Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields
Solvent-free synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones by ball-milling and without any catalyst is described. This method provides several advantages such as being environmentally friendly, using a simple workup procedure, and affording high yields.
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| Format: | Article |
| Language: | English |
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MDPI AG
2009-01-01
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| Series: | Molecules |
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| Online Access: | http://www.mdpi.com/1420-3049/14/1/474/ |
| _version_ | 1811286473424502784 |
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| author | M. Reza Naimi-Jamal Sara Mashkouri |
| author_facet | M. Reza Naimi-Jamal Sara Mashkouri |
| author_sort | M. Reza Naimi-Jamal |
| collection | DOAJ |
| description | Solvent-free synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones by ball-milling and without any catalyst is described. This method provides several advantages such as being environmentally friendly, using a simple workup procedure, and affording high yields. |
| first_indexed | 2024-04-13T03:00:32Z |
| format | Article |
| id | doaj.art-0a47870bc5f64dec8800756a824213cd |
| institution | Directory Open Access Journal |
| issn | 1420-3049 |
| language | English |
| last_indexed | 2024-04-13T03:00:32Z |
| publishDate | 2009-01-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Molecules |
| spelling | doaj.art-0a47870bc5f64dec8800756a824213cd2022-12-22T03:05:27ZengMDPI AGMolecules1420-30492009-01-0114147447910.3390/molecules14010474Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative YieldsM. Reza Naimi-JamalSara MashkouriSolvent-free synthesis of pyrano[2,3-d]pyrimidine-2,4(1H,3H)-diones by ball-milling and without any catalyst is described. This method provides several advantages such as being environmentally friendly, using a simple workup procedure, and affording high yields.http://www.mdpi.com/1420-3049/14/1/474/Solvent-free reactionBarbituric acidPyrimidinedionesHeterocyclic compoundsBall-milling |
| spellingShingle | M. Reza Naimi-Jamal Sara Mashkouri Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields Molecules Solvent-free reaction Barbituric acid Pyrimidinediones Heterocyclic compounds Ball-milling |
| title | Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields |
| title_full | Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields |
| title_fullStr | Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields |
| title_full_unstemmed | Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields |
| title_short | Mechanochemical Solvent-Free and Catalyst-Free One-Pot Synthesis of Pyrano[2,3-d]Pyrimidine-2,4(1H,3H)-Diones with Quantitative Yields |
| title_sort | mechanochemical solvent free and catalyst free one pot synthesis of pyrano 2 3 d pyrimidine 2 4 1h 3h diones with quantitative yields |
| topic | Solvent-free reaction Barbituric acid Pyrimidinediones Heterocyclic compounds Ball-milling |
| url | http://www.mdpi.com/1420-3049/14/1/474/ |
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