Isolation of cellulose microfibrils - An enzymatic approach

Isolation methods and applications of cellulose microfibrils are expanding rapidly due to environmental benefits and specific strength properties, especially in bio-composite science. In this research, we have success-fully developed and explored a novel bio-pretreatment for wood fibre that can subs...

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Main Authors: Sain, M., Janardhnan, S., and
Format: Article
Language:English
Published: North Carolina State University 2006-11-01
Series:BioResources
Subjects:
Online Access:http://ojs.cnr.ncsu.edu/index.php/BioRes/article/viewFile/BioRes_01_2_176_188_Janardnan_Sain_Isoluation_Cellulose_Microfibrils_Enzymatic/18
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author Sain, M.
Janardhnan, S., and
author_facet Sain, M.
Janardhnan, S., and
author_sort Sain, M.
collection DOAJ
description Isolation methods and applications of cellulose microfibrils are expanding rapidly due to environmental benefits and specific strength properties, especially in bio-composite science. In this research, we have success-fully developed and explored a novel bio-pretreatment for wood fibre that can substantially improve the microfibril yield, in comparison to current techniques used to isolate cellulose microfibrils. Microfibrils currently are isolated in the laboratory through a combination of high shear refining and cryocrushing. A high energy requirement of these procedures is hampering momentum in the direction of microfibril isolation on a sufficiently large scale to suit potential applications. Any attempt to loosen up the microfibrils by either complete or partial destruction of the hydrogen bonds before the mechanical process would be a step forward in the quest for economical isolation of cellulose microfibrils. Bleached kraft pulp was treated with OS1, a fungus isolated from Dutch Elm trees infected with Dutch elm disease, under different treatment conditions. The percentage yield of cellulose microfibrils, based on their diameter, showed a significant shift towards a lower diameter range after the high shear refining, compared to the yield of cellulose microfibrils from untreated fibres. The overall yield of cellulose microfibrils from the treated fibres did not show any sizeable decrease.
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spelling doaj.art-086a015b8c6047cd82204ec7432edbae2022-12-22T00:38:37ZengNorth Carolina State UniversityBioResources1930-21262006-11-0112176188Isolation of cellulose microfibrils - An enzymatic approachSain, M.Janardhnan, S., andIsolation methods and applications of cellulose microfibrils are expanding rapidly due to environmental benefits and specific strength properties, especially in bio-composite science. In this research, we have success-fully developed and explored a novel bio-pretreatment for wood fibre that can substantially improve the microfibril yield, in comparison to current techniques used to isolate cellulose microfibrils. Microfibrils currently are isolated in the laboratory through a combination of high shear refining and cryocrushing. A high energy requirement of these procedures is hampering momentum in the direction of microfibril isolation on a sufficiently large scale to suit potential applications. Any attempt to loosen up the microfibrils by either complete or partial destruction of the hydrogen bonds before the mechanical process would be a step forward in the quest for economical isolation of cellulose microfibrils. Bleached kraft pulp was treated with OS1, a fungus isolated from Dutch Elm trees infected with Dutch elm disease, under different treatment conditions. The percentage yield of cellulose microfibrils, based on their diameter, showed a significant shift towards a lower diameter range after the high shear refining, compared to the yield of cellulose microfibrils from untreated fibres. The overall yield of cellulose microfibrils from the treated fibres did not show any sizeable decrease.http://ojs.cnr.ncsu.edu/index.php/BioRes/article/viewFile/BioRes_01_2_176_188_Janardnan_Sain_Isoluation_Cellulose_Microfibrils_Enzymatic/18CelluloseCellulose microfibrilsFungal / Enzyme pretreatmentCellulose microfibrils isolationHydrogen bonds
spellingShingle Sain, M.
Janardhnan, S., and
Isolation of cellulose microfibrils - An enzymatic approach
BioResources
Cellulose
Cellulose microfibrils
Fungal / Enzyme pretreatment
Cellulose microfibrils isolation
Hydrogen bonds
title Isolation of cellulose microfibrils - An enzymatic approach
title_full Isolation of cellulose microfibrils - An enzymatic approach
title_fullStr Isolation of cellulose microfibrils - An enzymatic approach
title_full_unstemmed Isolation of cellulose microfibrils - An enzymatic approach
title_short Isolation of cellulose microfibrils - An enzymatic approach
title_sort isolation of cellulose microfibrils an enzymatic approach
topic Cellulose
Cellulose microfibrils
Fungal / Enzyme pretreatment
Cellulose microfibrils isolation
Hydrogen bonds
url http://ojs.cnr.ncsu.edu/index.php/BioRes/article/viewFile/BioRes_01_2_176_188_Janardnan_Sain_Isoluation_Cellulose_Microfibrils_Enzymatic/18
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