Analysis of Shear Bond Strength and the Quality of the Interface Between Composite Resin and Novel Hybrid Calcium Silicate Cements

Hybrid calcium silicate cements (HCSC) are new bioactive materials of the fourth generation with the main application as pulp capping agents and/or as liners in indirect pulp capping. The aim is to analyze the shear bond strength and the quality of the interface between a composite restorative mater...

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Main Authors: Ivanka DIMITROVA, Desislava TSANOVA-TOSHEVA
Format: Article
Language:English
Published: Kaunas University of Technology 2023-05-01
Series:Medžiagotyra
Subjects:
Online Access:https://matsc.ktu.lt/index.php/MatSc/article/view/32064
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author Ivanka DIMITROVA
Desislava TSANOVA-TOSHEVA
author_facet Ivanka DIMITROVA
Desislava TSANOVA-TOSHEVA
author_sort Ivanka DIMITROVA
collection DOAJ
description Hybrid calcium silicate cements (HCSC) are new bioactive materials of the fourth generation with the main application as pulp capping agents and/or as liners in indirect pulp capping. The aim is to analyze the shear bond strength and the quality of the interface between a composite restorative material and a new bioactive material and other hybrid cements at the same conditions. The used pulp-capping hybrid materials: TheraCal and the new hybrid biomaterial BioCal-Cap. In this study only one type of adhesive system (Scotchbond 3M, St. Paul, MN, US) and resin-based composites (Filtek Ultimate 3M, USA) were used. For this purpose, 60 molds were prepared and divided into 4 groups. Half of them were filled with TheraCal and the other 30 with BioCal-Cap. The shear bond strength between calcium-silicate cements and the composite material was investigated. Mann-Whitney test and Wilcoxon Signed Ranks Test were used for statistical analysis of the results. In both of the materials there was no statistically significant difference in the results after the immediate and postponed placement of the composite material. Nevertheless, in both of them there was a tendency for a slight increase in shear strength in the samples which delayed the application of the restorative material. The novel hybrid material BioCal-Cap was reported to have higher shear strength values (18.06 – 20.25 MPa) at both time periods in comparison to the values for TheraCal (13.71 – 15.58 MPa). The data clearly showed that the time of the composite material placement did not affect the shear bond strength in each of the observed groups. The median value was shifted higher after the immediate composite placement, which supported one-step treatment approach to the novel hybrid material BioCal-Cap, while the TheraCal LC exhibited the opposite tendency. The adhesive layers in both hybrid cements were homogeneous, properly structured, without the presence of microcracks and gaps, and had different thicknesses at different recovery times.
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spelling doaj.art-0d335c486ff4451ab704eb62d80971ee2023-05-17T04:09:10ZengKaunas University of TechnologyMedžiagotyra1392-13202029-72892023-05-0110.5755/j02.ms.3206437318Analysis of Shear Bond Strength and the Quality of the Interface Between Composite Resin and Novel Hybrid Calcium Silicate CementsIvanka DIMITROVA0https://orcid.org/0000-0002-9434-2858Desislava TSANOVA-TOSHEVA1https://orcid.org/0000-0002-6090-9502Sofia Medical UniversitySofia Medical UniversityHybrid calcium silicate cements (HCSC) are new bioactive materials of the fourth generation with the main application as pulp capping agents and/or as liners in indirect pulp capping. The aim is to analyze the shear bond strength and the quality of the interface between a composite restorative material and a new bioactive material and other hybrid cements at the same conditions. The used pulp-capping hybrid materials: TheraCal and the new hybrid biomaterial BioCal-Cap. In this study only one type of adhesive system (Scotchbond 3M, St. Paul, MN, US) and resin-based composites (Filtek Ultimate 3M, USA) were used. For this purpose, 60 molds were prepared and divided into 4 groups. Half of them were filled with TheraCal and the other 30 with BioCal-Cap. The shear bond strength between calcium-silicate cements and the composite material was investigated. Mann-Whitney test and Wilcoxon Signed Ranks Test were used for statistical analysis of the results. In both of the materials there was no statistically significant difference in the results after the immediate and postponed placement of the composite material. Nevertheless, in both of them there was a tendency for a slight increase in shear strength in the samples which delayed the application of the restorative material. The novel hybrid material BioCal-Cap was reported to have higher shear strength values (18.06 – 20.25 MPa) at both time periods in comparison to the values for TheraCal (13.71 – 15.58 MPa). The data clearly showed that the time of the composite material placement did not affect the shear bond strength in each of the observed groups. The median value was shifted higher after the immediate composite placement, which supported one-step treatment approach to the novel hybrid material BioCal-Cap, while the TheraCal LC exhibited the opposite tendency. The adhesive layers in both hybrid cements were homogeneous, properly structured, without the presence of microcracks and gaps, and had different thicknesses at different recovery times.https://matsc.ktu.lt/index.php/MatSc/article/view/32064 pulp-capping materialscomposite materialshear bond strengthhybrid calcium silicate cementadhesive layer
spellingShingle Ivanka DIMITROVA
Desislava TSANOVA-TOSHEVA
Analysis of Shear Bond Strength and the Quality of the Interface Between Composite Resin and Novel Hybrid Calcium Silicate Cements
Medžiagotyra
pulp-capping materials
composite material
shear bond strength
hybrid calcium silicate cement
adhesive layer
title Analysis of Shear Bond Strength and the Quality of the Interface Between Composite Resin and Novel Hybrid Calcium Silicate Cements
title_full Analysis of Shear Bond Strength and the Quality of the Interface Between Composite Resin and Novel Hybrid Calcium Silicate Cements
title_fullStr Analysis of Shear Bond Strength and the Quality of the Interface Between Composite Resin and Novel Hybrid Calcium Silicate Cements
title_full_unstemmed Analysis of Shear Bond Strength and the Quality of the Interface Between Composite Resin and Novel Hybrid Calcium Silicate Cements
title_short Analysis of Shear Bond Strength and the Quality of the Interface Between Composite Resin and Novel Hybrid Calcium Silicate Cements
title_sort analysis of shear bond strength and the quality of the interface between composite resin and novel hybrid calcium silicate cements
topic pulp-capping materials
composite material
shear bond strength
hybrid calcium silicate cement
adhesive layer
url https://matsc.ktu.lt/index.php/MatSc/article/view/32064
work_keys_str_mv AT ivankadimitrova analysisofshearbondstrengthandthequalityoftheinterfacebetweencompositeresinandnovelhybridcalciumsilicatecements
AT desislavatsanovatosheva analysisofshearbondstrengthandthequalityoftheinterfacebetweencompositeresinandnovelhybridcalciumsilicatecements