Optimization of a divided wall column for the separation of C4-C6 normal paraffin mixture using Box-Behnken design

In the present study, simulation of a divided wall column (DWC) was carried out to study the product quality and energy efficiency as a function of reflux rate, liquid spilt and vapour split for the separation of C4-C6 normal paraffin ternary mixture. Rigorous simulation of the DWC was carried ou...

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Main Authors: Sangal Vikas K., Kumar Vineet, Mishra Mani Indra
Format: Article
Language:English
Published: Association of the Chemical Engineers of Serbia 2013-01-01
Series:Chemical Industry and Chemical Engineering Quarterly
Subjects:
Online Access:http://www.doiserbia.nb.rs/img/doi/1451-9372/2013/1451-93721200047S.pdf
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author Sangal Vikas K.
Kumar Vineet
Mishra Mani Indra
author_facet Sangal Vikas K.
Kumar Vineet
Mishra Mani Indra
author_sort Sangal Vikas K.
collection DOAJ
description In the present study, simulation of a divided wall column (DWC) was carried out to study the product quality and energy efficiency as a function of reflux rate, liquid spilt and vapour split for the separation of C4-C6 normal paraffin ternary mixture. Rigorous simulation of the DWC was carried out using Multifrac model of ASPEN Plus software. Box-Behnken design (BBD) was used for the optimization of parameters and to evaluate the effects and interaction of the process parameters such as reflux rate (r), liquid split (l) and vapour split (v). It was found that the number of simulation runs reduced significantly for the optimization of DWC by BBD. Optimization by BBD under response surface methodology (RSM) vividly underscores interactions between variables and their effects. The predictions agree well with the results of the rigorous simulation.
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spelling doaj.art-08e4601e7dba4fd487ae5ff9efce41052022-12-22T01:15:20ZengAssociation of the Chemical Engineers of SerbiaChemical Industry and Chemical Engineering Quarterly1451-93722217-74342013-01-0119110711910.2298/CICEQ121019047SOptimization of a divided wall column for the separation of C4-C6 normal paraffin mixture using Box-Behnken designSangal Vikas K.Kumar VineetMishra Mani IndraIn the present study, simulation of a divided wall column (DWC) was carried out to study the product quality and energy efficiency as a function of reflux rate, liquid spilt and vapour split for the separation of C4-C6 normal paraffin ternary mixture. Rigorous simulation of the DWC was carried out using Multifrac model of ASPEN Plus software. Box-Behnken design (BBD) was used for the optimization of parameters and to evaluate the effects and interaction of the process parameters such as reflux rate (r), liquid split (l) and vapour split (v). It was found that the number of simulation runs reduced significantly for the optimization of DWC by BBD. Optimization by BBD under response surface methodology (RSM) vividly underscores interactions between variables and their effects. The predictions agree well with the results of the rigorous simulation.http://www.doiserbia.nb.rs/img/doi/1451-9372/2013/1451-93721200047S.pdfDivided wall column (DWC)Box-Behnken design (BBD)Energy efficiencyResponse surface methodology (RSM)Separation of C4-C6 normal paraffin ternary mixture
spellingShingle Sangal Vikas K.
Kumar Vineet
Mishra Mani Indra
Optimization of a divided wall column for the separation of C4-C6 normal paraffin mixture using Box-Behnken design
Chemical Industry and Chemical Engineering Quarterly
Divided wall column (DWC)
Box-Behnken design (BBD)
Energy efficiency
Response surface methodology (RSM)
Separation of C4-C6 normal paraffin ternary mixture
title Optimization of a divided wall column for the separation of C4-C6 normal paraffin mixture using Box-Behnken design
title_full Optimization of a divided wall column for the separation of C4-C6 normal paraffin mixture using Box-Behnken design
title_fullStr Optimization of a divided wall column for the separation of C4-C6 normal paraffin mixture using Box-Behnken design
title_full_unstemmed Optimization of a divided wall column for the separation of C4-C6 normal paraffin mixture using Box-Behnken design
title_short Optimization of a divided wall column for the separation of C4-C6 normal paraffin mixture using Box-Behnken design
title_sort optimization of a divided wall column for the separation of c4 c6 normal paraffin mixture using box behnken design
topic Divided wall column (DWC)
Box-Behnken design (BBD)
Energy efficiency
Response surface methodology (RSM)
Separation of C4-C6 normal paraffin ternary mixture
url http://www.doiserbia.nb.rs/img/doi/1451-9372/2013/1451-93721200047S.pdf
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