Influence of synthesis parameters on mechanical properties of nanocomposite PMMA-MXene
In this paper, the influence of solvents and reinforcement processing methods on the mechanical properties of nanocomposite poly-(methyl methacrylate) PMMA-Ti3C2Tx MXene was investigated. A weight fraction of reinforcement was 1% and two types of solvents were used for sample preparation: dimethylfo...
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| Format: | Article |
| Language: | English |
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Savez inženjera i tehničara Srbije
2021-01-01
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| Series: | Tehnika |
| Subjects: | |
| Online Access: | https://scindeks-clanci.ceon.rs/data/pdf/0040-2176/2021/0040-21762105545P.pdf |
| _version_ | 1818574705924243456 |
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| author | Pešić Ivan D. Petrović Miloš M. Radojević Vesna J. |
| author_facet | Pešić Ivan D. Petrović Miloš M. Radojević Vesna J. |
| author_sort | Pešić Ivan D. |
| collection | DOAJ |
| description | In this paper, the influence of solvents and reinforcement processing methods on the mechanical properties of nanocomposite poly-(methyl methacrylate) PMMA-Ti3C2Tx MXene was investigated. A weight fraction of reinforcement was 1% and two types of solvents were used for sample preparation: dimethylformamide (DMF) and acetone (Ac). Deionized water and DMF were used to delaminate the MXene. An additional peak at 1675 cm-1 was observed on the FTIR spectra of the obtained samples, which indicates that some amount of DMF remained in the material after drying. The results of microindentation show that samples where MXene was delaminated in deionized water and PMMA dissolved in acetone had a 74.46% higher reduced modulus of elasticity, which is supported by SEM images where better dispersion of MXenes is observed. |
| first_indexed | 2024-12-15T00:30:06Z |
| format | Article |
| id | doaj.art-075a8ca5060849929813a2035a863689 |
| institution | Directory Open Access Journal |
| issn | 0040-2176 2560-3086 |
| language | English |
| last_indexed | 2024-12-15T00:30:06Z |
| publishDate | 2021-01-01 |
| publisher | Savez inženjera i tehničara Srbije |
| record_format | Article |
| series | Tehnika |
| spelling | doaj.art-075a8ca5060849929813a2035a8636892022-12-21T22:42:02ZengSavez inženjera i tehničara SrbijeTehnika0040-21762560-30862021-01-0176554554910.5937/tehnika2105545P0040-21762105545PInfluence of synthesis parameters on mechanical properties of nanocomposite PMMA-MXenePešić Ivan D.0Petrović Miloš M.1https://orcid.org/0000-0003-2597-4023Radojević Vesna J.2https://orcid.org/0000-0001-9301-3983Univerzitet u Beogradu, Tehnološko-metalurški fakultet, SerbiaUniverzitet u Beogradu, Tehnološko-metalurški fakultet, SerbiaUniverzitet u Beogradu, Tehnološko-metalurški fakultet, SerbiaIn this paper, the influence of solvents and reinforcement processing methods on the mechanical properties of nanocomposite poly-(methyl methacrylate) PMMA-Ti3C2Tx MXene was investigated. A weight fraction of reinforcement was 1% and two types of solvents were used for sample preparation: dimethylformamide (DMF) and acetone (Ac). Deionized water and DMF were used to delaminate the MXene. An additional peak at 1675 cm-1 was observed on the FTIR spectra of the obtained samples, which indicates that some amount of DMF remained in the material after drying. The results of microindentation show that samples where MXene was delaminated in deionized water and PMMA dissolved in acetone had a 74.46% higher reduced modulus of elasticity, which is supported by SEM images where better dispersion of MXenes is observed.https://scindeks-clanci.ceon.rs/data/pdf/0040-2176/2021/0040-21762105545P.pdfsolventnanocompositepmmamxenemicrohardness |
| spellingShingle | Pešić Ivan D. Petrović Miloš M. Radojević Vesna J. Influence of synthesis parameters on mechanical properties of nanocomposite PMMA-MXene Tehnika solvent nanocomposite pmma mxene microhardness |
| title | Influence of synthesis parameters on mechanical properties of nanocomposite PMMA-MXene |
| title_full | Influence of synthesis parameters on mechanical properties of nanocomposite PMMA-MXene |
| title_fullStr | Influence of synthesis parameters on mechanical properties of nanocomposite PMMA-MXene |
| title_full_unstemmed | Influence of synthesis parameters on mechanical properties of nanocomposite PMMA-MXene |
| title_short | Influence of synthesis parameters on mechanical properties of nanocomposite PMMA-MXene |
| title_sort | influence of synthesis parameters on mechanical properties of nanocomposite pmma mxene |
| topic | solvent nanocomposite pmma mxene microhardness |
| url | https://scindeks-clanci.ceon.rs/data/pdf/0040-2176/2021/0040-21762105545P.pdf |
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