High-temperature tensile and thermal shock characterization of low-temperature rolled tungsten

A developed tungsten (W) grade was prepared by powder metallurgy technology plus multi-step low-temperature rolling. The relative density, thermal conductivity, microstructure, tensile properties of original and high-temperature annealed states, micro-hardness and transient thermal shock resistance...

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Main Authors: Xiaolei Ma, Xiaoxin Zhang, Fan Feng, Ting Wang, Xiang Liu, Jianbao Wang, Wei Lv, Shaoting Lang, Changchun Ge, Qingzhi Yan
Format: Article
Language:English
Published: Elsevier 2023-03-01
Series:Nuclear Materials and Energy
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2352179122002344
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author Xiaolei Ma
Xiaoxin Zhang
Fan Feng
Ting Wang
Xiang Liu
Jianbao Wang
Wei Lv
Shaoting Lang
Changchun Ge
Qingzhi Yan
author_facet Xiaolei Ma
Xiaoxin Zhang
Fan Feng
Ting Wang
Xiang Liu
Jianbao Wang
Wei Lv
Shaoting Lang
Changchun Ge
Qingzhi Yan
author_sort Xiaolei Ma
collection DOAJ
description A developed tungsten (W) grade was prepared by powder metallurgy technology plus multi-step low-temperature rolling. The relative density, thermal conductivity, microstructure, tensile properties of original and high-temperature annealed states, micro-hardness and transient thermal shock resistance were characterized. The results of tensile test with a strain rate of 2 × 10-4 s−1 show that the ductile–brittle transition temperature (DBTT) of rolled-W in the original and recrystallized state are 150–200 °C and 250–300 °C, respectively. The rolled-W presents high strength and great plasticity simultaneously. For example, the maximum ultimate tensile strength (UTS) below DBTT is as high as ∼ 1189 MPa, and the maximum total elongation (TE) above DBTT reaches 28.9 %. In particular, the TE of recrystallized W achieves an incredible 81.4 % at 500 °C, which is the highest value among all the published literatures so far. The results of transient thermal shock tests indicate that the rolled-W has an outstanding transient thermal shock resistance. It can withstand the thermal bombardment at an absorbed power densities (APD) of 0.33 GW·m−2 without causing any surface damages, and still no cracks are observed as the APD rises to 0.88 GW·m−2. Moreover, the failure mechanism of rolled-W was also studied in details. This work plays an important role in establishing a dependable China Fusion Engineering Test Reactor (CFETR) data-library on a unitary W grade, which can provide an effective reference for the identification of material performance under the high heat flux and subsequent numerical simulation.
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spelling doaj.art-08705cddf8354d238c86a50a021e8ebc2023-03-12T04:21:25ZengElsevierNuclear Materials and Energy2352-17912023-03-0134101353High-temperature tensile and thermal shock characterization of low-temperature rolled tungstenXiaolei Ma0Xiaoxin Zhang1Fan Feng2Ting Wang3Xiang Liu4Jianbao Wang5Wei Lv6Shaoting Lang7Changchun Ge8Qingzhi Yan9Institute of Nuclear Materials, School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, ChinaInstitute of Nuclear Materials, School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China; Corresponding authors.Southwestern Institute of Physics, Chengdu, Sichuan 610041, ChinaSchool of Physics, Beihang University, Beijing, 100191, ChinaSouthwestern Institute of Physics, Chengdu, Sichuan 610041, ChinaSouthwestern Institute of Physics, Chengdu, Sichuan 610041, ChinaInstitute for Advanced Materials, North China Electric Power University, Beijing 102206, ChinaMechanical and Electrical Engineering, Xinxiang University, Xinxiang, Henan 453000,ChinaInstitute of Nuclear Materials, School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, ChinaInstitute of Nuclear Materials, School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China; Corresponding authors.A developed tungsten (W) grade was prepared by powder metallurgy technology plus multi-step low-temperature rolling. The relative density, thermal conductivity, microstructure, tensile properties of original and high-temperature annealed states, micro-hardness and transient thermal shock resistance were characterized. The results of tensile test with a strain rate of 2 × 10-4 s−1 show that the ductile–brittle transition temperature (DBTT) of rolled-W in the original and recrystallized state are 150–200 °C and 250–300 °C, respectively. The rolled-W presents high strength and great plasticity simultaneously. For example, the maximum ultimate tensile strength (UTS) below DBTT is as high as ∼ 1189 MPa, and the maximum total elongation (TE) above DBTT reaches 28.9 %. In particular, the TE of recrystallized W achieves an incredible 81.4 % at 500 °C, which is the highest value among all the published literatures so far. The results of transient thermal shock tests indicate that the rolled-W has an outstanding transient thermal shock resistance. It can withstand the thermal bombardment at an absorbed power densities (APD) of 0.33 GW·m−2 without causing any surface damages, and still no cracks are observed as the APD rises to 0.88 GW·m−2. Moreover, the failure mechanism of rolled-W was also studied in details. This work plays an important role in establishing a dependable China Fusion Engineering Test Reactor (CFETR) data-library on a unitary W grade, which can provide an effective reference for the identification of material performance under the high heat flux and subsequent numerical simulation.http://www.sciencedirect.com/science/article/pii/S2352179122002344Rolled tungstenMicrostructureMechanical propertiesTransient thermal shock
spellingShingle Xiaolei Ma
Xiaoxin Zhang
Fan Feng
Ting Wang
Xiang Liu
Jianbao Wang
Wei Lv
Shaoting Lang
Changchun Ge
Qingzhi Yan
High-temperature tensile and thermal shock characterization of low-temperature rolled tungsten
Nuclear Materials and Energy
Rolled tungsten
Microstructure
Mechanical properties
Transient thermal shock
title High-temperature tensile and thermal shock characterization of low-temperature rolled tungsten
title_full High-temperature tensile and thermal shock characterization of low-temperature rolled tungsten
title_fullStr High-temperature tensile and thermal shock characterization of low-temperature rolled tungsten
title_full_unstemmed High-temperature tensile and thermal shock characterization of low-temperature rolled tungsten
title_short High-temperature tensile and thermal shock characterization of low-temperature rolled tungsten
title_sort high temperature tensile and thermal shock characterization of low temperature rolled tungsten
topic Rolled tungsten
Microstructure
Mechanical properties
Transient thermal shock
url http://www.sciencedirect.com/science/article/pii/S2352179122002344
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