Preparation and Characterization of Electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> Composite Fibers

In this work, the EVOH/Ti<sub>3</sub>C<sub>2</sub> composite fibers were prepared via electrospinning and the effect of added Ti<sub>3</sub>C<sub>2</sub> on the structure and properties of electrospun EVOH fibrous membranes was further investigated. Th...

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Main Authors: Xiang Li, Qiao Xu
Format: Article
Language:English
Published: MDPI AG 2024-02-01
Series:Polymers
Subjects:
Online Access:https://www.mdpi.com/2073-4360/16/5/630
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author Xiang Li
Qiao Xu
author_facet Xiang Li
Qiao Xu
author_sort Xiang Li
collection DOAJ
description In this work, the EVOH/Ti<sub>3</sub>C<sub>2</sub> composite fibers were prepared via electrospinning and the effect of added Ti<sub>3</sub>C<sub>2</sub> on the structure and properties of electrospun EVOH fibrous membranes was further investigated. The morphology, crystal structure, thermal properties, wettability, tensile properties, as well as air permeability and water vapor permeability of as-prepared EVOH/Ti<sub>3</sub>C<sub>2</sub> composite fibers were studied. The Ti<sub>3</sub>C<sub>2</sub> is uniformly loaded onto the surface and inside the composite fiber and affects the fiber diameters. Furthermore, The Ti<sub>3</sub>C<sub>2</sub> self-orients along the fiber axis and does not change the crystal structure of the electrospun EVOH fibers, improving the crystallinity and thermal stability of the electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> fibrous membranes. With the increase in the Ti<sub>3</sub>C<sub>2</sub> concentration in the electrospinning polymer solution, the addition of Ti<sub>3</sub>C<sub>2</sub> not only rapidly improves the wettability of the fibrous membranes, but also enhances their air permeability, compared with the pristine electrospun EVOH fibrous membranes. The experimental results provide theoretical guidance for the preparation of Ti<sub>3</sub>C<sub>2</sub> composite fibers, and also expand the application of electrospun EVOH and EVOH/Ti<sub>3</sub>C<sub>2</sub> fibrous membranes.
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spelling doaj.art-075125464852429399714b03e23c1f2e2024-03-12T16:53:29ZengMDPI AGPolymers2073-43602024-02-0116563010.3390/polym16050630Preparation and Characterization of Electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> Composite FibersXiang Li0Qiao Xu1Key Laboratory of Functional Fibers and Intelligent Textiles, Yuanpei College, Shaoxing University, Shaoxing 312000, ChinaKey Laboratory of Functional Fibers and Intelligent Textiles, Yuanpei College, Shaoxing University, Shaoxing 312000, ChinaIn this work, the EVOH/Ti<sub>3</sub>C<sub>2</sub> composite fibers were prepared via electrospinning and the effect of added Ti<sub>3</sub>C<sub>2</sub> on the structure and properties of electrospun EVOH fibrous membranes was further investigated. The morphology, crystal structure, thermal properties, wettability, tensile properties, as well as air permeability and water vapor permeability of as-prepared EVOH/Ti<sub>3</sub>C<sub>2</sub> composite fibers were studied. The Ti<sub>3</sub>C<sub>2</sub> is uniformly loaded onto the surface and inside the composite fiber and affects the fiber diameters. Furthermore, The Ti<sub>3</sub>C<sub>2</sub> self-orients along the fiber axis and does not change the crystal structure of the electrospun EVOH fibers, improving the crystallinity and thermal stability of the electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> fibrous membranes. With the increase in the Ti<sub>3</sub>C<sub>2</sub> concentration in the electrospinning polymer solution, the addition of Ti<sub>3</sub>C<sub>2</sub> not only rapidly improves the wettability of the fibrous membranes, but also enhances their air permeability, compared with the pristine electrospun EVOH fibrous membranes. The experimental results provide theoretical guidance for the preparation of Ti<sub>3</sub>C<sub>2</sub> composite fibers, and also expand the application of electrospun EVOH and EVOH/Ti<sub>3</sub>C<sub>2</sub> fibrous membranes.https://www.mdpi.com/2073-4360/16/5/630EVOHTi<sub>3</sub>C<sub>2</sub>electrospinningstructureproperties
spellingShingle Xiang Li
Qiao Xu
Preparation and Characterization of Electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> Composite Fibers
Polymers
EVOH
Ti<sub>3</sub>C<sub>2</sub>
electrospinning
structure
properties
title Preparation and Characterization of Electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> Composite Fibers
title_full Preparation and Characterization of Electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> Composite Fibers
title_fullStr Preparation and Characterization of Electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> Composite Fibers
title_full_unstemmed Preparation and Characterization of Electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> Composite Fibers
title_short Preparation and Characterization of Electrospun EVOH/Ti<sub>3</sub>C<sub>2</sub> Composite Fibers
title_sort preparation and characterization of electrospun evoh ti sub 3 sub c sub 2 sub composite fibers
topic EVOH
Ti<sub>3</sub>C<sub>2</sub>
electrospinning
structure
properties
url https://www.mdpi.com/2073-4360/16/5/630
work_keys_str_mv AT xiangli preparationandcharacterizationofelectrospunevohtisub3subcsub2subcompositefibers
AT qiaoxu preparationandcharacterizationofelectrospunevohtisub3subcsub2subcompositefibers