(3,5-Dimethyladamantan-1-yl)ammonium methanesulfonate (memantinium mesylate): synthesis, structure and solid-state properties
The asymmetric unit of the title compound, C12H22N+·CH3O3S−, consists of three (3,5-dimethyladamantan-1-yl)ammonium cations, C12H22N+, and three methanesulfonate anions, CH3O3S−. In the crystal, the cations and anions associate via N—H...O hydrogen bonds into layers, parallel to the (001) plane, whi...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2019-08-01
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| Series: | Acta Crystallographica Section E: Crystallographic Communications |
| Subjects: | |
| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2056989019009988 |
| _version_ | 1831706157790527488 |
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| author | Mihaela Tuksar Mirta Rubčić Ernest Meštrović |
| author_facet | Mihaela Tuksar Mirta Rubčić Ernest Meštrović |
| author_sort | Mihaela Tuksar |
| collection | DOAJ |
| description | The asymmetric unit of the title compound, C12H22N+·CH3O3S−, consists of three (3,5-dimethyladamantan-1-yl)ammonium cations, C12H22N+, and three methanesulfonate anions, CH3O3S−. In the crystal, the cations and anions associate via N—H...O hydrogen bonds into layers, parallel to the (001) plane, which include large supramolecular hydrogen-bonded rings. |
| first_indexed | 2024-12-20T16:34:18Z |
| format | Article |
| id | doaj.art-0c35432bb6504aac977afe84e8b8e836 |
| institution | Directory Open Access Journal |
| issn | 2056-9890 |
| language | English |
| last_indexed | 2024-12-20T16:34:18Z |
| publishDate | 2019-08-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | Acta Crystallographica Section E: Crystallographic Communications |
| spelling | doaj.art-0c35432bb6504aac977afe84e8b8e8362022-12-21T19:33:11ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902019-08-017581274127910.1107/S2056989019009988fy2137(3,5-Dimethyladamantan-1-yl)ammonium methanesulfonate (memantinium mesylate): synthesis, structure and solid-state propertiesMihaela Tuksar0Mirta Rubčić1Ernest Meštrović2PLIVA Croatia Ltd., TAPI Research and Development, Prilaz baruna Filipovića 29, HR-10000 Zagreb, CroatiaDepartment of Chemistry, Faculty of Science, University of Zagreb, Horvatovac 102a, HR-10000 Zagreb, CroatiaPLIVA Croatia Ltd., TAPI Research and Development, Prilaz baruna Filipovića 29, HR-10000 Zagreb, CroatiaThe asymmetric unit of the title compound, C12H22N+·CH3O3S−, consists of three (3,5-dimethyladamantan-1-yl)ammonium cations, C12H22N+, and three methanesulfonate anions, CH3O3S−. In the crystal, the cations and anions associate via N—H...O hydrogen bonds into layers, parallel to the (001) plane, which include large supramolecular hydrogen-bonded rings.http://scripts.iucr.org/cgi-bin/paper?S2056989019009988crystal structurememantineX-ray diffractiondifferential scanning calorimetry (DSC)thermogravimetric analysis (TGA)IR spectroscopy |
| spellingShingle | Mihaela Tuksar Mirta Rubčić Ernest Meštrović (3,5-Dimethyladamantan-1-yl)ammonium methanesulfonate (memantinium mesylate): synthesis, structure and solid-state properties Acta Crystallographica Section E: Crystallographic Communications crystal structure memantine X-ray diffraction differential scanning calorimetry (DSC) thermogravimetric analysis (TGA) IR spectroscopy |
| title | (3,5-Dimethyladamantan-1-yl)ammonium methanesulfonate (memantinium mesylate): synthesis, structure and solid-state properties |
| title_full | (3,5-Dimethyladamantan-1-yl)ammonium methanesulfonate (memantinium mesylate): synthesis, structure and solid-state properties |
| title_fullStr | (3,5-Dimethyladamantan-1-yl)ammonium methanesulfonate (memantinium mesylate): synthesis, structure and solid-state properties |
| title_full_unstemmed | (3,5-Dimethyladamantan-1-yl)ammonium methanesulfonate (memantinium mesylate): synthesis, structure and solid-state properties |
| title_short | (3,5-Dimethyladamantan-1-yl)ammonium methanesulfonate (memantinium mesylate): synthesis, structure and solid-state properties |
| title_sort | 3 5 dimethyladamantan 1 yl ammonium methanesulfonate memantinium mesylate synthesis structure and solid state properties |
| topic | crystal structure memantine X-ray diffraction differential scanning calorimetry (DSC) thermogravimetric analysis (TGA) IR spectroscopy |
| url | http://scripts.iucr.org/cgi-bin/paper?S2056989019009988 |
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