Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4
Lithium Ferro Phosphate Carbon Composite (LFP/C) had been synthesized using solid-state reaction method. Magnetite sand Fe3O4 was used as Fe- source in LFP/C synthesized. Calcination temperature of the sample performed at 400, 500, and 600°C. The phase and composition of samples determined by Rietv...
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| Format: | Article |
| Language: | English |
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University of Brawijaya
2020-04-01
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| Series: | Journal of Pure and Applied Chemistry Research |
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| Online Access: | https://jpacr.ub.ac.id/index.php/jpacr/article/view/517/pdf |
| _version_ | 1818343598972731392 |
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| author | Zuffa Anisa Mochammad Zainuri |
| author_facet | Zuffa Anisa Mochammad Zainuri |
| author_sort | Zuffa Anisa |
| collection | DOAJ |
| description | Lithium Ferro Phosphate Carbon Composite (LFP/C) had been synthesized using solid-state reaction method. Magnetite sand Fe3O4 was used as Fe- source in LFP/C synthesized. Calcination temperature of the sample performed at 400, 500, and 600°C. The phase and composition of samples determined by Rietveld analysis of X-ray diffraction (XRD) pattern. The dominant identified phase at 400°C was diphosphate LiFeP2O7, and the others phases were nasicon Li3Fe2(PO4)3 and hematite Fe2O3. As the temperature getting higher the diphosphate phase LiFeP2O7 transform to nasicon Li3Fe2(PO4)3.The chemical bonds, lattice vibration and other structural features of the sample were investigated using FTIR spectroscopy in range of 1400 – 400 cm-1. Specific vibration modes in LFP-1 to LFP-3 for each bonding were shown by the high intense in certain wavenumber. |
| first_indexed | 2024-12-13T16:33:08Z |
| format | Article |
| id | doaj.art-0717dd2cdaba46209c090234df8f7d1d |
| institution | Directory Open Access Journal |
| issn | 2302-4690 2302-4690 |
| language | English |
| last_indexed | 2024-12-13T16:33:08Z |
| publishDate | 2020-04-01 |
| publisher | University of Brawijaya |
| record_format | Article |
| series | Journal of Pure and Applied Chemistry Research |
| spelling | doaj.art-0717dd2cdaba46209c090234df8f7d1d2022-12-21T23:38:27ZengUniversity of BrawijayaJournal of Pure and Applied Chemistry Research2302-46902302-46902020-04-01911622http://dx.doi.org/10.21776/jpacr.ub.2020.009.01.517Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4Zuffa Anisa0Mochammad Zainuri1Chemistry Department, Faculty of Science and Engineering, University of Bojonegoro Physics Department, Faculty of Mathematic and Sciences, Institute Technology of Sepuluh NopemberLithium Ferro Phosphate Carbon Composite (LFP/C) had been synthesized using solid-state reaction method. Magnetite sand Fe3O4 was used as Fe- source in LFP/C synthesized. Calcination temperature of the sample performed at 400, 500, and 600°C. The phase and composition of samples determined by Rietveld analysis of X-ray diffraction (XRD) pattern. The dominant identified phase at 400°C was diphosphate LiFeP2O7, and the others phases were nasicon Li3Fe2(PO4)3 and hematite Fe2O3. As the temperature getting higher the diphosphate phase LiFeP2O7 transform to nasicon Li3Fe2(PO4)3.The chemical bonds, lattice vibration and other structural features of the sample were investigated using FTIR spectroscopy in range of 1400 – 400 cm-1. Specific vibration modes in LFP-1 to LFP-3 for each bonding were shown by the high intense in certain wavenumber.https://jpacr.ub.ac.id/index.php/jpacr/article/view/517/pdflfp/cmagnetitenasicondiphosphatephase |
| spellingShingle | Zuffa Anisa Mochammad Zainuri Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4 Journal of Pure and Applied Chemistry Research lfp/c magnetite nasicon diphosphate phase |
| title | Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4 |
| title_full | Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4 |
| title_fullStr | Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4 |
| title_full_unstemmed | Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4 |
| title_short | Synthesis and Characterization of Lithium Iron Phosphate Carbon Composite (LFP/C) using Magnetite Sand Fe3O4 |
| title_sort | synthesis and characterization of lithium iron phosphate carbon composite lfp c using magnetite sand fe3o4 |
| topic | lfp/c magnetite nasicon diphosphate phase |
| url | https://jpacr.ub.ac.id/index.php/jpacr/article/view/517/pdf |
| work_keys_str_mv | AT zuffaanisa synthesisandcharacterizationoflithiumironphosphatecarboncompositelfpcusingmagnetitesandfe3o4 AT mochammadzainuri synthesisandcharacterizationoflithiumironphosphatecarboncompositelfpcusingmagnetitesandfe3o4 |