.5 and 2 mol L−1 HNO3, respectively. The detection limits for Cd(II) and Pb(II) were 0.35 and 5.0 μg L−1, respectively. The accuracy of the method was confırmed both by analyzing the certified reference material (RM 8704 Buffalo river sediment) and performing recovery studies.http://www.sciencedirect.com/science/article/pii/S1878535213001068Preconcentration2-MercaptobenzothiazoleFlame atomic absorption spectrometry |
| spellingShingle | Şerife Tokalıoğlu Aysel Papak Şenol Kartal Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry Arabian Journal of Chemistry Preconcentration 2-Mercaptobenzothiazole Flame atomic absorption spectrometry |
| title | Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry |
| title_full | Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry |
| title_fullStr | Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry |
| title_full_unstemmed | Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry |
| title_short | Separation/preconcentration of trace Pb(II) and Cd(II) with 2-mercaptobenzothiazole impregnated Amberlite XAD-1180 resin and their determination by flame atomic absorption spectrometry |
| title_sort | separation preconcentration of trace pb ii and cd ii with 2 mercaptobenzothiazole impregnated amberlite xad 1180 resin and their determination by flame atomic absorption spectrometry |
| topic | Preconcentration 2-Mercaptobenzothiazole Flame atomic absorption spectrometry |
| url | http://www.sciencedirect.com/science/article/pii/S1878535213001068 |
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