Dispersive liquid-liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determination

In the proposed method, carbon tetrachloride and ethanol were used as extraction and dispersive solvents. Several factors that may be affected on the extraction process, such as extraction solvent, disperser solvent, the volume of extraction and disperser solvent, pH of the aqueous solution and extr...

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Main Authors: Sayed Zia Mohammadi, Yar Mohammad Baghelani, Fatemeh Mansori, Tayebeh Shamspur, Daryoush Afzali
Format: Article
Language:English
Published: Sociedade Brasileira de Química 2012-01-01
Series:Química Nova
Subjects:
Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422012000100034&lng=en&tlng=en
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author Sayed Zia Mohammadi
Yar Mohammad Baghelani
Fatemeh Mansori
Tayebeh Shamspur
Daryoush Afzali
author_facet Sayed Zia Mohammadi
Yar Mohammad Baghelani
Fatemeh Mansori
Tayebeh Shamspur
Daryoush Afzali
author_sort Sayed Zia Mohammadi
collection DOAJ
description In the proposed method, carbon tetrachloride and ethanol were used as extraction and dispersive solvents. Several factors that may be affected on the extraction process, such as extraction solvent, disperser solvent, the volume of extraction and disperser solvent, pH of the aqueous solution and extraction time were optimized. Under the optimal conditions, linearity was maintained between 1.0 ng mL-1 to 1.5 mg mL-1 for zinc and 1.0 ng mL-1 to 0.4 mg mL-1 for cadmium. The proposed method has been applied for determination of trace amount of zinc and cadmium in standard and water samples with satisfactory results.
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spelling doaj.art-09a87cebc1d14e879804a42fe11a6af12022-12-22T03:37:17ZengSociedade Brasileira de QuímicaQuímica Nova1678-70642012-01-0135119820210.1590/S0100-40422012000100034S0100-40422012000100034Dispersive liquid-liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determinationSayed Zia Mohammadi0Yar Mohammad Baghelani1Fatemeh Mansori2Tayebeh Shamspur3Daryoush Afzali4Payame Noor UniversityPayame Noor UniversityPayame Noor UniversityShahid Bahonar University of KermanInternational Center for Science, High Technology & Environmental SciencesIn the proposed method, carbon tetrachloride and ethanol were used as extraction and dispersive solvents. Several factors that may be affected on the extraction process, such as extraction solvent, disperser solvent, the volume of extraction and disperser solvent, pH of the aqueous solution and extraction time were optimized. Under the optimal conditions, linearity was maintained between 1.0 ng mL-1 to 1.5 mg mL-1 for zinc and 1.0 ng mL-1 to 0.4 mg mL-1 for cadmium. The proposed method has been applied for determination of trace amount of zinc and cadmium in standard and water samples with satisfactory results.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422012000100034&lng=en&tlng=endispersive liquid-liquid microextractioncadmium determinationzinc determination
spellingShingle Sayed Zia Mohammadi
Yar Mohammad Baghelani
Fatemeh Mansori
Tayebeh Shamspur
Daryoush Afzali
Dispersive liquid-liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determination
Química Nova
dispersive liquid-liquid microextraction
cadmium determination
zinc determination
title Dispersive liquid-liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determination
title_full Dispersive liquid-liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determination
title_fullStr Dispersive liquid-liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determination
title_full_unstemmed Dispersive liquid-liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determination
title_short Dispersive liquid-liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determination
title_sort dispersive liquid liquid microextraction for the simultaneous separation of trace amounts of zinc and cadmium ions in water samples prior to flame atomic absorption spectrometry determination
topic dispersive liquid-liquid microextraction
cadmium determination
zinc determination
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422012000100034&lng=en&tlng=en
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