Structural investigations of Fe-Zr-Si-Cu metallic glass with low glass-forming ability produced in laser powder bed fusion technology

Fe-based metallic glasses (MG) have become the subject of extensive research in recent years due to their favorable mechanical and magnetic properties. In particular, the production of this type of materials in Laser Powder Bed Fusion (LPBF), also known as Selective Laser Melting (SLM) technology, i...

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Main Authors: Łukasz Szczepański, Markus Bambach, Felix Jensch, Andrzej Ambroziak, Tomasz Kurzynowski
Format: Article
Language:English
Published: Elsevier 2021-11-01
Series:Materials & Design
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S0264127521006675
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author Łukasz Szczepański
Markus Bambach
Felix Jensch
Andrzej Ambroziak
Tomasz Kurzynowski
author_facet Łukasz Szczepański
Markus Bambach
Felix Jensch
Andrzej Ambroziak
Tomasz Kurzynowski
author_sort Łukasz Szczepański
collection DOAJ
description Fe-based metallic glasses (MG) have become the subject of extensive research in recent years due to their favorable mechanical and magnetic properties. In particular, the production of this type of materials in Laser Powder Bed Fusion (LPBF), also known as Selective Laser Melting (SLM) technology, is a kind of breakthrough, as it has become possible to produce elements of any shape. An important factor influencing the properties of the manufactured parts is their microstructure. For metallic glass Fe79Zr6Si14Cu1 with low glass-forming ability, produced in SLM technology, tests were carried out in the field of structural X-ray diffraction, Scanning Electron Microscopy, and Transmission Electron Microscopy. In addition, porosity analysis was compared with process parameters such as laser power and scanning speed. The paper shows that the fusion line comprises a solid solution α-Fe(Si) and low fraction of intermetallic Fe23Zr6 and FeZr2 phases. Furthermore, in the melt pool area, a nanometric α-Fe(Si) phase and an amorphous matrix was observed. The presented research results of the Fe79Zr6Si14Cu1 alloy produced for the first time in SLM technology will undoubtendly contribute to further optimization of parameters for elements produced in Additive Manufacturing technology using Fe-based MG.
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spelling doaj.art-08f3dfe4f12a4a7faa425a5e3818380a2022-12-21T19:54:00ZengElsevierMaterials & Design0264-12752021-11-01210110112Structural investigations of Fe-Zr-Si-Cu metallic glass with low glass-forming ability produced in laser powder bed fusion technologyŁukasz Szczepański0Markus Bambach1Felix Jensch2Andrzej Ambroziak3Tomasz Kurzynowski4Wroclaw University of Science and Technology, Wybrzeże Wyspiańskiego 27, 50-370 Wroclaw, Poland; Corresponding author.Swiss Federal Institute of Technology in Zurich, Rämistrasse 101, 8092 Zürich, SwitzerlandBrandenburg University of Technology Cottbus – Senftenberg, Platz der Deutschen Einheit 1, 03046 Cottbus, GermanyWroclaw University of Science and Technology, Wybrzeże Wyspiańskiego 27, 50-370 Wroclaw, PolandWroclaw University of Science and Technology, Wybrzeże Wyspiańskiego 27, 50-370 Wroclaw, PolandFe-based metallic glasses (MG) have become the subject of extensive research in recent years due to their favorable mechanical and magnetic properties. In particular, the production of this type of materials in Laser Powder Bed Fusion (LPBF), also known as Selective Laser Melting (SLM) technology, is a kind of breakthrough, as it has become possible to produce elements of any shape. An important factor influencing the properties of the manufactured parts is their microstructure. For metallic glass Fe79Zr6Si14Cu1 with low glass-forming ability, produced in SLM technology, tests were carried out in the field of structural X-ray diffraction, Scanning Electron Microscopy, and Transmission Electron Microscopy. In addition, porosity analysis was compared with process parameters such as laser power and scanning speed. The paper shows that the fusion line comprises a solid solution α-Fe(Si) and low fraction of intermetallic Fe23Zr6 and FeZr2 phases. Furthermore, in the melt pool area, a nanometric α-Fe(Si) phase and an amorphous matrix was observed. The presented research results of the Fe79Zr6Si14Cu1 alloy produced for the first time in SLM technology will undoubtendly contribute to further optimization of parameters for elements produced in Additive Manufacturing technology using Fe-based MG.http://www.sciencedirect.com/science/article/pii/S0264127521006675Selective Laser MeltingFe-based metallic glassLow glass-forming abilityMicrostructureTransmission electron microscopy
spellingShingle Łukasz Szczepański
Markus Bambach
Felix Jensch
Andrzej Ambroziak
Tomasz Kurzynowski
Structural investigations of Fe-Zr-Si-Cu metallic glass with low glass-forming ability produced in laser powder bed fusion technology
Materials & Design
Selective Laser Melting
Fe-based metallic glass
Low glass-forming ability
Microstructure
Transmission electron microscopy
title Structural investigations of Fe-Zr-Si-Cu metallic glass with low glass-forming ability produced in laser powder bed fusion technology
title_full Structural investigations of Fe-Zr-Si-Cu metallic glass with low glass-forming ability produced in laser powder bed fusion technology
title_fullStr Structural investigations of Fe-Zr-Si-Cu metallic glass with low glass-forming ability produced in laser powder bed fusion technology
title_full_unstemmed Structural investigations of Fe-Zr-Si-Cu metallic glass with low glass-forming ability produced in laser powder bed fusion technology
title_short Structural investigations of Fe-Zr-Si-Cu metallic glass with low glass-forming ability produced in laser powder bed fusion technology
title_sort structural investigations of fe zr si cu metallic glass with low glass forming ability produced in laser powder bed fusion technology
topic Selective Laser Melting
Fe-based metallic glass
Low glass-forming ability
Microstructure
Transmission electron microscopy
url http://www.sciencedirect.com/science/article/pii/S0264127521006675
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