2-[2-(2-Anilino-4-oxo-3,4-dihydroquinazolin-3-yl)phenoxy]-3-phenylquinazolin-4(3H)-one methanol hemisolvate
In the title compound, C34H23N5O3·0.5CH3OH, each pyrimidinone heterocycle and its adjacent benzene ring are almost coplanar, making dihedral angles of 0.69 (13) and 1.87 (13)°. The lower pyrimidinone ring makes a dihedral angle of 40.41&#...
| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2010-08-01
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| Series: | Acta Crystallographica Section E |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536810028011 |
| _version_ | 1830410163650035712 |
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| author | Tao Gao Xiao-Bao Chen Xu-Hong Yang Xiang Wang |
| author_facet | Tao Gao Xiao-Bao Chen Xu-Hong Yang Xiang Wang |
| author_sort | Tao Gao |
| collection | DOAJ |
| description | In the title compound, C34H23N5O3·0.5CH3OH, each pyrimidinone heterocycle and its adjacent benzene ring are almost coplanar, making dihedral angles of 0.69 (13) and 1.87 (13)°. The lower pyrimidinone ring makes a dihedral angle of 40.41 (15)° with the —NH— bonded phenyl ring. O—H...O hydrogen bonds and weak C—H...π interactions are observed in the crystal structure. The methanol solvent molecule is disordered over two positions of equal occupancy. |
| first_indexed | 2024-12-20T19:25:47Z |
| format | Article |
| id | doaj.art-0ad303203e2b4cbd90a9fcffe097dc92 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-12-20T19:25:47Z |
| publishDate | 2010-08-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-0ad303203e2b4cbd90a9fcffe097dc922022-12-21T19:28:53ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-08-01668o2075o207610.1107/S16005368100280112-[2-(2-Anilino-4-oxo-3,4-dihydroquinazolin-3-yl)phenoxy]-3-phenylquinazolin-4(3H)-one methanol hemisolvateTao GaoXiao-Bao ChenXu-Hong YangXiang WangIn the title compound, C34H23N5O3·0.5CH3OH, each pyrimidinone heterocycle and its adjacent benzene ring are almost coplanar, making dihedral angles of 0.69 (13) and 1.87 (13)°. The lower pyrimidinone ring makes a dihedral angle of 40.41 (15)° with the —NH— bonded phenyl ring. O—H...O hydrogen bonds and weak C—H...π interactions are observed in the crystal structure. The methanol solvent molecule is disordered over two positions of equal occupancy.http://scripts.iucr.org/cgi-bin/paper?S1600536810028011 |
| spellingShingle | Tao Gao Xiao-Bao Chen Xu-Hong Yang Xiang Wang 2-[2-(2-Anilino-4-oxo-3,4-dihydroquinazolin-3-yl)phenoxy]-3-phenylquinazolin-4(3H)-one methanol hemisolvate Acta Crystallographica Section E |
| title | 2-[2-(2-Anilino-4-oxo-3,4-dihydroquinazolin-3-yl)phenoxy]-3-phenylquinazolin-4(3H)-one methanol hemisolvate |
| title_full | 2-[2-(2-Anilino-4-oxo-3,4-dihydroquinazolin-3-yl)phenoxy]-3-phenylquinazolin-4(3H)-one methanol hemisolvate |
| title_fullStr | 2-[2-(2-Anilino-4-oxo-3,4-dihydroquinazolin-3-yl)phenoxy]-3-phenylquinazolin-4(3H)-one methanol hemisolvate |
| title_full_unstemmed | 2-[2-(2-Anilino-4-oxo-3,4-dihydroquinazolin-3-yl)phenoxy]-3-phenylquinazolin-4(3H)-one methanol hemisolvate |
| title_short | 2-[2-(2-Anilino-4-oxo-3,4-dihydroquinazolin-3-yl)phenoxy]-3-phenylquinazolin-4(3H)-one methanol hemisolvate |
| title_sort | 2 2 2 anilino 4 oxo 3 4 dihydroquinazolin 3 yl phenoxy 3 phenylquinazolin 4 3h one methanol hemisolvate |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536810028011 |
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