Silver containing calcium phosphate bone cement with Ag/Ca atomic ratio equal to 0.05: synthesis and characterization

The introduction of silver into calcium phosphate bone cement (CPC) increases the strength and antimicrobial activity of the material. In this study, we synthesized silver-containing CPC by introducing silver phosphate salt Ag3PO4 in the cement powder with an Ag/Ca atomic ratio equal to 0.05. α-Tric...

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Main Authors: Brahim Chafik El Idrissi, Majda Fathi, Asmaa Massit, Salah-Eddin El Youbi
Format: Article
Language:English
Published: PURKH 2019-08-01
Series:To Chemistry Journal
Subjects:
Online Access:https://www.purkh.com/index.php/tochem/article/view/394
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author Brahim Chafik El Idrissi
Majda Fathi
Asmaa Massit
Salah-Eddin El Youbi
author_facet Brahim Chafik El Idrissi
Majda Fathi
Asmaa Massit
Salah-Eddin El Youbi
author_sort Brahim Chafik El Idrissi
collection DOAJ
description The introduction of silver into calcium phosphate bone cement (CPC) increases the strength and antimicrobial activity of the material. In this study, we synthesized silver-containing CPC by introducing silver phosphate salt Ag3PO4 in the cement powder with an Ag/Ca atomic ratio equal to 0.05. α-Tricalcium calcium phosphate (α-TCP, Ca3(PO4)2) and Hydroxyapatite (HA) were mixed with dicalcium phosphate dihydrate (DCPD, CaHPO4.2H2O) to form the cement powder. Deionized water (DI) solution was used as the cement fluid. CPC based on silver containing apatite phase was obtained. The phase composition and setting time of the cement was determined. The formation of apatite was verified by XRD and FTIR analysis, the initial and final setting times of the cement are 11 and 35 min.
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spelling doaj.art-0d66a7a1b90442bd82a524fe124310e12022-12-22T00:36:27ZengPURKHTo Chemistry Journal2581-75072019-08-013Silver containing calcium phosphate bone cement with Ag/Ca atomic ratio equal to 0.05: synthesis and characterizationBrahim Chafik El Idrissi0Majda FathiAsmaa MassitSalah-Eddin El YoubiUniversity Ibn TofailThe introduction of silver into calcium phosphate bone cement (CPC) increases the strength and antimicrobial activity of the material. In this study, we synthesized silver-containing CPC by introducing silver phosphate salt Ag3PO4 in the cement powder with an Ag/Ca atomic ratio equal to 0.05. α-Tricalcium calcium phosphate (α-TCP, Ca3(PO4)2) and Hydroxyapatite (HA) were mixed with dicalcium phosphate dihydrate (DCPD, CaHPO4.2H2O) to form the cement powder. Deionized water (DI) solution was used as the cement fluid. CPC based on silver containing apatite phase was obtained. The phase composition and setting time of the cement was determined. The formation of apatite was verified by XRD and FTIR analysis, the initial and final setting times of the cement are 11 and 35 min.https://www.purkh.com/index.php/tochem/article/view/394calcium phosphate cementSilversetting time
spellingShingle Brahim Chafik El Idrissi
Majda Fathi
Asmaa Massit
Salah-Eddin El Youbi
Silver containing calcium phosphate bone cement with Ag/Ca atomic ratio equal to 0.05: synthesis and characterization
To Chemistry Journal
calcium phosphate cement
Silver
setting time
title Silver containing calcium phosphate bone cement with Ag/Ca atomic ratio equal to 0.05: synthesis and characterization
title_full Silver containing calcium phosphate bone cement with Ag/Ca atomic ratio equal to 0.05: synthesis and characterization
title_fullStr Silver containing calcium phosphate bone cement with Ag/Ca atomic ratio equal to 0.05: synthesis and characterization
title_full_unstemmed Silver containing calcium phosphate bone cement with Ag/Ca atomic ratio equal to 0.05: synthesis and characterization
title_short Silver containing calcium phosphate bone cement with Ag/Ca atomic ratio equal to 0.05: synthesis and characterization
title_sort silver containing calcium phosphate bone cement with ag ca atomic ratio equal to 0 05 synthesis and characterization
topic calcium phosphate cement
Silver
setting time
url https://www.purkh.com/index.php/tochem/article/view/394
work_keys_str_mv AT brahimchafikelidrissi silvercontainingcalciumphosphatebonecementwithagcaatomicratioequalto005synthesisandcharacterization
AT majdafathi silvercontainingcalciumphosphatebonecementwithagcaatomicratioequalto005synthesisandcharacterization
AT asmaamassit silvercontainingcalciumphosphatebonecementwithagcaatomicratioequalto005synthesisandcharacterization
AT salaheddinelyoubi silvercontainingcalciumphosphatebonecementwithagcaatomicratioequalto005synthesisandcharacterization