Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate
The title compound, C14H28N2O5S, was synthesized by the reaction of 2-[(methylsulfanyl)methyl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, molecules are linked by N—H...O and O—H...O hydrogen bonds into supramolecular chains propagating along the b-axis direction.
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2014-08-01
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| Series: | Acta Crystallographica Section E |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536814015062 |
| _version_ | 1798024449267597312 |
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| author | Xiao-Guang Bai Xiao-Yu Yang Ju-Xian Wang |
| author_facet | Xiao-Guang Bai Xiao-Yu Yang Ju-Xian Wang |
| author_sort | Xiao-Guang Bai |
| collection | DOAJ |
| description | The title compound, C14H28N2O5S, was synthesized by the reaction of 2-[(methylsulfanyl)methyl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, molecules are linked by N—H...O and O—H...O hydrogen bonds into supramolecular chains propagating along the b-axis direction. |
| first_indexed | 2024-04-11T18:03:46Z |
| format | Article |
| id | doaj.art-0c006ef8c3ae4c68bc2b686d8c428c16 |
| institution | Directory Open Access Journal |
| issn | 1600-5368 |
| language | English |
| last_indexed | 2024-04-11T18:03:46Z |
| publishDate | 2014-08-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E |
| spelling | doaj.art-0c006ef8c3ae4c68bc2b686d8c428c162022-12-22T04:10:23ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682014-08-01708o843o84310.1107/S1600536814015062xu5797Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylateXiao-Guang Bai0Xiao-Yu Yang1Ju-Xian Wang2Institute of Medicinal Biotechnology, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, People's Republic of ChinaHangDeXin (Beijing) Pharmatech. Co. Ltd, Fengtai District, Beijing 100050, People's Republic of ChinaInstitute of Medicinal Biotechnology, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, People's Republic of ChinaThe title compound, C14H28N2O5S, was synthesized by the reaction of 2-[(methylsulfanyl)methyl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, molecules are linked by N—H...O and O—H...O hydrogen bonds into supramolecular chains propagating along the b-axis direction.http://scripts.iucr.org/cgi-bin/paper?S1600536814015062crystal structure |
| spellingShingle | Xiao-Guang Bai Xiao-Yu Yang Ju-Xian Wang Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate Acta Crystallographica Section E crystal structure |
| title | Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate |
| title_full | Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate |
| title_fullStr | Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate |
| title_full_unstemmed | Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate |
| title_short | Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate |
| title_sort | di tert butyl 1 2 hydroxy 3 methylsulfanyl propyl hydrazine 1 2 dicarboxylate |
| topic | crystal structure |
| url | http://scripts.iucr.org/cgi-bin/paper?S1600536814015062 |
| work_keys_str_mv | AT xiaoguangbai ditertbutyl12hydroxy3methylsulfanylpropylhydrazine12dicarboxylate AT xiaoyuyang ditertbutyl12hydroxy3methylsulfanylpropylhydrazine12dicarboxylate AT juxianwang ditertbutyl12hydroxy3methylsulfanylpropylhydrazine12dicarboxylate |