Production of Biodiesel from Coconut Oil Using Microwave: Effect of Some Parameters on Transesterification Reaction by NaOH Catalyst

The purpose of this research was to study the effect of reaction time and NaOH catalyst in transesterification of coconut oil enhanced by microwave and to obtain a biodiesel. Reaction was conducted in batch reactor which equipped by microwave. Coconut oil contains saturated fatty acids about 70% wit...

Full description

Bibliographic Details
Main Authors: A. Suryanto, Suprapto Suprapto, Mahfud Mahfud
Format: Article
Language:English
Published: Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS) 2015-08-01
Series:Bulletin of Chemical Reaction Engineering & Catalysis
Subjects:
Online Access:https://journal.bcrec.id/index.php/bcrec/article/view/19367
_version_ 1827810203923382272
author A. Suryanto
Suprapto Suprapto
Mahfud Mahfud
author_facet A. Suryanto
Suprapto Suprapto
Mahfud Mahfud
author_sort A. Suryanto
collection DOAJ
description The purpose of this research was to study the effect of reaction time and NaOH catalyst in transesterification of coconut oil enhanced by microwave and to obtain a biodiesel. Reaction was conducted in batch reactor which equipped by microwave. Coconut oil contains saturated fatty acids about 70% with medium chain (C8-C14), especially lauric acid and myristic acid. The reaction was initiated by mixing oil and methanol with oil to methanol mole ratios of 1:3, 1:6, 1:9 and 1:12, catalyst concentration of 0.1, 0.15, 0.2, 0.25 and 0.3 wt.%, as well as setting electrical power at 100, 264 and 400 W. The reaction times were of  0.5, 1, 1.5, 2, 2.5, 3 and 3.5 min. The result showed that microwave could be employed as an energy source and was able to accelerate the transesterification process to produce biodiesel using NaOH catalyst. The biodiesel yields increase with increasing microwave power. The highest yield of biodiesel obtained  was of  97.37%  with reaction conditions set at 0.2 wt.% catalyst, a reaction time of 2 min, molar ratio of methanol to oil 1:9 and microwave power of 400 watt. © 2015 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)
first_indexed 2024-03-11T22:49:23Z
format Article
id doaj.art-0bdd8217fc8940fc8de2f955d705ba1c
institution Directory Open Access Journal
issn 1978-2993
language English
last_indexed 2024-03-11T22:49:23Z
publishDate 2015-08-01
publisher Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
record_format Article
series Bulletin of Chemical Reaction Engineering & Catalysis
spelling doaj.art-0bdd8217fc8940fc8de2f955d705ba1c2023-09-22T03:52:57ZengMasyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)Bulletin of Chemical Reaction Engineering & Catalysis1978-29932015-08-0110216216810.9767/bcrec.10.2.8080.162-1688085Production of Biodiesel from Coconut Oil Using Microwave: Effect of Some Parameters on Transesterification Reaction by NaOH CatalystA. Suryanto0Suprapto Suprapto1Mahfud Mahfud2Department of Chemical Engineering Faculty of Industrial Technology, Sepuluh Nopember Institute of Technology, Sukolilo, Surabaya 60111, IndonesiaDepartment of Chemical Engineering Faculty of Industrial Technology, Sepuluh Nopember Institute of Technology, Sukolilo, Surabaya 60111, IndonesiaDepartment of Chemical Engineering Faculty of Industrial Technology, Sepuluh Nopember Institute of Technology, Sukolilo, Surabaya 60111, IndonesiaThe purpose of this research was to study the effect of reaction time and NaOH catalyst in transesterification of coconut oil enhanced by microwave and to obtain a biodiesel. Reaction was conducted in batch reactor which equipped by microwave. Coconut oil contains saturated fatty acids about 70% with medium chain (C8-C14), especially lauric acid and myristic acid. The reaction was initiated by mixing oil and methanol with oil to methanol mole ratios of 1:3, 1:6, 1:9 and 1:12, catalyst concentration of 0.1, 0.15, 0.2, 0.25 and 0.3 wt.%, as well as setting electrical power at 100, 264 and 400 W. The reaction times were of  0.5, 1, 1.5, 2, 2.5, 3 and 3.5 min. The result showed that microwave could be employed as an energy source and was able to accelerate the transesterification process to produce biodiesel using NaOH catalyst. The biodiesel yields increase with increasing microwave power. The highest yield of biodiesel obtained  was of  97.37%  with reaction conditions set at 0.2 wt.% catalyst, a reaction time of 2 min, molar ratio of methanol to oil 1:9 and microwave power of 400 watt. © 2015 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0)https://journal.bcrec.id/index.php/bcrec/article/view/19367transesterificationbiodieselcoconut oilmicrowavenaoh catalyst
spellingShingle A. Suryanto
Suprapto Suprapto
Mahfud Mahfud
Production of Biodiesel from Coconut Oil Using Microwave: Effect of Some Parameters on Transesterification Reaction by NaOH Catalyst
Bulletin of Chemical Reaction Engineering & Catalysis
transesterification
biodiesel
coconut oil
microwave
naoh catalyst
title Production of Biodiesel from Coconut Oil Using Microwave: Effect of Some Parameters on Transesterification Reaction by NaOH Catalyst
title_full Production of Biodiesel from Coconut Oil Using Microwave: Effect of Some Parameters on Transesterification Reaction by NaOH Catalyst
title_fullStr Production of Biodiesel from Coconut Oil Using Microwave: Effect of Some Parameters on Transesterification Reaction by NaOH Catalyst
title_full_unstemmed Production of Biodiesel from Coconut Oil Using Microwave: Effect of Some Parameters on Transesterification Reaction by NaOH Catalyst
title_short Production of Biodiesel from Coconut Oil Using Microwave: Effect of Some Parameters on Transesterification Reaction by NaOH Catalyst
title_sort production of biodiesel from coconut oil using microwave effect of some parameters on transesterification reaction by naoh catalyst
topic transesterification
biodiesel
coconut oil
microwave
naoh catalyst
url https://journal.bcrec.id/index.php/bcrec/article/view/19367
work_keys_str_mv AT asuryanto productionofbiodieselfromcoconutoilusingmicrowaveeffectofsomeparametersontransesterificationreactionbynaohcatalyst
AT supraptosuprapto productionofbiodieselfromcoconutoilusingmicrowaveeffectofsomeparametersontransesterificationreactionbynaohcatalyst
AT mahfudmahfud productionofbiodieselfromcoconutoilusingmicrowaveeffectofsomeparametersontransesterificationreactionbynaohcatalyst