The Surface Characteristics, Microstructure and Mechanical Properties of PEEK Printed by Fused Deposition Modeling with Different Raster Angles

Additive manufacturing provides a novel and robust way to prepare medical product with anatomic matched geometry and tailored mechanical performance. In this study, the surface characteristics, microstructure, and mechanical properties of fused deposition modeling (FDM) prepared polyether-ether-keto...

Full description

Bibliographic Details
Main Authors: Sasa Gao, Ruijuan Liu, Hua Xin, Haitao Liang, Yunfei Wang, Junhong Jia
Format: Article
Language:English
Published: MDPI AG 2021-12-01
Series:Polymers
Subjects:
Online Access:https://www.mdpi.com/2073-4360/14/1/77
_version_ 1797497822513201152
author Sasa Gao
Ruijuan Liu
Hua Xin
Haitao Liang
Yunfei Wang
Junhong Jia
author_facet Sasa Gao
Ruijuan Liu
Hua Xin
Haitao Liang
Yunfei Wang
Junhong Jia
author_sort Sasa Gao
collection DOAJ
description Additive manufacturing provides a novel and robust way to prepare medical product with anatomic matched geometry and tailored mechanical performance. In this study, the surface characteristics, microstructure, and mechanical properties of fused deposition modeling (FDM) prepared polyether-ether-ketone (PEEK) were systematically studied. During the FDM process, the crystal unit cell and thermal attribute of PEEK material remained unchanged, whereas the surface layer generally became more hydrophilic with an obvious reduction in surface hardness. Raster angle has a significant effect on the mechanical strength but not on the failure mechanism. In practice, FDM fabricated PEEK acted more like a laminate rather than a unified structure. Its main failure mechanism was correlated to the internal voids. The results show that horizontal infill orientation with 30° raster angle is promising for a better comprehensive mechanical performance, and the corresponding tensile, flexural, and shear strengths are (76.5 ± 1.4) MPa, (149.7 ± 3.0) MPa, and (55.5 ± 1.8) MPa, respectively. The findings of this study provide guidelines for FDM-PEEK to enable its realization in applications such as orthopedic implants.
first_indexed 2024-03-10T03:24:43Z
format Article
id doaj.art-09edb52a8d3c425dab5943ab6c6b19a1
institution Directory Open Access Journal
issn 2073-4360
language English
last_indexed 2024-03-10T03:24:43Z
publishDate 2021-12-01
publisher MDPI AG
record_format Article
series Polymers
spelling doaj.art-09edb52a8d3c425dab5943ab6c6b19a12023-11-23T12:09:30ZengMDPI AGPolymers2073-43602021-12-011417710.3390/polym14010077The Surface Characteristics, Microstructure and Mechanical Properties of PEEK Printed by Fused Deposition Modeling with Different Raster AnglesSasa Gao0Ruijuan Liu1Hua Xin2Haitao Liang3Yunfei Wang4Junhong Jia5College of Mechanical & Electrical Engineering, Shaanxi University of Science & Technology, Xi’an 710021, ChinaCollege of Mechanical & Electrical Engineering, Shaanxi University of Science & Technology, Xi’an 710021, ChinaCollege of Mechanical & Electrical Engineering, Shaanxi University of Science & Technology, Xi’an 710021, ChinaCollege of Mechanical & Electrical Engineering, Shaanxi University of Science & Technology, Xi’an 710021, ChinaCollege of Mechanical & Electrical Engineering, Shaanxi University of Science & Technology, Xi’an 710021, ChinaCollege of Mechanical & Electrical Engineering, Shaanxi University of Science & Technology, Xi’an 710021, ChinaAdditive manufacturing provides a novel and robust way to prepare medical product with anatomic matched geometry and tailored mechanical performance. In this study, the surface characteristics, microstructure, and mechanical properties of fused deposition modeling (FDM) prepared polyether-ether-ketone (PEEK) were systematically studied. During the FDM process, the crystal unit cell and thermal attribute of PEEK material remained unchanged, whereas the surface layer generally became more hydrophilic with an obvious reduction in surface hardness. Raster angle has a significant effect on the mechanical strength but not on the failure mechanism. In practice, FDM fabricated PEEK acted more like a laminate rather than a unified structure. Its main failure mechanism was correlated to the internal voids. The results show that horizontal infill orientation with 30° raster angle is promising for a better comprehensive mechanical performance, and the corresponding tensile, flexural, and shear strengths are (76.5 ± 1.4) MPa, (149.7 ± 3.0) MPa, and (55.5 ± 1.8) MPa, respectively. The findings of this study provide guidelines for FDM-PEEK to enable its realization in applications such as orthopedic implants.https://www.mdpi.com/2073-4360/14/1/77surface characteristicsmechanical propertiesfused deposition modeling (FDM)polyether-ether-ketone (PEEK)raster angle
spellingShingle Sasa Gao
Ruijuan Liu
Hua Xin
Haitao Liang
Yunfei Wang
Junhong Jia
The Surface Characteristics, Microstructure and Mechanical Properties of PEEK Printed by Fused Deposition Modeling with Different Raster Angles
Polymers
surface characteristics
mechanical properties
fused deposition modeling (FDM)
polyether-ether-ketone (PEEK)
raster angle
title The Surface Characteristics, Microstructure and Mechanical Properties of PEEK Printed by Fused Deposition Modeling with Different Raster Angles
title_full The Surface Characteristics, Microstructure and Mechanical Properties of PEEK Printed by Fused Deposition Modeling with Different Raster Angles
title_fullStr The Surface Characteristics, Microstructure and Mechanical Properties of PEEK Printed by Fused Deposition Modeling with Different Raster Angles
title_full_unstemmed The Surface Characteristics, Microstructure and Mechanical Properties of PEEK Printed by Fused Deposition Modeling with Different Raster Angles
title_short The Surface Characteristics, Microstructure and Mechanical Properties of PEEK Printed by Fused Deposition Modeling with Different Raster Angles
title_sort surface characteristics microstructure and mechanical properties of peek printed by fused deposition modeling with different raster angles
topic surface characteristics
mechanical properties
fused deposition modeling (FDM)
polyether-ether-ketone (PEEK)
raster angle
url https://www.mdpi.com/2073-4360/14/1/77
work_keys_str_mv AT sasagao thesurfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT ruijuanliu thesurfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT huaxin thesurfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT haitaoliang thesurfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT yunfeiwang thesurfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT junhongjia thesurfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT sasagao surfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT ruijuanliu surfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT huaxin surfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT haitaoliang surfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT yunfeiwang surfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles
AT junhongjia surfacecharacteristicsmicrostructureandmechanicalpropertiesofpeekprintedbyfuseddepositionmodelingwithdifferentrasterangles